Chemical etching and phase transformation of Nickel-Cobalt Prussian blue analogs for improved solar-driven water-splitting applications
[Display omitted] Although Prussian blue and its analogs (PB/PBAs) have open framework structures, large surface areas, uniform metal active sites, and tunable compositions, and have been investigated for a long time, owing to their unfavorable visible light responsiveness, they rarely been reported...
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| Published in | Journal of Colloid and Interface Science Vol. 641; pp. 861 - 874 |
|---|---|
| Main Authors | , , |
| Format | Journal Article |
| Language | English |
| Published |
United States
Elsevier Inc
01.07.2023
Elsevier BV |
| Subjects | |
| Online Access | Get full text |
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| Abstract | [Display omitted]
Although Prussian blue and its analogs (PB/PBAs) have open framework structures, large surface areas, uniform metal active sites, and tunable compositions, and have been investigated for a long time, owing to their unfavorable visible light responsiveness, they rarely been reported in photocatalysis. This largely limits their applications in solar-to-chemical energy conversion. Here, a continuous-evolution strategy was conducted to convert the poor-performance NiCo PBA (NCP) toward high-efficiency complex photocatalytic nanomaterials. First, chemical etching was performed to transform raw NCP (NCP-0) to hollow-structured NCP (including NCP-30, and NCP-60) with enhanced diffusion, penetration, mass transmission of reaction species, and accessible surface area. Then, the resultant hollow NCP-60 frameworks were further converted into advanced functional nanomaterials including CoO/3NiO, NiCoP nanoparticles, and CoNi2S4 nanorods with a considerably improved photocatalytic H2 evolution performance. The hollow-structured NCP-60 particles exhibit an enhanced H2 evolution rate (1.28 mol g-1h−1) compared with the raw NCP-0 (0.64 mol g-1h−1). Furthermore, the H2 evolution rate of the resulting NiCoP nanoparticles reached 16.6 mol g-1h−1, 25 times that of the NCP-0, without any cocatalysts. |
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| AbstractList | Although Prussian blue and its analogs (PB/PBAs) have open framework structures, large surface areas, uniform metal active sites, and tunable compositions, and have been investigated for a long time, owing to their unfavorable visible light responsiveness, they rarely been reported in photocatalysis. This largely limits their applications in solar-to-chemical energy conversion. Here, a continuous-evolution strategy was conducted to convert the poor-performance NiCo PBA (NCP) toward high-efficiency complex photocatalytic nanomaterials. First, chemical etching was performed to transform raw NCP (NCP-0) to hollow-structured NCP (including NCP-30, and NCP-60) with enhanced diffusion, penetration, mass transmission of reaction species, and accessible surface area. Then, the resultant hollow NCP-60 frameworks were further converted into advanced functional nanomaterials including CoO/3NiO, NiCoP nanoparticles, and CoNi
S
nanorods with a considerably improved photocatalytic H
evolution performance. The hollow-structured NCP-60 particles exhibit an enhanced H
evolution rate (1.28 mol g
h
) compared with the raw NCP-0 (0.64 mol g
h
). Furthermore, the H
evolution rate of the resulting NiCoP nanoparticles reached 16.6 mol g
h
, 25 times that of the NCP-0, without any cocatalysts. Although Prussian blue and its analogs (PB/PBAs) have open framework structures, large surface areas, uniform metal active sites, and tunable compositions, and have been investigated for a long time, owing to their unfavorable visible light responsiveness, they rarely been reported in photocatalysis. This largely limits their applications in solar-to-chemical energy conversion. Here, a continuous-evolution strategy was conducted to convert the poor-performance NiCo PBA (NCP) toward high-efficiency complex photocatalytic nanomaterials. First, chemical etching was performed to transform raw NCP (NCP-0) to hollow-structured NCP (including NCP-30, and NCP-60) with enhanced diffusion, penetration, mass transmission of reaction species, and accessible surface area. Then, the resultant hollow NCP-60 frameworks were further converted into advanced functional nanomaterials including CoO/3NiO, NiCoP nanoparticles, and CoNi2S4 nanorods with a considerably improved photocatalytic H2 evolution performance. The hollow-structured NCP-60 particles exhibit an enhanced H2 evolution rate (1.28 mol g-1h-1) compared with the raw NCP-0 (0.64 mol g-1h-1). Furthermore, the H2 evolution rate of the resulting NiCoP nanoparticles reached 16.6 mol g-1h-1, 25 times that of the NCP-0, without any cocatalysts.Although Prussian blue and its analogs (PB/PBAs) have open framework structures, large surface areas, uniform metal active sites, and tunable compositions, and have been investigated for a long time, owing to their unfavorable visible