Adsorption of phenol and o-chlorophenol by mesoporous MCM-41
Water pollution by toxic organic compounds is of concern and the demand for effective adsorbents for the removal of toxic compounds is increasing. Present work deals with the adsorption of phenol (PhOH) and o-chlorophenol ( o-CP) on mesoporous MCM-41 material. The effect of surfactant template in MC...
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| Published in | Journal of hazardous materials Vol. 160; no. 2; pp. 414 - 421 |
|---|---|
| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
Kidlington
Elsevier B.V
30.12.2008
Elsevier |
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| Online Access | Get full text |
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| Abstract | Water pollution by toxic organic compounds is of concern and the demand for effective adsorbents for the removal of toxic compounds is increasing. Present work deals with the adsorption of phenol (PhOH) and
o-chlorophenol (
o-CP) on mesoporous MCM-41 material. The effect of surfactant template in MCM-41 on the removal of PhOH and
o-CP was investigated. The comparison of adsorption of PhOH and
o-CP on uncalcined MCM-41 (noted as MCM-41) and calcined MCM-41 (noted as C-MCM-41) was investigated. It was found that MCM-41 shows significant adsorption for PhOH and
o-CP as compared to C-MCM-41, this may be because of the hydrophobicity created by surfactant template in the MCM-41. Batch adsorption studies were carried out to study the effect of various parameters like adsorbent dose, pH, initial concentration and the presence of co-existing ions. It was found that adsorption of PhOH and
o-CP depends upon the solution pH as well as co-existing ions present in the aqueous solution. The equilibrium adsorption data for PhOH and
o-CP was analyzed by using Freundlich adsorption isotherm model. From the sorption studies it was observed that the uptake of
o-CP was higher than PhOH. |
|---|---|
| AbstractList | Water pollution by toxic organic compounds is of concern and the demand for effective adsorbents for the removal of toxic compounds is increasing. Present work deals with the adsorption of phenol (PhOH) and o-chlorophenol (o-CP) on mesoporous MCM-41 material. The effect of surfactant template in MCM-41 on the removal of PhOH and o-CP was investigated. The comparison of adsorption of PhOH and o-CP on uncalcined MCM-41 (noted as MCM-41) and calcined MCM-41 (noted as C-MCM-41) was investigated. It was found that MCM-41 shows significant adsorption for PhOH and o-CP as compared to C-MCM-41, this may be because of the hydrophobicity created by surfactant template in the MCM-41. Batch adsorption studies were carried out to study the effect of various parameters like adsorbent dose, pH, initial concentration and the presence of co-existing ions. It was found that adsorption of PhOH and o-CP depends upon the solution pH as well as co-existing ions present in the aqueous solution. The equilibrium adsorption data for PhOH and o-CP was analyzed by using Freundlich adsorption isotherm model. From the sorption studies it was observed that the uptake of o-CP was higher than PhOH. The sorption properties of MCM-41 with C-MCM-41 (members of family of silicate mesoporous material) to assess quantitatively the role of the organic template were compared. The adsorbents were characterized with respect to surface area, particle size, XRD and Fourier Transform Infrared (FTIR). The specific surface areas of adsorbent samples were determined using a specific surface area analyzer with nitrogen gas as the adsorbate and the particle size was determined on Fritsch particle sizer. The BET surface area of the mesoporous MCM-41 was found to be 45.1m super(2) g super(-1), which was very low as compared to the C-MCM-41. It was concluded that pH and the presence of co-existing ions play an important role in the removal of phenol (PhOH) and o-CP from wastewater. Water pollution by toxic organic compounds is of concern and the demand for effective adsorbents for the removal of toxic compounds is increasing. Present work deals with the adsorption of phenol (PhOH) and o-chlorophenol ( o-CP) on mesoporous MCM-41 material. The effect of surfactant template in MCM-41 on the removal of PhOH and o-CP was investigated. The comparison of adsorption of PhOH and o-CP on uncalcined MCM-41 (noted as MCM-41) and calcined MCM-41 (noted as C-MCM-41) was investigated. It was found that MCM-41 shows significant adsorption for PhOH and o-CP as compared to C-MCM-41, this may be because of the hydrophobicity created by surfactant template in the MCM-41. Batch adsorption studies were carried out to study the effect of various parameters like adsorbent dose, pH, initial concentration and the presence of co-existing ions. It was found that adsorption of PhOH and o-CP depends upon the solution pH as well as co-existing ions present in the aqueous solution. The equilibrium adsorption data for PhOH and o-CP was analyzed by using Freundlich adsorption isotherm model. From the sorption studies it was observed that the uptake of o-CP was higher than PhOH. |
| Author | Mangrulkar, Priti A. Kamble, Sanjay P. Meshram, J. Rayalu, Sadhana S. |
| Author_xml | – sequence: 1 givenname: Priti A. surname: Mangrulkar fullname: Mangrulkar, Priti A. organization: Environmental Materials Unit, National Environmental Engineering Research Institute (CSIR), Nagpur 440 020, India – sequence: 2 givenname: Sanjay P. surname: Kamble fullname: Kamble, Sanjay P. organization: Environmental Materials Unit, National Environmental Engineering Research Institute (CSIR), Nagpur 440 020, India – sequence: 3 givenname: J. surname: Meshram fullname: Meshram, J. organization: Chemistry Department, RTM, Nagpur University, Nagpur, India – sequence: 4 givenname: Sadhana S. surname: Rayalu fullname: Rayalu, Sadhana S. email: s_rayalu@neeri.res.in organization: Environmental Materials Unit, National Environmental Engineering Research Institute (CSIR), Nagpur 440 020, India |
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| Keywords | pH and anion effects TMAOH o-Chlorophenol MCM-41 CTAB Phenol Mesoporous MCM-41 PhOH Adsorption Surfactant template o-CP HDTMA TMOS C-MCM-41 Adsorption isotherm Hydrophobicity Surfactant Modeling Uptake Calcining Sorption Batchwise Phenols pH Water pollution Aqueous solution |
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| Snippet | Water pollution by toxic organic compounds is of concern and the demand for effective adsorbents for the removal of toxic compounds is increasing. Present work... The sorption properties of MCM-41 with C-MCM-41 (members of family of silicate mesoporous material) to assess quantitatively the role of the organic template... |
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| SubjectTerms | Adsorption Anions - chemistry Applied sciences Biological and physicochemical phenomena Cetrimonium Compounds - chemistry Chemical engineering Chlorophenols - isolation & purification Exact sciences and technology Hydrogen-Ion Concentration Indicators and Reagents Kinetics Mesoporous MCM-41 Natural water pollution o-Chlorophenol pH and anion effects Phenol Phenols - isolation & purification Pollution Porosity Silicon Dioxide - chemistry Spectroscopy, Fourier Transform Infrared Surface-Active Agents - analysis Surfactant template Thermodynamics Water Pollutants, Chemical - analysis Water treatment and pollution X-Ray Diffraction |
| Title | Adsorption of phenol and o-chlorophenol by mesoporous MCM-41 |
| URI | https://dx.doi.org/10.1016/j.jhazmat.2008.03.013 https://www.ncbi.nlm.nih.gov/pubmed/18524474 https://search.proquest.com/docview/14036322 https://search.proquest.com/docview/19687132 https://search.proquest.com/docview/35723240 |
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