Microstructure of Ti(CN)-WC-NbC-Ni Cermets
An investigation of the microstructural evolution and dissolution phenomena in a Ti(C0.7N0.3)–xWC–yNbC–20Ni system is reported. In Ti(C0.7N0.3)–yNbC–20Ni systems, a phase separation occurs between the Ti(CN) core and the (Ti,Nb)(CN) rim phases when the system contains >15 wt% NbC. This phase sepa...
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| Published in | Journal of the American Ceramic Society Vol. 84; no. 4; pp. 843 - 849 |
|---|---|
| Main Authors | , , |
| Format | Journal Article |
| Language | English |
| Published |
Westerville, Ohio
American Ceramics Society
01.04.2001
Blackwell |
| Subjects | |
| Online Access | Get full text |
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| Abstract | An investigation of the microstructural evolution and dissolution phenomena in a Ti(C0.7N0.3)–xWC–yNbC–20Ni system is reported. In Ti(C0.7N0.3)–yNbC–20Ni systems, a phase separation occurs between the Ti(CN) core and the (Ti,Nb)(CN) rim phases when the system contains >15 wt% NbC. This phase separation results from the increased misfit between the cores and the solid‐solution rim phases with the addition of NbC. Based on data obtained from a previous study and compositional analyses of the rim structure of the Ti(C0.7N0.3)–yNbC–20Ni system, the average dissolution rates of WC and NbC appear to be approximately the same with respect to that of Ti(CN), under given sintering conditions (1510°C for 1 h). In addition, compositional changes in the rim structure of the Ti(C0.7N0.3)–xWC–yNbC–20Ni system are compared with those for a Ti(C0.7N0.3)–xWC–20Ni system to explain the effect of NbC on WC dissolution in the Ti(C0.7N0.3)–WC–NbC–Ni system. The presence of NbC in the Ti(C0.7N0.3)–xWC–20Ni system is found to suppress the dissolution of WC. |
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| AbstractList | An investigation of the microstructural evolution and dissolution phenomena in a Ti(C0.7N0.3)–xWC–yNbC–20Ni system is reported. In Ti(C0.7N0.3)–yNbC–20Ni systems, a phase separation occurs between the Ti(CN) core and the (Ti,Nb)(CN) rim phases when the system contains >15 wt% NbC. This phase separation results from the increased misfit between the cores and the solid‐solution rim phases with the addition of NbC. Based on data obtained from a previous study and compositional analyses of the rim structure of the Ti(C0.7N0.3)–yNbC–20Ni system, the average dissolution rates of WC and NbC appear to be approximately the same with respect to that of Ti(CN), under given sintering conditions (1510°C for 1 h). In addition, compositional changes in the rim structure of the Ti(C0.7N0.3)–xWC–yNbC–20Ni system are compared with those for a Ti(C0.7N0.3)–xWC–20Ni system to explain the effect of NbC on WC dissolution in the Ti(C0.7N0.3)–WC–NbC–Ni system. The presence of NbC in the Ti(C0.7N0.3)–xWC–20Ni system is found to suppress the dissolution of WC. An investigation of the microstructural evolution and dissolution phenomena in a Ti(C 0.7 N 0.3 )– x WC– y NbC–20Ni system is reported. In Ti(C 0.7 N 0.3 )– y NbC–20Ni systems, a phase separation occurs between the Ti(CN) core and the (Ti,Nb)(CN) rim phases when the system contains >15 wt% NbC. This phase separation results from the increased misfit between the cores and the solid‐solution rim phases with the addition of NbC. Based on data obtained from a previous study and compositional analyses of the rim structure of the Ti(C 0.7 N 0.3 )– y NbC–20Ni system, the average dissolution rates of WC and NbC appear to be approximately the same with respect to that of Ti(CN), under given sintering conditions (1510°C for 1 h). In addition, compositional changes in the rim structure of the Ti(C 0.7 N 0.3 )– x WC– y NbC–20Ni system are compared with those for a Ti(C 0.7 N 0.3 )– x WC–20Ni system to explain the effect of NbC on WC dissolution