light responsiveness, they rarely been reported in photocatalysis. This largely limits their applications in solar-to-chemical energy conversion. Here, a continuous-evolution strategy was conducted to convert the poor-performance NiCo PBA (NCP) toward high-efficiency complex photocatalytic nanomaterials. First, chemical etching was performed to transform raw NCP (NCP-0) to hollow-structured NCP (including NCP-30, and NCP-60) with enhanced diffusion, penetration, mass transmission of reaction species, and accessible surface area. Then, the resultant hollow NCP-60 frameworks were further converted into advanced functional nanomaterials including CoO/3NiO, NiCoP nanoparticles, and CoNi2S4 nanorods with a considerably improved photocatalytic H2 evolution performance. The hollow-structured NCP-60 particles exhibit an enhanced H2 evolution rate (1.28 mol g-1h-1) compared with the raw NCP-0 (0.64 mol g-1h-1). Furthermore, the H2 evolution rate of the resulting NiCoP nanoparticles reached 16.6 mol g-1h-1, 25 times that of the NCP-0, without any cocatalysts. Although Prussian blue and its analogs (PB/PBAs) have open framework structures, large surface areas, uniform metal active sites, and tunable compositions, and have been investigated for a long time, owing to their unfavorable visible light responsiveness, they rarely been reported in photocatalysis. This largely limits their applications in solar-to-chemical energy conversion. Here, a continuous-evolution strategy was conducted to convert the poor-performance NiCo PBA (NCP) toward high-efficiency complex photocatalytic nanomaterials. First, chemical etching was performed to transform raw NCP (NCP-0) to hollow-structured NCP (including NCP-30, and NCP-60) with enhanced diffusion, penetration, mass transmission of reaction species, and accessible surface area. Then, the resultant hollow NCP-60 frameworks were further convertedinto advanced functional nanomaterials including CoO/3NiO, NiCoP nanoparticles, and CoNi₂S₄ nanorods with a considerably improved photocatalytic H₂ evolution performance. The hollow-structured NCP-60 particles exhibit an enhanced H₂ evolution rate (1.28 mol g⁻¹ h⁻¹) compared with the raw NCP-0 (0.64 mol g⁻¹ h⁻¹). Furthermore, the H₂ evolution rate of the resulting NiCoP nanoparticles reached 16.6 mol g⁻¹ h⁻¹, 25 times that of the NCP-0, without any cocatalysts. [Display omitted] Although Prussian blue and its analogs (PB/PBAs) have open framework structures, large surface areas, uniform metal active sites, and tunable compositions, and have been investigated for a long time, owing to their unfavorable visible light responsiveness, they rarely been reported in photocatalysis. This largely limits their applications in solar-to-chemical energy conversion. Here, a continuous-evolution strategy was conducted to convert the poor-performance NiCo PBA (NCP) toward high-efficiency complex photocatalytic nanomaterials. First, chemical etching was performed to transform raw NCP (NCP-0) to hollow-structured NCP (including NCP-30, and NCP-60) with enhanced diffusion, penetration, mass transmission of reaction species, and accessible surface area. Then, the resultant hollow NCP-60 frameworks were further converted into advanced functional nanomaterials including CoO/3NiO, NiCoP nanoparticles, and CoNi2S4 nanorods with a considerably improved photocatalytic H2 evolution performance. The hollow-structured NCP-60 particles exhibit an enhanced H2 evolution rate (1.28 mol g-1h−1) compared with the raw NCP-0 (0.64 mol g-1h−1). Furthermore, the H2 evolution rate of the resulting NiCoP nanoparticles reached 16.6 mol g-1h−1, 25 times that of the NCP-0, without any cocatalysts. |
| Author | Jin, Zhiliang Tsubaki, Noritatsu Li, Yanbing |
| Author_xml | – sequence: 1 givenname: Yanbing surname: Li fullname: Li, Yanbing organization: Department of Applied Chemistry, School of Engineering, University of Toyama, Gofuku 3190, Toyama 930-8555, Japan – sequence: 2 givenname: Zhiliang orcidid: 0000-0002-3793-6588 surname: Jin fullname: Jin, Zhiliang email: zl-jin@nun.edu.cn organization: School of Chemistry and Chemical Engineering, North Minzu University, Yinchuan 750021, PR China – sequence: 3 givenname: Noritatsu surname: Tsubaki fullname: Tsubaki, Noritatsu email: tsubaki@eng.u-toyama.ac.jp organization: Department of Applied Chemistry, School of Engineering, University of Toyama, Gofuku 3190, Toyama 930-8555, Japan |
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Although Prussian blue and its analogs (PB/PBAs) have open framework structures, large surface areas, uniform metal active sites, and tunable... Although Prussian blue and its analogs (PB/PBAs) have open framework structures, large surface areas, uniform metal active sites, and tunable compositions, and... |
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| Title | Chemical etching and phase transformation of Nickel-Cobalt Prussian blue analogs for improved solar-driven water-splitting applications |
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