Nanoscale structural oscillations in perovskite oxides induced by oxygen evolution

Understanding the interaction between water and oxides is critical for many technological applications, including energy storage, surface wetting/self-cleaning, photocatalysis and sensors. Here, we report observations of strong structural oscillations of Ba 0.5 Sr 0.5 Co 0.8 Fe 0.2 O 3−δ (BSCF) in t...

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Published inNature materials Vol. 16; no. 1; pp. 121 - 126
Main Authors Han, Binghong, Stoerzinger, Kelsey A., Tileli, Vasiliki, Gamalski, Andrew D., Stach, Eric A., Shao-Horn, Yang
Format Journal Article
LanguageEnglish
Published London Nature Publishing Group UK 01.01.2017
Nature Publishing Group
Subjects
121/143
639/301/299/161/886
639/301/930/328/2082
639/638/542
Biomaterials
Bubbles
Center for Functional Nanomaterials
Collapse
Condensed Matter Physics
electron beam interactions
Electron irradiation
ENERGY STORAGE
Formations
Irradiation
MATERIALS SCIENCE
Nanostructure
Nanotechnology
Optical and Electronic Materials
Oscillations
Oxidation
Oxides
Oxygen
Perovskite
photocatalysis
Sensors
Spectroscopy
Water
water splitting
Water uptake
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Abstract Understanding the interaction between water and oxides is critical for many technological applications, including energy storage, surface wetting/self-cleaning, photocatalysis and sensors. Here, we report observations of strong structural oscillations of Ba 0.5 Sr 0.5 Co 0.8 Fe 0.2 O 3−δ (BSCF) in the presence of both H 2 O vapour and electron irradiation using environmental transmission electron microscopy. These oscillations are related to the formation and collapse of gaseous bubbles. Electron energy-loss spectroscopy provides direct evidence of O 2 formation in these bubbles due to the incorporation of H 2 O into BSCF. SrCoO 3−δ was found to exhibit small oscillations, while none were observed for La 0.5 Sr 0.5 CoO 3−δ and LaCoO 3 . The structural oscillations of BSCF can be attributed to the fact that its oxygen 2 p -band centre is close to the Fermi level, which leads to a low energy penalty for oxygen vacancy formation, high ion mobility, and high water uptake. This work provides surprising insights into the interaction between water and oxides under electron-beam irradiation. Understanding interactions between water and oxides is crucial for energy storage and photocatalysis. The combined effect of water and electron irradiation on perovskite catalysts results in structural oscillation triggered by gaseous bubbles.
AbstractList Understanding the interaction between water and oxides is critical for many technological applications, including energy storage, surface wetting/self-cleaning, photocatalysis and sensors. Here, we report observations of strong structural oscillations of Ba Sr Co Fe O (BSCF) in the presence of both H O vapour and electron irradiation using environmental transmission electron microscopy. These oscillations are related to the formation and collapse of gaseous bubbles. Electron energy-loss spectroscopy provides direct evidence of O formation in these bubbles due to the incorporation of H O into BSCF. SrCoO was found to exhibit small oscillations, while none were observed for La Sr CoO and LaCoO . The structural oscillations of BSCF can be attributed to the fact that its oxygen 2p-band centre is close to the Fermi level, which leads to a low energy penalty for oxygen vacancy formation, high ion mobility, and high water uptake. This work provides surprising insights into the interaction between water and oxides under electron-beam irradiation.
Understanding the interaction between water and oxides is critical for many technological applications, including energy storage, surface wetting/self-cleaning, photocatalysis and sensors. In this paper, we report observations of strong structural oscillations of Ba0.5Sr0.5Co0.8Fe0.2O3$-$δ (BSCF) in the presence of both H2O vapour and electron irradiation using environmental transmission electron microscopy. These oscillations are related to the formation and collapse of gaseous bubbles. Electron energy-loss spectroscopy provides direct evidence of O2 formation in these bubbles due to the incorporation of H2O into BSCF. SrCoO3$-$δ was found to exhibit small oscillations, while none were observed for La0.5Sr0.5CoO3$-$δ and LaCoO3. The structural oscillations of BSCF can be attributed to the fact that its oxygen 2p-band centre is close to the Fermi level, which leads to a low energy penalty for oxygen vacancy formation, high ion mobility, and high water uptake. This work provides surprising insights into the interaction between water and oxides under electron-beam irradiation.