in the Ti(C 0.7 N 0.3 )–WC–NbC–Ni system. The presence of NbC in the Ti(C 0.7 N 0.3 ) –x WC–20Ni system is found to suppress the dissolution of WC. Titanium carbonitride-based cermets are important components of high speed cutting tools. A typical hard phase in cermets has a core/rim structure. Dissolution-reprecipitation is involved in the mechanism for the formation of the structure. An investigation of the microstructural evolution and dissolution phenomena in a Ti(C sub 0.7 N sub 0.3 )-xWC-yNbC-20Ni system is reported. In Ti(C sub 0.7 N sub 0.3 )-yNbC-20Ni systems, a phase separation occurs between the Ti(CN) core and the (Ti,Nb)(CN) rim phases when the system contains > 15 wt.% NbC. This phase separation results from the increased misfit between the cores and the solid-solution rim phases wtih the addition of NbC. Based on data obtained from a prevous study and compositional analyses of the rim structure of the Ti(C sub 0.7 N sub 0.3 )-yNbC-20Ni system, the average dissolution rates of WC and NbC appear to approximately the same with respect to that of Ti(CN), under given sintering conditions (1510 deg C for 1 h). In addition, compositional changes in the rim structure of the Ti(C sub 0.7 N sub 0.3 )-xWC-yNbC-20Ni system are compared with those for a Ti(C sub 0.7 N sub 0.3 )-xWC-20Ni system to explain the effect of NbC on WC dissolution in the Ti(C sub 0.7 N sub 0.3 )-WC-NbC-Ni system. The presence of NbC in the Ti(C sub 0.7 N sub 0.3 )-xWC-20Ni system is found to suppress the dissolution of WC. |
| Author | Kim, Seong-Won Ahn, Sun-Yong Kang, Shinhoo |
| Author_xml | – sequence: 1 givenname: Sun-Yong surname: Ahn fullname: Ahn, Sun-Yong organization: School of Materials Science and Engineering, Seoul National University, Seoul 151-742, Korea – sequence: 2 givenname: Seong-Won surname: Kim fullname: Kim, Seong-Won organization: School of Materials Science and Engineering, Seoul National University, Seoul 151-742, Korea – sequence: 3 givenname: Shinhoo surname: Kang fullname: Kang, Shinhoo organization: School of Materials Science and Engineering, Seoul National University, Seoul 151-742, Korea |
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| Cites_doi | 10.1111/j.1151-2916.1994.tb07024.x 10.1016/0022-5088(73)90044-1 10.1557/JMR.1999.0556 10.1016/S0921-5093(98)00609-1 10.1007/978-1-4684-7712-2_6 10.1016/S0924-0136(97)00437-8 10.1111/j.1151-2916.1994.tb07277.x 10.1111/j.1151-2916.2000.tb01415.x 10.1016/0263-4368(95)00027-G 10.1016/S0025-5408(99)00172-5 10.1016/S0167-577X(96)00110-3 10.1016/0921-5093(93)90588-6 |
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| Keywords | Tungsten carbide Niobium carbide Cermet Phase separation Titanium Carbides nitrides Nickel Microstructure Powder metallurgy Lattice parameters Dissolution |
| Language | English |
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| Notes | ArticleID:JACE843 istex:C4FDB03BE6BF06BFB1BFEADC787CA04CBFBA088C ark:/67375/WNG-Q8T3V5PJ-S Supported by Grant No. KRF–99–0422–E00133, from the Basic Research Program of the Korea Research Foundation (KRF), in 2000. N. Padture—contributing editor Member, American Ceramic Society. ObjectType-Article-2 SourceType-Scholarly Journals-1 ObjectType-Feature-1 content type line 23 |
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| References_xml | – volume: 77 start-page: 337 year: 1998 end-page: 43 article-title: Tool‐Life Reliability of Cermet Inserts in Milling Tests publication-title: J. Mater. Proc. Technol. – volume: 3 start-page: 83 year: 1966 end-page: 94 article-title: Cemented Titanium Carbide Cutting Tools publication-title: Mod. Dev. Powder Metall. – volume: 77 start-page: 1093 issue: 4 year: 1994 end-page: 97 article-title: Microstructure Characterization of Gas‐Pressure‐Sintered Silicon Nitride Containing Large Silicon Nitride Seeds publication-title: J. Am. Ceram. Soc. – volume: 