Photooxidative decomposition and defluorination of perfluorooctanoic acid (PFOA) using an innovative technology of UV–vis/ZnxCu1-xFe2O4/oxalic acid
Per- and polyfluoroalkyl substances (PFAS) are a large group of perfluorinated organic molecules that have been in use since the 1940s for industrial, commercial, and consumer applications. PFAS are a growing concern because some of them have shown persistent, bioaccumulative and toxic effects. Here...
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| Published in | Chemosphere (Oxford) Vol. 280; no. C; p. 130660 |
|---|---|
| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
United Kingdom
Elsevier Ltd
01.10.2021
Elsevier |
| Subjects | |
| Online Access | Get full text |
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| Abstract | Per- and polyfluoroalkyl substances (PFAS) are a large group of perfluorinated organic molecules that have been in use since the 1940s for industrial, commercial, and consumer applications. PFAS are a growing concern because some of them have shown persistent, bioaccumulative and toxic effects. Herein, we demonstrate an innovative technology of UV–vis/ZnxCu1-xFe2O4/oxalic acid for the degradation of perfluorooctanoic acid (PFOA) in water. The magnetically retrievable nanocrystalline heterogeneous ferrite catalysts, ZnxCu1-xFe2O4 were synthesized using a sol-gel auto-combustion process followed by calcination at 400 °C. The combination of ZnxCu1-xFe2O4 and oxalic acid generate reactive species under UV light irradiation. These reactive species are then shown to be capable of the photodegradation of PFOA. The degree of degradation is tracked by identifying transformation products using liquid chromatography coupled with quadrupole time-of-flight mass spectroscopy (LC-QTOF-MS).
[Display omitted]
•Synthesis, characterization, and UV light performance of ZnxCu1-xFe2O4 catalysts.•UV light mediated in-situ generation of·OH radicals.•Heterogeneous photo-Fenton like system without the addition of H2O2.•Photo-mineralization of PFOA has been observed. |
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| AbstractList | Per- and polyfluoroalkyl substances (PFAS) are a large group of perfluorinated organic molecules that have been in use since the 1940s for industrial, commercial, and consumer applications. PFAS are a growing concern because some of them have shown persistent, bioaccumulative and toxic effects. Herein, we demonstrate an innovative technology of UVevis/Zn
x
Cu
1-x
Fe
2
O
4
/oxalic acid for the degradation of perfluorooctanoic acid (PFOA) in water. The magnetically retrievable nanocrystalline heterogeneous ferrite catalysts, Zn
x
Cu
1-x
Fe
2
O
4
were synthesized using a sol-gel auto-combustion process followed by calcination at 400 °C. The combination of Zn
x
Cu
1-x
Fe
2
O
4
and oxalic acid generate reactive species under UV light irradiation. These reactive species are then shown to be capable of the photodegradation of PFOA. The degree of degradation is tracked by identifying transformation products using liquid chromatography coupled with quadrupole time-of-flight mass spectroscopy (LC-QTOF-MS). Per- and polyfluoroalkyl substances (PFAS) are a large group of perfluorinated organic molecules that have been in use since the 1940s for industrial, commercial, and consumer applications. PFAS are a growing concern because some of them have shown persistent, bioaccumulative and toxic effects. Herein, we demonstrate an innovative technology of UV–vis/ZnxCu1-xFe2O4/oxalic acid for the degradation of perfluorooctanoic acid (PFOA) in water. The magnetically retrievable nanocrystalline heterogeneous ferrite catalysts, ZnxCu1-xFe2O4 were synthesized using a sol-gel auto-combustion process followed by calcination at 400 °C. The combination of ZnxCu1-xFe2O4 and oxalic acid generate reactive species under UV light irradiation. These reactive species are then shown to be capable of the photodegradation of PFOA. The degree of degradation is tracked by identifying transformation products using liquid chromatography coupled with quadrupole time-of-flight mass spectroscopy (LC-QTOF-MS). [Display omitted] •Synthesis, characterization, and UV light performance of ZnxCu1-xFe2O4 catalysts.