Effect of nanoconfinement on the formation, structural transition and magnetic behavior of mesoporous copper ferrite
[Display omitted] •Fabrication of superparamagnetic cubic single phase, ordered mesoporous CuFe2O4.•Reduction of formation temperature of copper ferrite through nanoconfinement.•Suppression of Jahn–Teller effect through nanoconfinement.•Stabilization of cubic high temperature phase of copper ferrite...
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| Published in | Journal of alloys and compounds Vol. 598; pp. 191 - 197 |
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| Main Authors | , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Kidlington
Elsevier B.V
15.06.2014
Elsevier |
| Subjects | |
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| Abstract | [Display omitted]
•Fabrication of superparamagnetic cubic single phase, ordered mesoporous CuFe2O4.•Reduction of formation temperature of copper ferrite through nanoconfinement.•Suppression of Jahn–Teller effect through nanoconfinement.•Stabilization of cubic high temperature phase of copper ferrite at RT.•Investigation of blocking temperature by different methods.
Superparamagnetic, cubic single phase, ordered mesoporous copper ferrite is synthesized through confinement in nanocages of mesoporous silica. The heat generated during the reaction is conserved in the silica template pore channels, which allows the formation of copper ferrite at a relatively low processing temperature. The Jahn–Teller distortion is suppressed due to the effect of nanoconfinement and thus the high temperature phase of cubic copper ferrite is stabilized at room temperature. The particle size obtained from TEM, the crystallite size calculated from XRD and the magnetic domain size estimated from magnetization measurements are all in good agreement, manifesting the significant role of the confinement in the growth and fabrication of crystalline, single magnetic domain, nanoparticles with superparamagnetic behavior at room temperature. |
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| AbstractList | Superparamagnetic, cubic single phase, ordered mesoporous copper ferrite is synthesized through confinement in nanocages of mesoporous silica. The heat generated during the reaction is conserved in the silica template pore channels, which allows the formation of copper ferrite at a relatively low processing temperature. The Jahn-Teller distortion is suppressed due to the effect of nanoconfinement and thus the high temperature phase of cubic copper ferrite is stabilized at room temperature. The particle size obtained from TEM, the crystallite size calculated from XRD and the magnetic domain size estimated from magnetization measurements are all in good agreement, manifesting the significant role of the confinement in the growth and fabrication of crystalline, single magnetic domain, nanoparticles with super-paramagnetic behavior at room temperature. Superparamagnetic, cubic single phase, ordered mesoporous copper ferrite is synthesized through confinement in nanocages of mesoporous silica. The heat generated during the reaction is conserved in the silica template pore channels, which allows the formation of copper ferrite at a relatively low processing temperature. The Jahn-Teller distortion is suppressed due to the effect of nanoconfinement and thus the high temperature phase of cubic copper ferrite is stabilized at room temperature. The particle size obtained from TEM, the crystallite size calculated from XRD and the magnetic domain size estimated from magnetization measurements are all in good agreement, manifesting the significant role of the confinement in the growth and fabrication of crystalline, single magnetic domain, nanoparticles with superparamagnetic behavior at room temperature. [Display omitted] •Fabrication of superparamagnetic cubic single phase, ordered mesoporous CuFe2O4.•Reduction of formation temperature of copper ferrite through nanoconfinement.•Suppression of Jahn–Teller effect through nanoconfinement.•Stabilization of cubic high temperature phase of copper ferrite at RT.•Investigation of blocking temperature by different methods. Superparamagnetic, cubic single phase, ordered mesoporous copper ferrite is synthesized through confinement in nanocages of mesoporous silica. The heat generated during the reaction is conserved in the silica template pore channels, which allows the formation of copper ferrite at a relatively low processing temperature. The Jahn–Teller distortion is suppressed due to the effect of nanoconfinement and thus the high temperature phase of cubic copper ferrite is stabilized at room temperature. The particle size obtained from TEM, the crystallite size calculated from XRD and the magnetic domain size estimated from magnetization measurements are all in good agreement, manifesting the significant role of the confinement in the growth and fabrication of crystalline, single magnetic domain, nanoparticles with superparamagnetic behavior at room temperature. |
