An Armored Mixed Conductor Interphase on a Dendrite‐Free Lithium‐Metal Anode

Lithium‐metal electrodes have undergone a comprehensive renaissance to meet the requirements of high‐energy‐density batteries due to their lowest electrode potential and the very high theoretical capacity. Unfortunately, the unstable interface between lithium and nonaqueous electrolyte induces dendr...

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Published in	Advanced materials (Weinheim) Vol. 30; no. 45; pp. e1804461 - n/a
Main Authors	Yan, Chong, Cheng, Xin‐Bing, Yao, Yu‐Xing, Shen, Xin, Li, Bo‐Quan, Li, Wen‐Jun, Zhang, Rui, Huang, Jia‐Qi, Li, Hong, Zhang, Qiang
Format	Journal Article
Language	English
Published	Germany Wiley Subscription Services, Inc 01.11.2018
Subjects	Anode effect Anodic protection Armor Chemical reactions Conductors cupric fluoride dendrite growth Dendritic structure Electrodes Electrolytes Electrolytic cells Ion currents Lithium Lithium batteries lithium‐metal anodes lithium‐metal batteries Materials science mixed conductor interface Modulus of elasticity Nonaqueous electrolytes Organic chemistry Protective coatings mixed conductor interface lithium-metal batteries cupric fluoride dendrite growth lithium-metal anodes
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Abstract	Lithium‐metal electrodes have undergone a comprehensive renaissance to meet the requirements of high‐energy‐density batteries due to their lowest electrode potential and the very high theoretical capacity. Unfortunately, the unstable interface between lithium and nonaqueous electrolyte induces dendritic Li and low Coulombic efficiency during repeated Li plating/stripping, which is one of the huge obstacles toward practical lithium‐metal batteries. Here, a composite mixed ionic/electronic conductor interphase (MCI) is formed on the surface of Li by in situ chemical reactions of a copper‐fluoride‐based solution and Li metal at room temperature. The as‐obtained MCI film acts like the armor of a soldier to protect the Li‐metal anode by its prioritized lithium storage, high ionic conductivity, and high Young's modulus. The armored MCI can effectively suppress Li‐dendrite growth and work effectively in LiNi0.5Co0.2Mn0.3O2/Li cells. The armored MCI presents fresh insights into the formation and regulation of the stable electrode–electrolyte interface and an effective strategy to protect Li‐metal anodes in working Li‐metal batteries. A composite mixed ionic/electronic conductor interphase (MCI) is formed on the surface of lithium by in situ chemical reactions of copper‐fluoride‐based solution and Li metal at room temperature. The as‐obtained MCI film acts like the armor of a soldier to protect the Li‐metal anode by its prioritized lithium storage, high ionic conductivity, and high Young's modulus.
AbstractList	Lithium‐metal electrodes have undergone a comprehensive renaissance to meet the requirements of high‐energy‐density batteries due to their lowest electrode potential and the very high theoretical capacity. Unfortunately, the unstable interface between lithium and nonaqueous electrolyte induces dendritic Li and low Coulombic efficiency during repeated Li plating/stripping, which is one of the huge obstacles toward practical lithium‐metal batteries. Here, a composite mixed ionic/electronic conductor interphase (MCI) is formed on the surface of Li by in situ chemical reactions of a copper‐fluoride‐based solution and Li metal at room temperature. The as‐obtained MCI film acts like the armor of a soldier to protect the Li‐metal anode by its prioritized lithium storage, high ionic conductivity, and high Young's modulus. The armored MCI can effectively suppress Li‐dendrite growth and work effectively in LiNi0.5Co0.2Mn0.3O2/Li cells. The armored MCI presents fresh insights into the formation and regulation of the stable electrode–electrolyte interface and an effective strategy to protect Li‐metal anodes in working Li‐metal batteries. A composite mixed ionic/electronic conductor interphase (MCI) is formed on the surface of lithium by in situ chemical reactions of copper‐fluoride‐based solution and Li metal at room temperature. The as‐obtained MCI film acts like the armor of a soldier to protect the Li‐metal anode by its prioritized lithium storage, high ionic conductivity, and high Young's modulus. Lithium‐metal electrodes have undergone a comprehensive renaissance to meet the requirements of high‐energy‐density batteries due to their lowest electrode potential and the very high theoretical capacity. Unfortunately, the unstable interface between lithium and nonaqueous electrolyte induces dendritic Li and low Coulombic efficiency during repeated Li plating/stripping, which is one of the huge obstacles toward practical lithium‐metal batteries. Here, a composite mixed ionic/electronic conductor interphase (MCI) is formed on the surface of Li by in situ chemical reactions of a copper‐fluoride‐based solution and Li metal at room temperature. The as‐obtained MCI film acts like the