A pH-stable positively charged composite nanofiltration membrane with excellent rejection performance
A novel kind of pH-stable positively charged composite nanofiltration (NF) membrane with excellent rejection performance was developed via interfacial polymerization on the surface of a polysulfone (PSF) ultrafiltration (UF) membrane, using a mixture of polyethyleneimine (PEI) and piperazine (PIP) a...
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| Published in | RSC advances Vol. 9; no. 64; pp. 37546 - 37555 |
|---|---|
| Main Authors | , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
England
Royal Society of Chemistry
18.11.2019
The Royal Society of Chemistry |
| Subjects | |
| Online Access | Get full text |
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| Abstract | A novel kind of pH-stable positively charged composite nanofiltration (NF) membrane with excellent rejection performance was developed
via
interfacial polymerization on the surface of a polysulfone (PSF) ultrafiltration (UF) membrane, using a mixture of polyethyleneimine (PEI) and piperazine (PIP) as the monomers of the aqueous phase, and cyanuric chloride (CC) as the monomer of the organic phase. The strong electron withdrawing and steric hindrance effects of the chloride group in the molecules of CC could protect the amido bond from the attack of hydrogen ions (H
+
) or hydroxyl ions (OH
−
) under acidic or alkaline conditions, thus the resultant polyamide composite membranes could be stable in acidic or alkali aqueous solution. A more compact PA active layer could be developed
via
mixing PIP into the PEI aqueous solution, where the PIP molecules could fill the pores of the polymer networks. There was no obvious change in the surface morphologies, the chemical structures, and the rejection performances after immersing the resultant polyamine composite NF membranes in the strong acidic solution (pH 1) and the strong alkaline solution (pH 13) for 30 days, respectively. The rejection performances of this kind of polyamine composite NF membranes could be adjusted through adjusting the mass ratio of PEI to PIP in the aqueous phase.
A pH-stable positively charged composite nanofiltration (NF) membrane was developed
via
the interfacial polymerization (IP) between polyethyleneimine (PEI), piperazine (PIP), and cyanuric chloride (CC). |
|---|---|
| AbstractList | A novel kind of pH-stable positively charged composite nanofiltration (NF) membrane with excellent rejection performance was developed via interfacial polymerization on the surface of a polysulfone (PSF) ultrafiltration (UF) membrane, using a mixture of polyethyleneimine (PEI) and piperazine (PIP) as the monomers of the aqueous phase, and cyanuric chloride (CC) as the monomer of the organic phase. The strong electron withdrawing and steric hindrance effects of the chloride group in the molecules of CC could protect the amido bond from the attack of hydrogen ions (H+) or hydroxyl ions (OH-) under acidic or alkaline conditions, thus the resultant polyamide composite membranes could be stable in acidic or alkali aqueous solution. A more compact PA active layer could be developed via mixing PIP into the PEI aqueous solution, where the PIP molecules could fill the pores of the polymer networks. There was no obvious change in the surface morphologies, the chemical structures, and the rejection performances after immersing the resultant polyamine composite NF membranes in the strong acidic solution (pH 1) and the strong alkaline solution (pH 13) for 30 days, respectively. The rejection performances of this kind of polyamine composite NF membranes could be adjusted through adjusting the mass ratio of PEI to PIP in the aqueous phase.A novel kind of pH-stable positively charged composite nanofiltration (NF) membrane with excellent rejection performance was developed via interfacial polymerization on the surface of a polysulfone (PSF) ultrafiltration (UF) membrane, using a mixture of polyethyleneimine (PEI) and piperazine (PIP) as the monomers of the aqueous phase, and cyanuric chloride (CC) as the monomer of the organic phase. The strong electron withdrawing and steric hindrance effects of the chloride group in the molecules of CC could protect the amido bond from the attack of hydrogen ions (H+) or hydroxyl ions (OH-) under acidic or alkaline conditions, thus the resultant polyamide composite membranes could be stable in acidic or alkali aqueous solution. A more compact PA active layer could be developed via mixing PIP into the PEI aqueous solution, where the PIP molecules could fill the pores of the polymer networks. There was no obvious change in the surface morphologies, the chemical structures, and the rejection performances after immersing the resultant polyamine composite NF membranes in the strong acidic solution (pH 1) and the strong alkaline solution (pH 13) for 30 days, respectively. The rejection performances of this kind of polyamine composite NF membranes could be adjusted through adjusting the mass ratio of PEI to PIP