High‐Density Nanopore Confined Vortical Dipoles and Magnetic Domains on Hierarchical Macro/Meso/Micro/Nano Porous Ultra‐Light Graphited Carbon for Adsorbing Electromagnetic Wave
Atomic‐level structural editing is a promising way for facile synthesis and accurately constructing dielectric/magnetic synergistic attenuated hetero‐units in electromagnetic wave absorbers (EWAs), but it is hard to realize. Herein, utilizing the rapid explosive volume expansion of the CoFe‐bimetall...
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| Published in | Advanced science Vol. 10; no. 28; pp. e2303217 - n/a |
|---|---|
| Main Authors | , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Germany
John Wiley & Sons, Inc
01.10.2023
John Wiley and Sons Inc Wiley |
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| Abstract | Atomic‐level structural editing is a promising way for facile synthesis and accurately constructing dielectric/magnetic synergistic attenuated hetero‐units in electromagnetic wave absorbers (EWAs), but it is hard to realize. Herein, utilizing the rapid explosive volume expansion of the CoFe‐bimetallic energetic metallic triazole framework (CoFe@E‐MTF) during the heat treatment, the effective absorption bandwidth and the maximum absorption intensity of a series of atomic CoFe‐inserted hierarchical porous carbon (CoFe@HPC) EWAs can be modified under the diverse synthetic temperature. Under the filler loading of 15 wt%, the fully covered X and Ku bands at 3 and 2.5 mm for CoFe@HPC800 and the superb minimum reflection loss (
RL
min
) of −53.15 dB and specific reflection loss (
SRL
) of −101.24 dB mg
−1
mm
−1
for CoFe@HPC1000 are achieved. More importantly, the single‐atomic chemical bonding among Co─Fe on the nanopores is captured by extended X‐ray absorption fine structure, which reveals the formation mechanism of nanopore‐confined vortical dipoles and magnetic domains. This work heralds the infinite possibilities of atomic editing EWA in the future. |
|---|---|
| AbstractList | Abstract Atomic‐level structural editing is a promising way for facile synthesis and accurately constructing dielectric/magnetic synergistic attenuated hetero‐units in electromagnetic wave absorbers (EWAs), but it is hard to realize. Herein, utilizing the rapid explosive volume expansion of the CoFe‐bimetallic energetic metallic triazole framework (CoFe@E‐MTF) during the heat treatment, the effective absorption bandwidth and the maximum absorption intensity of a series of atomic CoFe‐inserted hierarchical porous carbon (CoFe@HPC) EWAs can be modified under the diverse synthetic temperature. Under the filler loading of 15 wt%, the fully covered X and Ku bands at 3 and 2.5 mm for CoFe@HPC800 and the superb minimum reflection loss (RLmin) of −53.15 dB and specific reflection loss (SRL) of −101.24 dB mg−1 mm−1 for CoFe@HPC1000 are achieved. More importantly, the single‐atomic chemical bonding among Co─Fe on the nanopores is captured by extended X‐ray absorption fine structure, which reveals the formation mechanism of nanopore‐confined vortical dipoles and magnetic domains. This work heralds the infinite possibilities of atomic editing EWA in the future. Atomic‐level structural editing is a promising way for facile synthesis and accurately constructing dielectric/magnetic synergistic attenuated hetero‐units in electromagnetic wave absorbers (EWAs), but it is hard to realize. Herein, utilizing the rapid explosive volume expansion of the CoFe‐bimetallic energetic metallic triazole framework (CoFe@E‐MTF) during the heat treatment, the effective absorption bandwidth and the maximum absorption intensity of a series of atomic CoFe‐inserted hierarchical porous carbon (CoFe@HPC) EWAs can be modified under the diverse synthetic temperature. Under the filler loading of 15 wt%, the fully covered X and Ku bands at 3 and 2.5 mm for CoFe@HPC800 and the superb minimum reflection loss ( RL min ) of −53.15 dB and specific reflection loss ( SRL ) of −101.24 dB mg −1 mm −1 for CoFe@HPC1000 