•UV light mediated in-situ generation of·OH radicals.•Heterogeneous photo-Fenton like system without the addition of H2O2.•Photo-mineralization of PFOA has been observed. |
| ArticleNumber | 130660 |
| Author | Sahle-Demessie, Endalkachew Mezgebe, Bineyam Nadagouda, Mallikarjuna N. Verma, Sanny |
| AuthorAffiliation | b Pegasus Technical Services, Inc., 46 E. Hollister Street, Cincinnati, OH, 45219, USA a Oak Ridge Institute for Science and Education, P. O. Box 117, Oak Ridge, TN, 37831, USA c Land Remediation and Technology Division, Center for Environmental Solutions and Emergency Response, U. S. EPA, 26 West Martin Luther King Drive, Cincinnati, OH, 45268, USA d Water Infrastructure Division, Center for Environmental Solutions and Emergency Response, U. S. EPA, 26 West Martin Luther King Drive, Cincinnati, OH, 45268, USA |
| AuthorAffiliation_xml | – name: b Pegasus Technical Services, Inc., 46 E. Hollister Street, Cincinnati, OH, 45219, USA – name: c Land Remediation and Technology Division, Center for Environmental Solutions and Emergency Response, U. S. EPA, 26 West Martin Luther King Drive, Cincinnati, OH, 45268, USA – name: a Oak Ridge Institute for Science and Education, P. O. Box 117, Oak Ridge, TN, 37831, USA – name: d Water Infrastructure Division, Center for Environmental Solutions and Emergency Response, U. S. EPA, 26 West Martin Luther King Drive, Cincinnati, OH, 45268, USA |
| Author_xml | – sequence: 1 givenname: Sanny surname: Verma fullname: Verma, Sanny organization: Oak Ridge Institute for Science and Education, P. O. Box 117, Oak Ridge, TN, 37831, USA – sequence: 2 givenname: Bineyam surname: Mezgebe fullname: Mezgebe, Bineyam organization: Oak Ridge Institute for Science and Education, P. O. Box 117, Oak Ridge, TN, 37831, USA – sequence: 3 givenname: Endalkachew surname: Sahle-Demessie fullname: Sahle-Demessie, Endalkachew email: Sahle-Demessie.Endalkachew@epa.gov organization: Land Remediation and Technology Division, Center for Environmental Solutions and Emergency Response, U. S. EPA, 26 West Martin Luther King Drive, Cincinnati, OH, 45268, USA – sequence: 4 givenname: Mallikarjuna N. orcidid: 0000-0002-4800-4436 surname: Nadagouda fullname: Nadagouda, Mallikarjuna N. email: Nadagouda.Mallikarjuna@epa.gov organization: Water Infrastructure Division, Center for Environmental Solutions and Emergency Response, U. S. EPA, 26 West Martin Luther King Drive, Cincinnati, OH, 45268, USA |
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| Keywords | Magnetically retrievable catalyst UV–Vis Oxalic acid PFAS PFOA Heterogeneous photocatalytic system |
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| Snippet | Per- and polyfluoroalkyl substances (PFAS) are a large group of perfluorinated organic molecules that have been in use since the 1940s for industrial,... |
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| SubjectTerms | Heterogeneous photocatalytic system Magnetically retrievable catalyst Oxalic acid PFAS PFOA UV–Vis |
| Title | Photooxidative decomposition and defluorination of perfluorooctanoic acid (PFOA) using an innovative technology of UV–vis/ZnxCu1-xFe2O4/oxalic acid |
| URI | https://dx.doi.org/10.1016/j.chemosphere.2021.130660 https://www.osti.gov/biblio/1818550 https://pubmed.ncbi.nlm.nih.gov/PMC10353478 |
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