Phosphine- and ammonium-functionalized ordered mesoporous carbons as supports for cluster-derived metal nanoparticles
•An ordered mesoporous carbon was functionalized with ammonium or phosphine groups.•The surface functions were used as anchors for bimetallic cluster compounds.•The anchored clusters were ideal precursors of heterometallic nanoparticles.•Nanoparticles embedded within the mesopores of OMC were obtain...
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Published in | Catalysis today Vol. 235; pp. 112 - 126 |
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Main Authors | , , , , , |
Format | Journal Article Conference Proceeding Web Resource |
Language | English |
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Amsterdam
Elsevier B.V
15.10.2014
Elsevier Elsevier Science |
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Abstract | •An ordered mesoporous carbon was functionalized with ammonium or phosphine groups.•The surface functions were used as anchors for bimetallic cluster compounds.•The anchored clusters were ideal precursors of heterometallic nanoparticles.•Nanoparticles embedded within the mesopores of OMC were obtained.
An ordered mesoporous carbon (OMC) was functionalized with ammonium or chelating phosphine ligands. In both cases, the functionalization procedure started by oxidation by nitric acid treatment, followed by activation of surface carboxylic acid groups with thionyl chloride, then formation of amide bonds with diamines. The pendant amine groups were then either quaternized or further reacted with phosphine. The introduced functions were used as anchors for molecular mixed-metal clusters. These organometallic grafted species could then be thermally transformed into hetero-metallic nanoparticles (NP) embedded within the mesoporous framework. The NP/OMC nanocomposites could find application in hydrogenation heterogeneous catalysis or as electrodes in fuel cells. |
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AbstractList | An ordered mesoporous carbon (OMC) was functionalized with ammonium or chelating phosphine ligands. In both cases, the functionalization procedure started by oxidation by nitric acid treatment, followed by activation of surface carboxylic acid groups with thionyl chloride, then formation of amide bonds with diamines. The pendant amine groups were then either quaternized or further reacted with phosphine. The introduced functions were used as anchors for molecular mixed-metal clusters. These organometallic grafted species could then be thermally transformed into hetero-metallic nanoparticles (NP) embedded within the mesoporous framework. The NP/OMC nanocomposites could find application in hydrogenation, heterogeneous catalysis or as electrodes in fuel cells. •An ordered mesoporous carbon was functionalized with ammonium or phosphine groups.•The surface functions were used as anchors for bimetallic cluster compounds.•The anchored clusters were ideal precursors of heterometallic nanoparticles.•Nanoparticles embedded within the mesopores of OMC were obtained. An ordered mesoporous carbon (OMC) was functionalized with ammonium or chelating phosphine ligands. In both cases, the functionalization procedure started by oxidation by nitric acid treatment, followed by activation of surface carboxylic acid groups with thionyl chloride, then formation of amide bonds with diamines. The pendant amine groups were then either quaternized or further reacted with phosphine. The introduced functions were used as anchors for molecular mixed-metal clusters. These organometallic grafted species could then be thermally transformed into hetero-metallic nanoparticles (NP) embedded within the mesoporous framework. The NP/OMC nanocomposites could find application in hydrogenation heterogeneous catalysis or as electrodes in fuel cells. |
Author | Leonard, A.F. Devillers, M. Hermans, S. Delcorte, A. Vidick, D. Poleunis, C. |
Author_xml | – sequence: 1 givenname: D. surname: Vidick fullname: Vidick, D. organization: Institute of Condensed Matter and Nanosciences, Université catholique de Louvain, Place Louis Pasteur 1, 1348 Louvain-la-Neuve, Belgium – sequence: 2 givenname: A.F. surname: Leonard fullname: Leonard, A.F. organization: Laboratoire de Génie chimique-Nanomatériaux, Catalyse, Electrochimie, Université de Liège, Institut de Chimie, B6a, Sart-Tilman, B-4000 Liège, Belgium – sequence: 3 givenname: C. surname: Poleunis fullname: Poleunis, C. organization: Institute of Condensed Matter and Nanosciences, Université catholique de Louvain, Croix du Sud 1, 1348 Louvain-la-Neuve, Belgium – sequence: 4 givenname: A. surname: Delcorte fullname: Delcorte, A. organization: Institute of Condensed Matter and Nanosciences, Université catholique de Louvain, Croix du Sud 1, 1348 Louvain-la-Neuve, Belgium – sequence: 5 givenname: M. surname: Devillers fullname: Devillers, M. organization: Institute of Condensed Matter and Nanosciences, Université catholique de Louvain, Place Louis Pasteur 1, 1348 Louvain-la-Neuve, Belgium – sequence: 6 givenname: S. surname: Hermans fullname: Hermans, S. email: sophie.hermans@uclouvain.be organization: Institute of Condensed Matter and Nanosciences, Université catholique de Louvain, Place Louis Pasteur 1, 1348 Louvain-la-Neuve, Belgium |
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Keywords | Nanoparticles Cluster Functionalization Ordered mesoporous carbon Bimetallic Heterogeneous catalysis Support Nanoparticle Phosphine Porous material Carbon Mesoporosity |
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Snippet | •An ordered mesoporous carbon was functionalized with ammonium or phosphine groups.•The surface functions were used as anchors for bimetallic cluster... An ordered mesoporous carbon (OMC) was functionalized with ammonium or chelating phosphine ligands. In both cases, the functionalization procedure started by... |
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StartPage | 112 |
SubjectTerms | Bimetallic Catalysis Chemistry Chimie Cluster Colloidal state and disperse state Exact sciences and technology Functionalization General and physical chemistry Nanoparticles Ordered Mesoporous Carbon Physical and chemical studies. Granulometry. Electrokinetic phenomena Physical, chemical, mathematical & earth Sciences Physique, chimie, mathématiques & sciences de la terre Porous materials Theory of reactions, general kinetics. Catalysis. Nomenclature, chemical documentation, computer chemistry |
Title | Phosphine- and ammonium-functionalized ordered mesoporous carbons as supports for cluster-derived metal nanoparticles |
URI | https://dx.doi.org/10.1016/j.cattod.2014.03.017 http://orbi.ulg.ac.be/handle/2268/169864 |
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