are achieved. More importantly, the single‐atomic chemical bonding among Co─Fe on the nanopores is captured by extended X‐ray absorption fine structure, which reveals the formation mechanism of nanopore‐confined vortical dipoles and magnetic domains. This work heralds the infinite possibilities of atomic editing EWA in the future. Atomic-level structural editing is a promising way for facile synthesis and accurately constructing dielectric/magnetic synergistic attenuated hetero-units in electromagnetic wave absorbers (EWAs), but it is hard to realize. Herein, utilizing the rapid explosive volume expansion of the CoFe-bimetallic energetic metallic triazole framework (CoFe@E-MTF) during the heat treatment, the effective absorption bandwidth and the maximum absorption intensity of a series of atomic CoFe-inserted hierarchical porous carbon (CoFe@HPC) EWAs can be modified under the diverse synthetic temperature. Under the filler loading of 15 wt%, the fully covered X and Ku bands at 3 and 2.5 mm for CoFe@HPC800 and the superb minimum reflection loss (RLmin) of −53.15 dB and specific reflection loss (SRL) of −101.24 dB mg−1 mm−1 for CoFe@HPC1000 are achieved. More importantly, the single-atomic chemical bonding among Co─Fe on the nanopores is captured by extended X-ray absorption fine structure, which reveals the formation mechanism of nanopore-confined vortical dipoles and magnetic domains. This work heralds the infinite possibilities of atomic editing EWA in the future. Atomic-level structural editing is a promising way for facile synthesis and accurately constructing dielectric/magnetic synergistic attenuated hetero-units in electromagnetic wave absorbers (EWAs), but it is hard to realize. Herein, utilizing the rapid explosive volume expansion of the CoFe-bimetallic energetic metallic triazole framework (CoFe@E-MTF) during the heat treatment, the effective absorption bandwidth and the maximum absorption intensity of a series of atomic CoFe-inserted hierarchical porous carbon (CoFe@HPC) EWAs can be modified under the diverse synthetic temperature. Under the filler loading of 15 wt%, the fully covered X and Ku bands at 3 and 2.5 mm for CoFe@HPC800 and the superb minimum reflection loss (RLmin ) of -53.15 dB and specific reflection loss (SRL) of -101.24 dB mg-1 mm-1 for CoFe@HPC1000 are achieved. More importantly, the single-atomic chemical bonding among Co─Fe on the nanopores is captured by extended X-ray absorption fine structure, which reveals the formation mechanism of nanopore-confined vortical dipoles and magnetic domains. This work heralds the infinite possibilities of atomic editing EWA in the future.Atomic-level structural editing is a promising way for facile synthesis and accurately constructing dielectric/magnetic synergistic attenuated hetero-units in electromagnetic wave absorbers (EWAs), but it is hard to realize. Herein, utilizing the rapid explosive volume expansion of the CoFe-bimetallic energetic metallic triazole framework (CoFe@E-MTF) during the heat treatment, the effective absorption bandwidth and the maximum absorption intensity of a series of atomic CoFe-inserted hierarchical porous carbon (CoFe@HPC) EWAs can be modified under the diverse synthetic temperature. Under the filler loading of 15 wt%, the fully covered X and Ku bands at 3 and 2.5 mm for CoFe@HPC800 and the superb minimum reflection loss (RLmin ) of -53.15 dB and specific reflection loss (SRL) of -101.24 dB mg-1 mm-1 for CoFe@HPC1000 are achieved. More importantly, the single-atomic chemical bonding among Co─Fe on the nanopores is captured by extended X-ray absorption fine structure, which reveals the formation mechanism of nanopore-confined vortical dipoles and magnetic domains. This work heralds the infinite possibilities of atomic editing EWA in the future. Atomic‐level structural editing is a promising way for facile synthesis and accurately constructing dielectric/magnetic synergistic attenuated hetero‐units in electromagnetic wave absorbers (EWAs), but it is hard