Screening for Mercury in Aqueous Environmental Samples and Urine Samples Using Thin Layer Chromatography
A method for screening based on thin layer chromatography (TLC) comprising silica gel 'G' as a stationary phase and benzene as a mobile phase was found to be most suitable for the detection of mercury in aqueous samples and spiked human urine, without digesting the samples. A broad range f...
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| Published in | Water environment research Vol. 79; no. 12; pp. 2457 - 2463 |
|---|---|
| Main Authors | , |
| Format | Journal Article |
| Language | English |
| Published |
Alexandria, VA
Water Environment Federation
01.11.2007
Blackwell Publishing Ltd |
| Subjects | |
| Online Access | Get full text |
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| Abstract | A method for screening based on thin layer chromatography (TLC) comprising silica gel 'G' as a stationary phase and benzene as a mobile phase was found to be most suitable for the detection of mercury in aqueous samples and spiked human urine, without digesting the samples. A broad range for the detection of mercury, from 20 μg/L (20 ppb) to 1000 mg/L (1000 ppm), was established, by optimizing the experimental conditions. In urine samples, mercury could be detected also, at levels as low as 50 μg/L (50 ppb) or above. Mercury was detected by complexation with dithizone followed by TLC, also in the presence of other heavy metals, including arsenic, cadmium, lead, copper, iron, zinc, and nickel. The method is simple, cheap, and has no interference of the matrix present in the natural water and aqueous industrial effluent samples obtained from the field. Further, no sophisticated instrument is needed for the detection of mercury. |
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| AbstractList | A method for screening based on thin layer chromatography (TLC) comprising silica gel 'G' as a stationary phase and benzene as a mobile phase was found to be most suitable for the detection of mercury in aqueous samples and spiked human urine, without digesting the samples. A broad range for the detection of mercury, from 20 μg/L (20 ppb) to 1000 mg/L (1000 ppm), was established, by optimizing the experimental conditions. In urine samples, mercury could be detected also, at levels as low as 50 μg/L (50 ppb) or above. Mercury was detected by complexation with dithizone followed by TLC, also in the presence of other heavy metals, including arsenic, cadmium, lead, copper, iron, zinc, and nickel. The method is simple, cheap, and has no interference of the matrix present in the natural water and aqueous industrial effluent samples obtained from the field. Further, no sophisticated instrument is needed for the detection of mercury. A method for screening based on thin layer chromatography (TLC) comprising silica gel 'G' as a stationary phase and benzene as a mobile phase was found to be most suitable for the detection of mercury in aqueous samples and spiked human urine, without digesting the samples. A broad range for the detection of mercury, from 20 microg/L (20 ppb) to 1000 mg/L (1000 ppm), was established, by optimizing the experimental conditions. In urine samples, mercury could be detected also, at levels as low as 50 microg/L (50 ppb) or above. Mercury was detected by complexation with dithizone followed by TLC, also in the presence of other heavy metals, including arsenic, cadmium, lead, copper, iron, zinc, and nickel. The method is simple, cheap, and has no interference of the matrix present in the natural water and aqueous industrial effluent samples obtained from the field. Further, no sophisticated instrument is needed for the detection of mercury.A method for screening based on thin layer chromatography (TLC) comprising silica gel 'G' as a stationary phase and benzene as a mobile phase was found to be most suitable for the detection of mercury in aqueous samples and spiked human urine, without digesting the samples. A broad range for the detection of mercury, from 20 microg/L (20 ppb) to 1000 mg/L (1000 ppm), was established, by optimizing the experimental conditions. In urine samples, mercury could be detected also, at levels as low as 50 microg/L (50 ppb) or above. Mercury was detected by complexation with dithizone followed by TLC, also in the presence of other heavy metals, including arsenic, cadmium, lead, copper, iron, zinc, and nickel. The method is simple, cheap, and has no interference of the matrix present in the natural water and aqueous industrial effluent samples obtained from the field. Further, no sophisticated instrument is needed for the detection of mercury. A method for screening based on thin layer chromatography (TLC) comprising silica gel `G' as a stationary phase and benzene as a mobile phase was found to be most suitable for the detection of mercury in aqueous samples and spiked human urine, without digesting the samples. A broad range for the detection of mercury, from 20 [mu]g/L (20 ppb) to 1000 mg/L (1000 ppm), was