in the aqueous phase. A novel kind of pH-stable positively charged composite nanofiltration (NF) membrane with excellent rejection performance was developed via interfacial polymerization on the surface of a polysulfone (PSF) ultrafiltration (UF) membrane, using a mixture of polyethyleneimine (PEI) and piperazine (PIP) as the monomers of the aqueous phase, and cyanuric chloride (CC) as the monomer of the organic phase. The strong electron withdrawing and steric hindrance effects of the chloride group in the molecules of CC could protect the amido bond from the attack of hydrogen ions (H + ) or hydroxyl ions (OH − ) under acidic or alkaline conditions, thus the resultant polyamide composite membranes could be stable in acidic or alkali aqueous solution. A more compact PA active layer could be developed via mixing PIP into the PEI aqueous solution, where the PIP molecules could fill the pores of the polymer networks. There was no obvious change in the surface morphologies, the chemical structures, and the rejection performances after immersing the resultant polyamine composite NF membranes in the strong acidic solution (pH 1) and the strong alkaline solution (pH 13) for 30 days, respectively. The rejection performances of this kind of polyamine composite NF membranes could be adjusted through adjusting the mass ratio of PEI to PIP in the aqueous phase. A pH-stable positively charged composite nanofiltration (NF) membrane was developed via the interfacial polymerization (IP) between polyethyleneimine (PEI), piperazine (PIP), and cyanuric chloride (CC). A novel kind of pH-stable positively charged composite nanofiltration (NF) membrane with excellent rejection performance was developed via interfacial polymerization on the surface of a polysulfone (PSF) ultrafiltration (UF) membrane, using a mixture of polyethyleneimine (PEI) and piperazine (PIP) as the monomers of the aqueous phase, and cyanuric chloride (CC) as the monomer of the organic phase. The strong electron withdrawing and steric hindrance effects of the chloride group in the molecules of CC could protect the amido bond from the attack of hydrogen ions (H⁺) or hydroxyl ions (OH⁻) under acidic or alkaline conditions, thus the resultant polyamide composite membranes could be stable in acidic or alkali aqueous solution. A more compact PA active layer could be developed via mixing PIP into the PEI aqueous solution, where the PIP molecules could fill the pores of the polymer networks. There was no obvious change in the surface morphologies, the chemical structures, and the rejection performances after immersing the resultant polyamine composite NF membranes in the strong acidic solution (pH 1) and the strong alkaline solution (pH 13) for 30 days, respectively. The rejection performances of this kind of polyamine composite NF membranes could be adjusted through adjusting the mass ratio of PEI to PIP in the aqueous phase. A novel kind of pH-stable positively charged composite nanofiltration (NF) membrane with excellent rejection performance was developed via interfacial polymerization on the surface of a polysulfone (PSF) ultrafiltration (UF) membrane, using a mixture of polyethyleneimine (PEI) and piperazine (PIP) as the monomers of the aqueous phase, and cyanuric chloride (CC) as the monomer of the organic phase. The strong electron withdrawing and steric hindrance effects of the chloride group in the molecules of CC could protect the amido bond from the attack of hydrogen ions (H+) or hydroxyl ions (OH−) under acidic or alkaline conditions, thus the resultant polyamide composite membranes could be stable in acidic or alkali aqueous solution. A more compact PA active layer could be developed via mixing PIP into the PEI aqueous solution, where the PIP molecules could fill the pores of the polymer networks. There was no obvious change in the surface morphologies, the chemical structures, and the rejection performances after immersing the resultant polyamine composite NF membranes in the strong acidic solution (pH 1) and the strong alkaline solution (pH 13) for 30 days, respectively. The rejection performances of this kind of polyamine composite NF membranes could be adjusted through adjusting the mass ratio of PEI to PIP in the aqueous phase. A novel kind of pH-stable positively charged composite nanofiltration (NF) membrane with excellent rejection performance was developed via interfacial polymerization on the surface of a polysulfone (PSF) ultrafiltration (UF) membrane, using a mixture of polyethyleneimine (PEI) and piperazine (PIP) as the monomers of the aqueous phase, and cyanuric chloride (CC) as the monomer of the organic phase. The strong electron withdrawing and steric hindrance effects of the chloride group in the molecules of CC could protect the amido bond from the attack of hydrogen ions (H + ) or hydroxyl ions (OH − ) under acidic or alkaline conditions, thus the resultant polyamide composite membranes could be stable in acidic or alkali aqueous solution. A more compact PA active layer could be developed