to realize. Herein, utilizing the rapid explosive volume expansion of the CoFe‐bimetallic energetic metallic triazole framework (CoFe@E‐MTF) during the heat treatment, the effective absorption bandwidth and the maximum absorption intensity of a series of atomic CoFe‐inserted hierarchical porous carbon (CoFe@HPC) EWAs can be modified under the diverse synthetic temperature. Under the filler loading of 15 wt%, the fully covered X and Ku bands at 3 and 2.5 mm for CoFe@HPC800 and the superb minimum reflection loss ( RL min ) of −53.15 dB and specific reflection loss ( SRL ) of −101.24 dB mg −1 mm −1 for CoFe@HPC1000 are achieved. More importantly, the single‐atomic chemical bonding among Co─Fe on the nanopores is captured by extended X‐ray absorption fine structure, which reveals the formation mechanism of nanopore‐confined vortical dipoles and magnetic domains. This work heralds the infinite possibilities of atomic editing EWA in the future. Four CoFe‐inserted hierarchical porous carbon captured under different temperatures revealed the evolution of Co/Fe from clusters to single atom states through XANES and EXAFS. The LTEM and hologram in situ monitor the high‐density nano‐vortex dipoles and magnetic domains on 3D network. The bifunctional regulation of fully covered X/Ku bands and superb specific reflection loss of −101.24 dB mg −1 mm −1 are achieved. Atomic-level structural editing is a promising way for facile synthesis and accurately constructing dielectric/magnetic synergistic attenuated hetero-units in electromagnetic wave absorbers (EWAs), but it is hard to realize. Herein, utilizing the rapid explosive volume expansion of the CoFe-bimetallic energetic metallic triazole framework (CoFe@E-MTF) during the heat treatment, the effective absorption bandwidth and the maximum absorption intensity of a series of atomic CoFe-inserted hierarchical porous carbon (CoFe@HPC) EWAs can be modified under the diverse synthetic temperature. Under the filler loading of 15 wt%, the fully covered X and Ku bands at 3 and 2.5 mm for CoFe@HPC800 and the superb minimum reflection loss (RL ) of -53.15 dB and specific reflection loss (SRL) of -101.24 dB mg mm for CoFe@HPC1000 are achieved. More importantly, the single-atomic chemical bonding among Co─Fe on the nanopores is captured by extended X-ray absorption fine structure, which reveals the formation mechanism of nanopore-confined vortical dipoles and magnetic domains. This work heralds the infinite possibilities of atomic editing EWA in the future. |
| Author | Zuo, Shouwei Zhang, Xingxing Che, Renchao Zhang, Jincang Kang, Yifan Huang, Wenhuan Qiu, Qiang Pei, Ke Chen, Jiamin |
| AuthorAffiliation | 2 Laboratory of Advanced Materials Shanghai Key Lab of Molecular Catalysis and Innovative Materials Academy for Engineering & Technology Fudan University Shanghai 200438 P. R. China 1 Key Laboratory of Chemical Additives for China National Light Industry College of Chemistry and Chemical Engineering Shaanxi University of Science and Technology Xi'an 710021 China 3 Zhejiang Laboratory Hangzhou 311100 P. R. China |
| AuthorAffiliation_xml | – name: 2 Laboratory of Advanced Materials Shanghai Key Lab of Molecular Catalysis and Innovative Materials Academy for Engineering & Technology Fudan University Shanghai 200438 P. R. China – name: 1 Key Laboratory of Chemical Additives for China National Light Industry College of Chemistry and Chemical Engineering Shaanxi University of Science and Technology Xi'an 710021 China – name: 3 Zhejiang Laboratory Hangzhou 311100 P. R. China |