| Author | Rezaie, Hamidreza Åkerman, Johan Toprak, Muhammet S. Najmoddin, Najmeh Ansari, Narges Niarchos, Dimitris Mohseni, Seyed Majid Muhammed, Mamoun Beitollahi, Ali Devlin, Eamonn |
| Author_xml | – sequence: 1 givenname: Najmeh surname: Najmoddin fullname: Najmoddin, Najmeh email: najmoddin@iust.ac.ir organization: Department of Materials and Nano Physics, KTH – Royal Institute of Technology, 16440 Kista-Stockholm, Sweden – sequence: 2 givenname: Ali surname: Beitollahi fullname: Beitollahi, Ali organization: Center of Excellence for Ceramic Materials in Energy and Environment Applications, School of Metallurgy & Materials Engineering, Iran University of Science and Technology (IUST), Narmak, Tehran 16846, Iran – sequence: 3 givenname: Mamoun surname: Muhammed fullname: Muhammed, Mamoun organization: Department of Materials and Nano Physics, KTH – Royal Institute of Technology, 16440 Kista-Stockholm, Sweden – sequence: 4 givenname: Narges surname: Ansari fullname: Ansari, Narges organization: Department of Materials and Nano Physics, KTH – Royal Institute of Technology, 16440 Kista-Stockholm, Sweden – sequence: 5 givenname: Eamonn surname: Devlin fullname: Devlin, Eamonn organization: Institute of Advanced Materials, Physicochemical Processes, Nanotechnology and Microsystems, NCSR Demokritos, Aghia Paraskevi, Athens 15310, Greece – sequence: 6 givenname: Seyed Majid surname: Mohseni fullname: Mohseni, Seyed Majid organization: Department of Materials and Nano Physics, KTH – Royal Institute of Technology, 16440 Kista-Stockholm, Sweden – sequence: 7 givenname: Hamidreza surname: Rezaie fullname: Rezaie, Hamidreza organization: Center of Excellence for Ceramic Materials in Energy and Environment Applications, School of Metallurgy & Materials Engineering, Iran University of Science and Technology (IUST), Narmak, Tehran 16846, Iran – sequence: 8 givenname: Dimitris surname: Niarchos fullname: Niarchos, Dimitris organization: Institute of Advanced Materials, Physicochemical Processes, Nanotechnology and Microsystems, NCSR Demokritos, Aghia Paraskevi, Athens 15310, Greece – sequence: 9 givenname: Johan surname: Åkerman fullname: Åkerman, Johan organization: Department of Materials and Nano Physics, KTH – Royal Institute of Technology, 16440 Kista-Stockholm, Sweden – sequence: 10 givenname: Muhammet S. surname: Toprak fullname: Toprak, Muhammet S. email: toprak@kth.se organization: Department of Materials and Nano Physics, KTH – Royal Institute of Technology, 16440 Kista-Stockholm, Sweden |
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| Keywords | Ferrites Nanoconfinement Nanostructured materials Porous materials Magnetically ordered materials Crystal structure Cubic lattices Confinement Particle size Magnetization Nanocage Superparamagnetism XRD High temperature Magnetic nanomaterial Jahn-Teller effect Mesoporosity Copper Iron Oxides Mixed Magnetic particles Transmission electron microscopy Magnetic domains |
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•Fabrication of superparamagnetic cubic single phase, ordered mesoporous CuFe2O4.•Reduction of formation temperature of copper ferrite... Superparamagnetic, cubic single phase, ordered mesoporous copper ferrite is synthesized through confinement in nanocages of mesoporous silica. The heat... |
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| SubjectTerms | Channels Condensed matter: electronic structure, electrical, magnetic, and optical properties Confinement Copper Crystal structure Exact sciences and technology FERRITE Ferrites Magnetic domains Magnetic properties and materials Magnetic properties of nanostructures Magnetically ordered materials Magnetization MICROSTRUCTURES Nanoconfinement Nanostructure Nanostructured materials PARTICLE SIZE AND SHAPE Physics POROSITY Porous materials SILICON DIOXIDE |
| Title | Effect of nanoconfinement on the formation, structural transition and magnetic behavior of mesoporous copper ferrite |
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