armor of a soldier to protect the Li‐metal anode by its prioritized lithium storage, high ionic conductivity, and high Young's modulus. The armored MCI can effectively suppress Li‐dendrite growth and work effectively in LiNi 0.5 Co 0.2 Mn 0.3 O 2 /Li cells. The armored MCI presents fresh insights into the formation and regulation of the stable electrode–electrolyte interface and an effective strategy to protect Li‐metal anodes in working Li‐metal batteries. Lithium-metal electrodes have undergone a comprehensive renaissance to meet the requirements of high-energy-density batteries due to their lowest electrode potential and the very high theoretical capacity. Unfortunately, the unstable interface between lithium and nonaqueous electrolyte induces dendritic Li and low Coulombic efficiency during repeated Li plating/stripping, which is one of the huge obstacles toward practical lithium-metal batteries. Here, a composite mixed ionic/electronic conductor interphase (MCI) is formed on the surface of Li by in situ chemical reactions of a copper-fluoride-based solution and Li metal at room temperature. The as-obtained MCI film acts like the armor of a soldier to protect the Li-metal anode by its prioritized lithium storage, high ionic conductivity, and high Young's modulus. The armored MCI can effectively suppress Li-dendrite growth and work effectively in LiNi Co Mn O /Li cells. The armored MCI presents fresh insights into the formation and regulation of the stable electrode-electrolyte interface and an effective strategy to protect Li-metal anodes in working Li-metal batteries. Lithium-metal electrodes have undergone a comprehensive renaissance to meet the requirements of high-energy-density batteries due to their lowest electrode potential and the very high theoretical capacity. Unfortunately, the unstable interface between lithium and nonaqueous electrolyte induces dendritic Li and low Coulombic efficiency during repeated Li plating/stripping, which is one of the huge obstacles toward practical lithium-metal batteries. Here, a composite mixed ionic/electronic conductor interphase (MCI) is formed on the surface of Li by in situ chemical reactions of a copper-fluoride-based solution and Li metal at room temperature. The as-obtained MCI film acts like the armor of a soldier to protect the Li-metal anode by its prioritized lithium storage, high ionic conductivity, and high Young's modulus. The armored MCI can effectively suppress Li-dendrite growth and work effectively in LiNi0.5 Co0.2 Mn0.3 O2 /Li cells. The armored MCI presents fresh insights into the formation and regulation of the stable electrode-electrolyte interface and an effective strategy to protect Li-metal anodes in working Li-metal batteries.Lithium-metal electrodes have undergone a comprehensive renaissance to meet the requirements of high-energy-density batteries due to their lowest electrode potential and the very high theoretical capacity. Unfortunately, the unstable interface between lithium and nonaqueous electrolyte induces dendritic Li and low Coulombic efficiency during repeated Li plating/stripping, which is one of the huge obstacles toward practical lithium-metal batteries. Here, a composite mixed ionic/electronic conductor interphase (MCI) is formed on the surface of Li by in situ chemical reactions of a copper-fluoride-based solution and Li metal at room temperature. The as-obtained MCI film acts like the armor of a soldier to protect the Li-metal anode by its prioritized lithium storage, high ionic conductivity, and high Young's modulus. The armored MCI can effectively suppress Li-dendrite growth and work effectively in LiNi0.5 Co0.2 Mn0.3 O2 /Li cells. The armored MCI presents fresh insights into the formation and regulation of the stable electrode-electrolyte interface and an effective strategy to protect Li-metal anodes in working Li-metal batteries. Lithium‐metal electrodes have undergone a comprehensive renaissance to meet the requirements of high‐energy‐density batteries due to their lowest electrode potential and the very high theoretical capacity. Unfortunately, the unstable interface between lithium and nonaqueous electrolyte induces dendritic Li and low Coulombic efficiency during repeated Li plating/stripping, which is one of the huge obstacles toward practical lithium‐metal batteries. Here, a composite mixed ionic/electronic conductor interphase (MCI) is formed on the surface of Li by in situ chemical reactions of a copper‐fluoride‐based solution and Li metal at room temperature. The as‐obtained MCI film acts like the armor of a soldier to protect the Li‐metal anode by its prioritized lithium storage, high ionic conductivity, and high Young's modulus. The armored MCI can effectively suppress Li‐dendrite growth and work effectively in LiNi0.5Co0.2Mn0.3O2/Li cells. The armored MCI presents fresh insights into the formation and regulation of the stable electrode–electrolyte interface and an effective strategy to protect Li‐metal anodes in working Li‐metal batteries.