| Author_xml | – sequence: 1 givenname: Wenhuan surname: Huang fullname: Huang, Wenhuan organization: Key Laboratory of Chemical Additives for China National Light Industry College of Chemistry and Chemical Engineering Shaanxi University of Science and Technology Xi'an 710021 China – sequence: 2 givenname: Xingxing surname: Zhang fullname: Zhang, Xingxing organization: Key Laboratory of Chemical Additives for China National Light Industry College of Chemistry and Chemical Engineering Shaanxi University of Science and Technology Xi'an 710021 China – sequence: 3 givenname: Jiamin surname: Chen fullname: Chen, Jiamin organization: Key Laboratory of Chemical Additives for China National Light Industry College of Chemistry and Chemical Engineering Shaanxi University of Science and Technology Xi'an 710021 China – sequence: 4 givenname: Qiang surname: Qiu fullname: Qiu, Qiang organization: Key Laboratory of Chemical Additives for China National Light Industry College of Chemistry and Chemical Engineering Shaanxi University of Science and Technology Xi'an 710021 China – sequence: 5 givenname: Yifan surname: Kang fullname: Kang, Yifan organization: Key Laboratory of Chemical Additives for China National Light Industry College of Chemistry and Chemical Engineering Shaanxi University of Science and Technology Xi'an 710021 China – sequence: 6 givenname: Ke surname: Pei fullname: Pei, Ke organization: Laboratory of Advanced Materials Shanghai Key Lab of Molecular Catalysis and Innovative Materials Academy for Engineering & Technology Fudan University Shanghai 200438 P. R. China – sequence: 7 givenname: Shouwei surname: Zuo fullname: Zuo, Shouwei organization: Key Laboratory of Chemical Additives for China National Light Industry College of Chemistry and Chemical Engineering Shaanxi University of Science and Technology Xi'an 710021 China – sequence: 8 givenname: Jincang surname: Zhang fullname: Zhang, Jincang organization: Zhejiang Laboratory Hangzhou 311100 P. R. China – sequence: 9 givenname: Renchao orcidid: 0000-0002-6583-7114 surname: Che fullname: Che, Renchao organization: Laboratory of Advanced Materials Shanghai Key Lab of Molecular Catalysis and Innovative Materials Academy for Engineering & Technology Fudan University Shanghai 200438 P. R. China, Zhejiang Laboratory Hangzhou 311100 P. R. China |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/37526339$$D View this record in MEDLINE/PubMed |
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| Copyright | 2023 The Authors. Advanced Science published by Wiley-VCH GmbH. 2023. This work is published under http://creativecommons.org/licenses/by/4.0/ (the “License”). Notwithstanding the ProQuest Terms and Conditions, you may use this content in accordance with the terms of the License. 2023 The Authors. Advanced Science published by Wiley‐VCH GmbH |
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| Keywords | vortical dipole electron holography electromagnetic wave absorber magnetic domain energetic metal-organic framework |
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| License | 2023 The Authors. Advanced Science published by Wiley-VCH GmbH. This is an open access article under the terms of the http://creativecommons.org/licenses/by/4.0/ License, which permits use, distribution and reproduction in any medium, provided the original work is properly cited. |
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| Snippet | Atomic‐level structural editing is a promising way for facile synthesis and accurately constructing dielectric/magnetic synergistic attenuated hetero‐units in... Atomic-level structural editing is a promising way for facile synthesis and accurately constructing dielectric/magnetic synergistic attenuated hetero-units in... Abstract Atomic‐level structural editing is a promising way for facile synthesis and accurately constructing dielectric/magnetic synergistic attenuated... |
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| SubjectTerms | Bandwidths Carbon electromagnetic wave absorber electron holography energetic metal‐organic framework High temperature magnetic domain Metals Morphology Spectrum analysis vortical dipole |
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| Title | High‐Density Nanopore Confined Vortical Dipoles and Magnetic Domains on Hierarchical Macro/Meso/Micro/Nano Porous Ultra‐Light Graphited Carbon for Adsorbing Electromagnetic Wave |
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