Understanding the interaction between water and oxides is critical for many technological applications, including energy storage, surface wetting/self-cleaning, photocatalysis and sensors. Here, we report observations of strong structural oscillations of Ba0.5Sr0.5Co0.8Fe0.2O3-δ (BSCF) in the presence of both H2O vapour and electron irradiation using environmental transmission electron microscopy. These oscillations are related to the formation and collapse of gaseous bubbles. Electron energy-loss spectroscopy provides direct evidence of O2 formation in these bubbles due to the incorporation of H2O into BSCF. SrCoO3-δ was found to exhibit small oscillations, while none were observed for La0.5Sr0.5CoO3-δ and LaCoO3. The structural oscillations of BSCF can be attributed to the fact that its oxygen 2p-band centre is close to the Fermi level, which leads to a low energy penalty for oxygen vacancy formation, high ion mobility, and high water uptake. This work provides surprising insights into the interaction between water and oxides under electron-beam irradiation.Understanding the interaction between water and oxides is critical for many technological applications, including energy storage, surface wetting/self-cleaning, photocatalysis and sensors. Here, we report observations of strong structural oscillations of Ba0.5Sr0.5Co0.8Fe0.2O3-δ (BSCF) in the presence of both H2O vapour and electron irradiation using environmental transmission electron microscopy. These oscillations are related to the formation and collapse of gaseous bubbles. Electron energy-loss spectroscopy provides direct evidence of O2 formation in these bubbles due to the incorporation of H2O into BSCF. SrCoO3-δ was found to exhibit small oscillations, while none were observed for La0.5Sr0.5CoO3-δ and LaCoO3. The structural oscillations of BSCF can be attributed to the fact that its oxygen 2p-band centre is close to the Fermi level, which leads to a low energy penalty for oxygen vacancy formation, high ion mobility, and high water uptake. This work provides surprising insights into the interaction between water and oxides under electron-beam irradiation.
Understanding the interaction between water and oxides is critical for many technological applications, including energy storage, surface wetting/self-cleaning, photocatalysis and sensors. Here, we report observations of strong structural oscillations of Ba sub(0.5)Sr sub(0.5)Co sub(0.8)Fe sub(0.2)O sub(3- delta ) (BSCF) in the presence of both H sub(2)O vapour and electron irradiation using environmental transmission electron microscopy. These oscillations are related to the formation and collapse of gaseous bubbles. Electron energy-loss spectroscopy provides direct evidence of O sub(2) formation in these bubbles due to the incorporation of H sub(2)O into BSCF. SrCoO sub(3- delta ) was found to exhibit small oscillations, while none were observed for La sub(0.5)Sr sub(0.5)CoO sub(3- delta ) and LaCoO sub(3). The structural oscillations of BSCF can be attributed to the fact that its oxygen 2p-band centre is close to the Fermi level, which leads to a low energy penalty for oxygen vacancy formation, high ion mobility, and high water uptake. This work provides surprising insights into the interaction between water and oxides under electron-beam irradiation.
Understanding the interaction between water and oxides is critical for many technological applications, including energy storage, surface wetting/self-cleaning, photocatalysis and sensors. Here, we report observations of strong structural oscillations of Ba 0.5 Sr 0.5 Co 0.8 Fe 0.2 O 3−δ (BSCF) in the presence of both H 2 O vapour and electron irradiation using environmental transmission electron microscopy. These oscillations are related to the formation and collapse of gaseous bubbles. Electron energy-loss spectroscopy provides direct evidence of O 2 formation in these bubbles due to the incorporation of H 2 O into BSCF. SrCoO 3−δ was found to exhibit small oscillations, while none were observed for La 0.5 Sr 0.5 CoO 3−δ and LaCoO 3 . The structural oscillations of BSCF can be attributed to the fact that its oxygen 2 p -band centre is close to the Fermi level, which leads to a low energy penalty for oxygen vacancy formation, high ion mobility, and high water uptake. This work provides surprising insights into the interaction between water and oxides under electron-beam irradiation. Understanding interactions between water and oxides is crucial for energy storage and photocatalysis. The combined effect of water and electron irradiation on perovskite catalysts results in structural oscillation triggered by gaseous bubbles.