Author	Huang, Jia‐Qi Li, Hong Yao, Yu‐Xing Li, Wen‐Jun Zhang, Qiang Li, Bo‐Quan Cheng, Xin‐Bing Shen, Xin Zhang, Rui Yan, Chong
Author_xml	– sequence: 1 givenname: Chong surname: Yan fullname: Yan, Chong organization: Beijing Institute of Technology – sequence: 2 givenname: Xin‐Bing surname: Cheng fullname: Cheng, Xin‐Bing organization: Tsinghua University – sequence: 3 givenname: Yu‐Xing surname: Yao fullname: Yao, Yu‐Xing organization: Tsinghua University – sequence: 4 givenname: Xin surname: Shen fullname: Shen, Xin organization: Tsinghua University – sequence: 5 givenname: Bo‐Quan surname: Li fullname: Li, Bo‐Quan organization: Tsinghua University – sequence: 6 givenname: Wen‐Jun surname: Li fullname: Li, Wen‐Jun organization: Chinese Academy of Sciences – sequence: 7 givenname: Rui surname: Zhang fullname: Zhang, Rui organization: Tsinghua University – sequence: 8 givenname: Jia‐Qi surname: Huang fullname: Huang, Jia‐Qi email: jqhuang@bit.edu.cn organization: Beijing Institute of Technology – sequence: 9 givenname: Hong surname: Li fullname: Li, Hong email: hli@iphy.ac.cn organization: Chinese Academy of Sciences – sequence: 10 givenname: Qiang orcidid: 0000-0002-3929-1541 surname: Zhang fullname: Zhang, Qiang email: zhang-qiang@mails.tsinghua.edu.cn organization: Tsinghua University
BackLink	https://www.ncbi.nlm.nih.gov/pubmed/30259585$$D View this record in MEDLINE/PubMed
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Snippet	Lithium‐metal electrodes have undergone a comprehensive renaissance to meet the requirements of high‐energy‐density batteries due to their lowest electrode... Lithium-metal electrodes have undergone a comprehensive renaissance to meet the requirements of high-energy-density batteries due to their lowest electrode...
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SubjectTerms	Anode effect Anodic protection Armor Chemical reactions Conductors cupric fluoride dendrite growth Dendritic structure Electrodes Electrolytes Electrolytic cells Ion currents Lithium Lithium batteries lithium‐metal anodes lithium‐metal batteries Materials science mixed conductor interface Modulus of elasticity Nonaqueous electrolytes Organic chemistry Protective coatings
Title	An Armored Mixed Conductor Interphase on a Dendrite‐Free Lithium‐Metal Anode
URI	https://onlinelibrary.wiley.com/doi/abs/10.1002%2Fadma.201804461 https://www.ncbi.nlm.nih.gov/pubmed/30259585 https://www.proquest.com/docview/2130068485 https://www.proquest.com/docview/2113286220
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