via mixing PIP into the PEI aqueous solution, where the PIP molecules could fill the pores of the polymer networks. There was no obvious change in the surface morphologies, the chemical structures, and the rejection performances after immersing the resultant polyamine composite NF membranes in the strong acidic solution (pH 1) and the strong alkaline solution (pH 13) for 30 days, respectively. The rejection performances of this kind of polyamine composite NF membranes could be adjusted through adjusting the mass ratio of PEI to PIP in the aqueous phase. A novel kind of pH-stable positively charged composite nanofiltration (NF) membrane with excellent rejection performance was developed interfacial polymerization on the surface of a polysulfone (PSF) ultrafiltration (UF) membrane, using a mixture of polyethyleneimine (PEI) and piperazine (PIP) as the monomers of the aqueous phase, and cyanuric chloride (CC) as the monomer of the organic phase. The strong electron withdrawing and steric hindrance effects of the chloride group in the molecules of CC could protect the amido bond from the attack of hydrogen ions (H ) or hydroxyl ions (OH ) under acidic or alkaline conditions, thus the resultant polyamide composite membranes could be stable in acidic or alkali aqueous solution. A more compact PA active layer could be developed mixing PIP into the PEI aqueous solution, where the PIP molecules could fill the pores of the polymer networks. There was no obvious change in the surface morphologies, the chemical structures, and the rejection performances after immersing the resultant polyamine composite NF membranes in the strong acidic solution (pH 1) and the strong alkaline solution (pH 13) for 30 days, respectively. The rejection performances of this kind of polyamine composite NF membranes could be adjusted through adjusting the mass ratio of PEI to PIP in the aqueous phase. |
| Author | Tu, Kai Hong, Xinjun Chen, Shunquan He, Yuantao Yang, Hao Zhang, Rui Zhang, Ling Jiang, Zhibin Miao, Jing Wang, Xi |
| AuthorAffiliation | Guangzhou Institute of Advanced Technology Chinese Academy of Sciences School of Chemistry and Environment South China Normal University School of Resource and Environment R & D Center Wuhan Institute of Technology Key Laboratory for Green Chemical Process of Ministry of Education Sinochem Ningbo River Membrane Technology Corp. Ltd Guangdong Key Laboratory of Membrane Materials and Membrane Separation School of Environmental Ecology and Biological Engineering University of Jinan |
| AuthorAffiliation_xml | – name: School of Resource and Environment – name: School of Chemistry and Environment – name: Chinese Academy of Sciences – name: Key Laboratory for Green Chemical Process of Ministry of Education – name: Guangzhou Institute of Advanced Technology – name: Wuhan Institute of Technology – name: School of Environmental Ecology and Biological Engineering – name: South China Normal University – name: Sinochem Ningbo River Membrane Technology Corp. Ltd – name: Guangdong Key Laboratory of Membrane Materials and Membrane Separation – name: University of Jinan – name: R & D Center |
| Author_xml | – sequence: 1 givenname: Zhibin surname: Jiang fullname: Jiang, Zhibin – sequence: 2 givenname: Jing surname: Miao fullname: Miao, Jing – sequence: 3 givenname: Yuantao surname: He fullname: He, Yuantao – sequence: 4 givenname: Xinjun surname: Hong fullname: Hong, Xinjun – sequence: 5 givenname: Kai surname: Tu fullname: Tu, Kai – sequence: 6 givenname: Xi surname: Wang fullname: Wang, Xi – sequence: 7 givenname: Shunquan surname: Chen fullname: Chen, Shunquan – sequence: 8 givenname: Hao surname: Yang fullname: Yang, Hao – sequence: 9 givenname: Ling surname: Zhang fullname: Zhang, Ling – sequence: 10 givenname: Rui surname: Zhang fullname: Zhang, Rui |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/35542300$$D View this record in MEDLINE/PubMed |
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| Snippet | A novel kind of pH-stable positively charged composite nanofiltration (NF) membrane with excellent rejection performance was developed
via
interfacial... A novel kind of pH-stable positively charged composite nanofiltration (NF) membrane with excellent rejection performance was developed interfacial... A novel kind of pH-stable positively charged composite nanofiltration (NF) membrane with excellent rejection performance was developed via interfacial... |
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| SubjectTerms | Aqueous solutions asymmetric membranes Chemical attack chemical structure Chemistry Chlorides cyanuric chloride Hydrogen ions Hydroxyl ions Membranes mixing Monomers Morphology Nanofiltration Organic chemistry piperazine Polyamide resins polyamides Polyamines Polyethyleneimine polymerization Polysulfone resins protons Rejection Steric hindrance Ultrafiltration |
| Title | A pH-stable positively charged composite nanofiltration membrane with excellent rejection performance |
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