Chain Structure in a Cross-Linked Polyurethane Magnetic Elastomer Under a Magnetic Field

The morphology of magnetic particles with a size of 7.0 μm was observed for magnetic elastomers with a concentration of magnetic particles of 70 wt% using an X-ray microscope remolded into high resolution. Computed tomography images revealed that magnetic particles were distributed isotopically in t...

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Published inInternational journal of molecular sciences Vol. 20; no. 12; p. 2879
Main Authors Watanabe, Mayuko, Takeda, Yoshihiro, Maruyama, Takayuki, Ikeda, Junko, Kawai, Mika, Mitsumata, Tetsu
Format Journal Article
LanguageEnglish
Published Switzerland MDPI AG 13.06.2019
MDPI
Subjects
Elastomers
Epoxy resins
Magnetic fields
Magnetism
Morphology
Physical properties
Rheology
Viscoelasticity
computed tomography
magnetic gel
viscoelastic property
magnetorheology
stimuli-responsive material
magnetic elastomer
Online AccessGet full text
ISSN1422-0067
1661-6596
1422-0067
DOI10.3390/ijms20122879

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Abstract The morphology of magnetic particles with a size of 7.0 μm was observed for magnetic elastomers with a concentration of magnetic particles of 70 wt% using an X-ray microscope remolded into high resolution. Computed tomography images revealed that magnetic particles were distributed isotopically in the absence of a magnetic field, but they formed a chain structure in the polyurethane network under a magnetic field of 270 mT. It was also established, by image analysis, that magnetic elastomers had an anisotropic structure under the magnetic field.
AbstractList The morphology of magnetic particles with a size of 7.0 μm was observed for magnetic elastomers with a concentration of magnetic particles of 70 wt% using an X-ray microscope remolded into high resolution. Computed tomography images revealed that magnetic particles were distributed isotopically in the absence of a magnetic field, but they formed a chain structure in the polyurethane network under a magnetic field of 270 mT. It was also established, by image analysis, that magnetic elastomers had an anisotropic structure under the magnetic field.
The morphology of magnetic particles with a size of 7.0 μm was observed for magnetic elastomers with a concentration of magnetic particles of 70 wt% using an X-ray microscope remolded into high resolution. Computed tomography images revealed that magnetic particles were distributed isotopically in the absence of a magnetic field, but they formed a chain structure in the polyurethane network under a magnetic field of 270 mT. It was also established, by image analysis, that magnetic elastomers had an anisotropic structure under the magnetic field.The morphology of magnetic particles with a size of 7.0 μm was observed for magnetic elastomers with a concentration of magnetic particles of 70 wt% using an X-ray microscope remolded into high resolution. Computed tomography images revealed that magnetic particles were distributed isotopically in the absence of a magnetic field, but they formed a chain structure in the polyurethane network under a magnetic field of 270 mT. It was also established, by image analysis, that magnetic elastomers had an anisotropic structure under the magnetic field.
Besides these studies, in situ observation has also been carried out. In 2014 Gundermann et al. observed magnetic elastomers containing magnetic particles (2 wt%) with a diameter of 35 μm using an X-ray μ-CT [22] under the following conditions: resolution 1 pixel = 3.2 μm, acceleration voltage 90 kV, current 170 μA, exposure time 4 s and 6.5 s. They showed that the combination of CT and digital image processing provided a tool for a quantitative analysis of single particle motion in a magnetorheological elastomer. [...]the silicone mold was removed from the epoxy resin. [...]magnetic particles in magnetic elastomers used in the CT observation randomly dispersed in the polyurethane matrix at the microscopic scale [28].
Author Watanabe, Mayuko
Takeda, Yoshihiro
Mitsumata, Tetsu
Maruyama, Takayuki
Ikeda, Junko
Kawai, Mika
AuthorAffiliation 3 Rigaku Corporation, Tokyo 196-8666, Japan; y-takeda@rigaku.co.jp
5 Nihon Rufuto Corporation, Tokyo 110-0015, Japan
1 Graduate School of Science and Technology, Niigata University, Niigata 950-2181, Japan; w-myk.265@i.softbank.jp (M.W.); j-ikeda@sanyo-trading.co.jp (J.I.); mikagoro@eng.niigata-u.ac.jp (M.K.)
4 Bridgestone Corporation, Tokyo 187-8531, Japan; takayuki.maruyama@bridgestone.com
2 ALCA, Japan Science and Technology Agency, Tokyo 102-0076, Japan
AuthorAffiliation_xml – name: 3 Rigaku Corporation, Tokyo 196-8666, Japan; y-takeda@rigaku.co.jp
– name: 5 Nihon Rufuto Corporation, Tokyo 110-0015, Japan
– name: 4 Bridgestone Corporation, Tokyo 187-8531, Japan; takayuki.maruyama@bridgestone.com
– name: 2 ALCA, Japan Science and Technology Agency, Tokyo 102-0076, Japan
– name: 1 Graduate School of Science and Technology, Niigata University, Niigata 950-2181, Japan; w-myk.265@i.softbank.jp (M.W.); j-ikeda@sanyo-trading.co.jp (J.I.); mikagoro@eng.niigata-u.ac.jp (M.K.)
Author_xml – sequence: 1
  givenname: Mayuko
  surname: Watanabe
  fullname: Watanabe, Mayuko
– sequence: 2
  givenname: Yoshihiro
  surname: Takeda
  fullname: Takeda, Yoshihiro
– sequence: 3
  givenname: Takayuki
  surname: Maruyama
  fullname: Maruyama, Takayuki
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  givenname: Mika
  surname: Kawai
  fullname: Kawai, Mika
– sequence: 6
  givenname: Tetsu
  orcidid: 0000-0002-1355-6775
  surname: Mitsumata
  fullname: Mitsumata, Tetsu
BackLink https://www.ncbi.nlm.nih.gov/pubmed/31200473$$D View this record in MEDLINE/PubMed
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Keywords computed tomography
magnetic gel
viscoelastic property
magnetorheology
stimuli-responsive material
magnetic elastomer
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Snippet The morphology of magnetic particles with a size of 7.0 μm was observed for magnetic elastomers with a concentration of magnetic particles of 70 wt% using an...
Besides these studies, in situ observation has also been carried out. In 2014 Gundermann et al. observed magnetic elastomers containing magnetic particles (2...
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StartPage 2879
SubjectTerms Elastomers
Epoxy resins
Magnetic fields
Magnetism
Morphology
Physical properties
Rheology
Viscoelasticity
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Title Chain Structure in a Cross-Linked Polyurethane Magnetic Elastomer Under a Magnetic Field
URI https://www.ncbi.nlm.nih.gov/pubmed/31200473
https://www.proquest.com/docview/2332755913
https://www.proquest.com/docview/2261972988
https://pubmed.ncbi.nlm.nih.gov/PMC6627056
Volume 20
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