14 start-page: 4129 issue: 11 year: 1999 end-page: 31 article-title: Nanoprobe Analysis of Core–Rim Structure of Carbides in TiC‐20 wt% Mo C–20 wt% Ni Cermet publication-title: J. Mater. Res. – volume: 34 start-page: 1629 issue: 10–11 year: 1999 end-page: 36 article-title: Effect of Additive Content on Liquid‐Phase Sintering on Silicon Carbide Ceramics publication-title: Mater. Res. Bull. – volume: 83 start-page: 1489 issue: 6 year: 2000 end-page: 94 article-title: Formation of Core/Rim Structures in Ti(CN)–WC–Ni Cermets via a Dissolution and Precipitation Process publication-title: J. Am. Ceram. Soc. – volume: 251 start-page: 276 year: 1998 end-page: 85 article-title: A Study on Microstructural Changes in Ti(CN)–NbC–Ni Cermets publication-title: Mater. Sci. Eng. A – volume: 13 start-page: 343 year: 1995 end-page: 51 article-title: Ti(CN) Cermets– Metallurgy and Properties publication-title: Int. J. Refract. Met. Hard Mater. – volume: 29 start-page: 1 issue: 1–3 year: 1996 end-page: 6 article-title: Formation of Solid Solutions between SiC and AlN during Liquid‐Phase Sintering publication-title: Mater. Lett. – volume: 163 start-page: 141 year: 1993 end-page: 48 article-title: Titanium Carbonitride‐Based Cermets: Process and Properties publication-title: Mater. Sci. Eng. A – volume: 33 start-page: 245 year: 1973 end-page: 73 article-title: Constitution of Ternary Titanium‐Tungsten‐Carbon Alloys publication-title: J. Less- Common Met. – volume: 35 start-page: 245 issue: 9 year: 1981 end-page: 73 article-title: Mechanisms of Surrounding Structure Formation in Sintered TiC–Mo2C–Ni Alloy publication-title: J. Jpn. Inst. Met. – volume: 77 start-page: 619 issue: 2 year: 1994 end-page: 23 article-title: In Situ‐Toughened Silicon Carbide publication-title: J. Am. Ceram. Soc. – volume: 1 start-page: 825 year: 1985 end-page: 43 – ident: e_1_2_1_12_2 doi: 10.1111/j.1151-2916.1994.tb07024.x – ident: e_1_2_1_6_2 doi: 10.1016/0022-5088(73)90044-1 – ident: e_1_2_1_15_2 doi: 10.1557/JMR.1999.0556 – ident: e_1_2_1_13_2 doi: 10.1016/S0921-5093(98)00609-1 – ident: e_1_2_1_7_2 doi: 10.1007/978-1-4684-7712-2_6 – start-page: 825 volume-title: Proceedings of the 11th International Plansee Seminar '85 year: 1985 ident: e_1_2_1_14_2 contributor: fullname: Doi A. – ident: e_1_2_1_4_2 doi: 10.1016/S0924-0136(97)00437-8 – ident: e_1_2_1_16_2 – ident: e_1_2_1_10_2 doi: 10.1111/j.1151-2916.1994.tb07277.x – ident: e_1_2_1_8_2 doi: 10.1111/j.1151-2916.2000.tb01415.x – ident: e_1_2_1_3_2 doi: 10.1016/0263-4368(95)00027-G – volume: 35 start-page: 245 issue: 9 year: 1981 ident: e_1_2_1_5_2 article-title: Mechanisms of Surrounding Structure Formation in Sintered TiC–Mo2C–Ni Alloy publication-title: J. Jpn. Inst. Met. contributor: fullname: Suzuki H. – ident: e_1_2_1_11_2 doi: 10.1016/S0025-5408(99)00172-5 – ident: e_1_2_1_9_2 doi: 10.1016/S0167-577X(96)00110-3 – ident: e_1_2_1_2_2 doi: 10.1016/0921-5093(93)90588-6 |
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| Snippet | An investigation of the microstructural evolution and dissolution phenomena in a Ti(C0.7N0.3)–xWC–yNbC–20Ni system is reported. In Ti(C0.7N0.3)–yNbC–20Ni... An investigation of the microstructural evolution and dissolution phenomena in a Ti(C 0.7 N 0.3 )– x WC– y NbC–20Ni system is reported. In Ti(C 0.7 N 0.3 )– y... Titanium carbonitride-based cermets are important components of high speed cutting tools. A typical hard phase in cermets has a core/rim structure.... |
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| SubjectTerms | Applied sciences ceramic-metal systems Exact sciences and technology Metals. Metallurgy microstructure Powder metallurgy. Composite materials Production techniques Sintered metals and alloys. Pseudo alloys. Cermets titanium carbonitride |
| Title | Microstructure of Ti(CN)-WC-NbC-Ni Cermets |
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