Understanding the interaction between water and oxides is critical for many technological applications, including energy storage, surface wetting/self-cleaning, photocatalysis and sensors. Here, we report observations of strong structural oscillations of Ba0.5Sr0.5Co0.8Fe0.2O3 (BSCF) in the presence of both H2O vapour and electron irradiation using environmental transmission electron microscopy. These oscillations are related to the formation and collapse of gaseous bubbles. Electron energy-loss spectroscopy provides direct evidence of O2 formation in these bubbles due to the incorporation of H2O into BSCF. SrCoO3 was found to exhibit small oscillations, while none were observed for La0.5Sr0.5CoO3 and LaCoO3. The structural oscillations of BSCF can be attributed to the fact that its oxygen 2p-band centre is close to the Fermi level, which leads to a low energy penalty for oxygen vacancy formation, high ion mobility, and high water uptake. This work provides surprising insights into the interaction between water and oxides under electron-beam irradiation.
Author Tileli, Vasiliki
Han, Binghong
Stoerzinger, Kelsey A.
Stach, Eric A.
Shao-Horn, Yang
Gamalski, Andrew D.
Author_xml – sequence: 1
  givenname: Binghong
  orcidid: 0000-0002-2919-3235
  surname: Han
  fullname: Han, Binghong
  organization: Department of Materials Science and Engineering
– sequence: 2
  givenname: Kelsey A.
  surname: Stoerzinger
  fullname: Stoerzinger, Kelsey A.
  organization: Department of Materials Science and Engineering
– sequence: 3
  givenname: Vasiliki
  surname: Tileli
  fullname: Tileli, Vasiliki
  organization: Institute of Materials, École Polytechnique Fédérale de Lausanne
– sequence: 4
  givenname: Andrew D.
  surname: Gamalski
  fullname: Gamalski, Andrew D.
  organization: Center for Functional Nanomaterials, Brookhaven National Laboratory
– sequence: 5
  givenname: Eric A.
  orcidid: 0000-0002-3366-2153
  surname: Stach
  fullname: Stach, Eric A.
  email: estach@bnl.gov
  organization: Center for Functional Nanomaterials, Brookhaven National Laboratory
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  givenname: Yang
  surname: Shao-Horn
  fullname: Shao-Horn, Yang
  email: shaohorn@mit.edu
  organization: Department of Materials Science and Engineering, Department of Mechanical Engineering, Massachusetts Institute of Technology
BackLink https://www.ncbi.nlm.nih.gov/pubmed/27698352$$D View this record in MEDLINE/PubMed
https://www.osti.gov/servlets/purl/1349577$$D View this record in Osti.gov
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ContentType Journal Article
Copyright Springer Nature Limited 2017
Copyright Nature Publishing Group Jan 2017
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– notice: Copyright Nature Publishing Group Jan 2017
CorporateAuthor Brookhaven National Laboratory (BNL), Upton, NY (United States). Center for Functional Nanomaterials (CFN)
CorporateAuthor_xml – name: Brookhaven National Laboratory (BNL), Upton, NY (United States). Center for Functional Nanomaterials (CFN)
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Snippet Understanding the interaction between water and oxides is critical for many technological applications, including energy storage, surface...
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SubjectTerms 121/143
639/301/299/161/886
639/301/930/328/2082
639/638/542
Biomaterials
Bubbles
Center for Functional Nanomaterials
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Condensed Matter Physics
electron beam interactions
Electron irradiation
ENERGY STORAGE
Formations
Irradiation
MATERIALS SCIENCE
Nanostructure
Nanotechnology
Optical and Electronic Materials
Oscillations
Oxidation
Oxides
Oxygen
Perovskite
photocatalysis
Sensors
Spectroscopy
Water
water splitting
Water uptake
Title Nanoscale structural oscillations in perovskite oxides induced by oxygen evolution
URI https://link.springer.com/article/10.1038/nmat4764
https://www.ncbi.nlm.nih.gov/pubmed/27698352
https://www.proquest.com/docview/1856908681
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https://www.osti.gov/servlets/purl/1349577
Volume 16
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