The effect of high-pressure carbon dioxide treatment on the crystallization behavior and mechanical properties of poly( l-lactic acid)/poly(methyl methacrylate) blends
The purpose of this study is to investigate the effect of carbon dioxide (CO 2) on the crystallization behavior and the mechanical properties of PLLA/PMMA blends with various weight fraction of PMMA. PLLA/PMMA blends can be crystallized even at a low temperature of 0 °C under high-pressure CO 2. The...
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Published in | Polymer (Guilford) Vol. 47; no. 11; pp. 3954 - 3960 |
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Main Authors | , , , , |
Format | Journal Article |
Language | English |
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Oxford
Elsevier Ltd
17.05.2006
Elsevier |
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Abstract | The purpose of this study is to investigate the effect of carbon dioxide (CO
2) on the crystallization behavior and the mechanical properties of PLLA/PMMA blends with various weight fraction of PMMA. PLLA/PMMA blends can be crystallized even at a low temperature of 0
°C under high-pressure CO
2. The films treated with high-pressure CO
2 at 0
°C have about three times larger strain at break than that of the amorphous and cold-crystallized film. The size of spherulites in the CO
2 treated film is considered to be smaller than the wavelength of the visible light because of a good transparency. The improvement of the strain at break is attributed to the reduction of the stress concentration during the deformation. |
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AbstractList | The purpose of this study is to investigate the effect of carbon dioxide (CO2) on the crystallization behavior and the mechanical properties of PLLA/PMMA blends with various weight fraction of PMMA. PLLA/PMMA blends can be crystallized even at a low temperature of 0 deg C under high-pressure CO2. The films treated with high-pressure CO2 at 0 deg C have about three times larger strain at break than that of the amorphous and cold-crystallized film. The size of spherulites in the CO2 treated film is considered to be smaller than the wavelength of the visible light because of a good transparency. The improvement of the strain at break is attributed to the reduction of the stress concentration during the deformation. The purpose of this study is to investigate the effect of carbon dioxide (CO 2) on the crystallization behavior and the mechanical properties of PLLA/PMMA blends with various weight fraction of PMMA. PLLA/PMMA blends can be crystallized even at a low temperature of 0 °C under high-pressure CO 2. The films treated with high-pressure CO 2 at 0 °C have about three times larger strain at break than that of the amorphous and cold-crystallized film. The size of spherulites in the CO 2 treated film is considered to be smaller than the wavelength of the visible light because of a good transparency. The improvement of the strain at break is attributed to the reduction of the stress concentration during the deformation. |
Author | Hirota, Shin-ichi Sumita, Masao Tominaga, Yoichi Sato, Takatoshi Asai, Shigeo |
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Cites_doi | 10.1021/ma60048a040 10.1002/polb.10353 10.1002/app.10367 10.1002/jctb.5010020901 10.1021/ma00204a041 10.1021/ma050373q |
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Keywords | Polymer blend Carbon dioxide Crystallization Crystal form Polymer blends Optically active polymer Property composition relationship Physical dressing Mechanical properties Methyl methacrylate polymer Experimental study Structure composition relationship High pressure Elongation at fracture Lactic acid polymer Supramolecular structure Miscibility Thermodynamic properties |
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References | Gordon, Taylor (bib3) 1952; 2 Zhang, Zhang, Wang, Shen (bib2) 2003; 41 Asai, Shimada, Tominaga, Sumita (bib1) 2005; 38 Asai, Ikura, Tominaga, Sumita (bib8) 2005 Huang, Chang (bib4) 2002; 84 Nishi, Wang (bib6) 1975; 8 MacKnight, Karasz, Fried (bib5) 1978 Hoogsteen, Postema, Pennings, Brinke (bib7) 1990; 23 Hoogsteen (10.1016/j.polymer.2006.03.069_bib7) 1990; 23 Huang (10.1016/j.polymer.2006.03.069_bib4) 2002; 84 MacKnight (10.1016/j.polymer.2006.03.069_bib5) 1978 Zhang (10.1016/j.polymer.2006.03.069_bib2) 2003; 41 Gordon (10.1016/j.polymer.2006.03.069_bib3) 1952; 2 Asai (10.1016/j.polymer.2006.03.069_bib1) 2005; 38 Asai (10.1016/j.polymer.2006.03.069_bib8) 2005 Nishi (10.1016/j.polymer.2006.03.069_bib6) 1975; 8 |
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SubjectTerms | Applied sciences Carbon dioxide Crystallization Exact sciences and technology Mechanical properties Organic polymers Physicochemistry of polymers Polymer blend Properties and characterization |
Title | The effect of high-pressure carbon dioxide treatment on the crystallization behavior and mechanical properties of poly( l-lactic acid)/poly(methyl methacrylate) blends |
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