established, by optimizing the experimental conditions. In urine samples, mercury could be detected also, at levels as low as 50 [mu]g/L (50 ppb) or above. Mercury was detected by complexation with dithizone followed by TLC, also in the presence of other heavy metals, including arsenic, cadmium, lead, copper, iron, zinc, and nickel. The method is simple, cheap, and has no interference of the matrix present in the natural water and aqueous industrial effluent samples obtained from the field. Further, no sophisticated instrument is needed for the detection of mercury. A method for screening based on thin layer chromatography (TLC) comprising silica gel 'G' as a stationary phase and benzene as a mobile phase was found to be most suitable for the detection of mercury in aqueous samples and spiked human urine, without digesting the samples. A broad range for the detection of mercury, from 20 µg/L (20 ppb) to 1000 mg/L (1000 ppm), was established, by optimizing the experimental conditions. In urine samples, mercury could be detected also, at levels as low as 50 µg/L (50 ppb) or above. Mercury was detected by complexation with dithizone followed by TLC, also in the presence of other heavy metals, including arsenic, cadmium, lead, copper, iron, zinc, and nickel. The method is simple, cheap, and has no interference of the matrix present in the natural water and aqueous industrial effluent samples obtained from the field. Further, no sophisticated instrument is needed for the detection of mercury. [PUBLICATION ABSTRACT] A method for screening based on thin layer chromatography (TLC) comprising silica gel 'G' as a stationary phase and benzene as a mobile phase was found to be most suitable for the detection of mercury in aqueous samples and spiked human urine, without digesting the samples. A broad range for the detection of mercury, from 20 microg/L (20 ppb) to 1000 mg/L (1000 ppm), was established, by optimizing the experimental conditions. In urine samples, mercury could be detected also, at levels as low as 50 microg/L (50 ppb) or above. Mercury was detected by complexation with dithizone followed by TLC, also in the presence of other heavy metals, including arsenic, cadmium, lead, copper, iron, zinc, and nickel. The method is simple, cheap, and has no interference of the matrix present in the natural water and aqueous industrial effluent samples obtained from the field. Further, no sophisticated instrument is needed for the detection of mercury. |
| Author | Agarwal, Rakhi Behari, Jai Raj |
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| Cites_doi | 10.1080/03067318508077038 10.1021/ac50015a029 10.1016/0048-9697(80)90122-9 10.1351/pac199870081585 10.1056/NEJM199010183231610 10.2116/analsci.18.187 10.1002/(SICI)1099-0739(200001)14:1<66::AID-AOC961>3.0.CO;2-K 10.1016/S1010-6030(00)00373-7 10.1002/aheh.19770050211 10.1039/b308834k 10.1080/00039896.1968.10665208 |
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| Copyright | Copyright 2007 The Water Environment Federation (WEF) 2007 Water Environment Federation 2008 INIST-CNRS Copyright Water Environment Federation Nov 2007 |
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| Keywords | Human Urine Thin layer chromatography Complexation Arsenic Instruments Industrial waste water Silica gel Mercury Optimization Operating conditions Heavy metal |
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| Snippet | A method for screening based on thin layer chromatography (TLC) comprising silica gel 'G' as a stationary phase and benzene as a mobile phase was found to be... A method for screening based on thin layer chromatography (TLC) comprising silica gel ‘G’ as a stationary phase and benzene as a mobile phase was found to be... A method for screening based on thin layer chromatography (TLC) comprising silica gel `G' as a stationary phase and benzene as a mobile phase was found to be... |
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| SubjectTerms | Applied sciences aqueous samples Aqueous solutions Arsenic Benzene Cadmium Chemicals Chromatography Chromatography, Thin Layer - methods Copper dithizone Dithizone - analysis Dithizone - chemistry Environmental Monitoring - methods Exact sciences and technology General purification processes Heavy metals Human subjects Humans Hydrochloric acid Industrial effluents Industrial wastewater Lead Mass spectrometry Mercury Mercury - analysis Mercury - chemistry Mercury - urine Mercury Compounds - analysis Mercury Compounds - chemistry Mercury Compounds - urine Metals - analysis Metals - chemistry Molecular Structure Nickel Pollution Protons Reproducibility of Results Research methodology Research Note Scholarships & fellowships Silica Solvents Thin layer chromatography Urine urine sample Wastewaters Water - analysis Water - chemistry Water samples Water treatment and pollution Zinc |
| Title | Screening for Mercury in Aqueous Environmental Samples and Urine Samples Using Thin Layer Chromatography |
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