Manganese Catalyzed Hydrogenation of Organic Carbonates to Methanol and Alcohols
The first example of a homogeneous catalyst based on an earth‐abundant metal for the hydrogenation of organic carbonates to methanol and alcohols is reported. Based on the mechanistic investigation, which indicates metal‐ligand cooperation between the manganese center and the N−H group of the pincer...
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| Published in | Angewandte Chemie International Edition Vol. 57; no. 37; pp. 12076 - 12080 |
|---|---|
| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
WEINHEIM
Wiley
10.09.2018
Wiley Subscription Services, Inc |
| Edition | International ed. in English |
| Subjects | |
| Online Access | Get full text |
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| Abstract | The first example of a homogeneous catalyst based on an earth‐abundant metal for the hydrogenation of organic carbonates to methanol and alcohols is reported. Based on the mechanistic investigation, which indicates metal‐ligand cooperation between the manganese center and the N−H group of the pincer ligand, we propose that the hydrogenation of organic carbonates to methanol occurs via formate and aldehyde intermediates. The reaction offers an indirect route for the conversion of CO2 to methanol, which coupled with the use of an earth abundant catalyst, makes the overall process environmentally benign and sustainable.
The first example of a homogeneous catalyst based on an earth‐abundant metal for the hydrogenation of organic carbonates to methanol is reported. The reaction is catalyzed by a manganese pincer complex and offers an indirect route to convert CO2 to methanol, making the overall process environmentally benign and sustainable. |
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| AbstractList | The first example of a homogeneous catalyst based on an earth-abundant metal for the hydrogenation of organic carbonates to methanol and alcohols is reported. Based on the mechanistic investigation, which indicates metal-ligand cooperation between the manganese center and the N II group of the pincer ligand, we propose that the hydrogenation of organic carbonates to methanol occurs via formate and aldehyde intermediates. The reaction offers an indirect route for the conversion of CO2 to methanol, which coupled with the use of an earth abundant catalyst, makes the overall process environmentally benign and sustainable. The first example of a homogeneous catalyst based on an earth-abundant metal for the hydrogenation of organic carbonates to methanol and alcohols is reported. Based on the mechanistic investigation, which indicates metal-ligand cooperation between the manganese center and the N-H group of the pincer ligand, we propose that the hydrogenation of organic carbonates to methanol occurs via formate and aldehyde intermediates. The reaction offers an indirect route for the conversion of CO2 to methanol, which coupled with the use of an earth abundant catalyst, makes the overall process environmentally benign and sustainable. The first example of a homogeneous catalyst based on an earth-abundant metal for the hydrogenation of organic carbonates to methanol and alcohols is reported. Based on the mechanistic investigation, which indicates metal-ligand cooperation between the manganese center and the N-H group of the pincer ligand, we propose that the hydrogenation of organic carbonates to methanol occurs via formate and aldehyde intermediates. The reaction offers an indirect route for the conversion of CO to methanol, which coupled with the use of an earth abundant catalyst, makes the overall process environmentally benign and sustainable. The first example of a homogeneous catalyst based on an earth‐abundant metal for the hydrogenation of organic carbonates to methanol and alcohols is reported. Based on the mechanistic investigation, which indicates metal‐ligand cooperation between the manganese center and the N−H group of the pincer ligand, we propose that the hydrogenation of organic carbonates to methanol occurs via formate and aldehyde intermediates. The reaction offers an indirect route for the conversion of CO2 to methanol, which coupled with the use of an earth abundant catalyst, makes the overall process environmentally benign and sustainable. The first example of a homogeneous catalyst based on an earth‐abundant metal for the hydrogenation of organic carbonates to methanol is reported. The reaction is catalyzed by a manganese pincer complex and offers an indirect route to convert CO2 to methanol, making the overall process environmentally benign and sustainable. The first example of a homogeneous catalyst based on an earth‐abundant metal for the hydrogenation of organic carbonates to methanol and alcohols is reported. Based on the mechanistic investigation, which indicates metal‐ligand cooperation between the manganese center and the N−H group of the pincer ligand, we propose that the hydrogenation of organic carbonates to methanol occurs via formate and aldehyde intermediates. The reaction offers an indirect route for the conversion of CO2 to methanol, which coupled with the use of an earth abundant catalyst, makes the overall process environmentally benign and sustainable. Abstract The first example of a homogeneous catalyst based on an earth‐abundant metal for the hydrogenation of organic carbonates to methanol and alcohols is reported. Based on the mechanistic investigation, which indicates metal‐ligand cooperation between the manganese center and the N−H group of the pincer ligand, we propose that the hydrogenation of organic carbonates to methanol occurs via formate and aldehyde intermediates. The reaction offers an indirect route for the conversion of CO 2 to methanol, which coupled with the use of an earth abundant catalyst, makes the overall process environmentally benign and sustainable. |
| Author | Kumar, Amit Milstein, David Espinosa‐Jalapa, Noel Angel Janes, Trevor |
| Author_xml | – sequence: 1 givenname: Amit surname: Kumar fullname: Kumar, Amit organization: Weizmann Institute of Science – sequence: 2 givenname: Trevor surname: Janes fullname: Janes, Trevor organization: Weizmann Institute of Science – sequence: 3 givenname: Noel Angel surname: Espinosa‐Jalapa fullname: Espinosa‐Jalapa, Noel Angel organization: Universität Regensburg – sequence: 4 givenname: David orcidid: 0000-0002-2320-0262 surname: Milstein fullname: Milstein, David email: david.milstein@weizmann.ac.il organization: Weizmann Institute of Science |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/30035855$$D View this record in MEDLINE/PubMed |
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| Keywords | carbon dioxide LOW-PRESSURE HYDROGENATION BICARBONATES DEFINED IRON CATALYST CO2 carbonates hydrogenation DIOXIDE HYDROGENATION AMINES methanol HOMOGENEOUS CATALYSIS CYCLIC CARBONATES PINCER COMPLEX DERIVATIVES Manganese |
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| Snippet | The first example of a homogeneous catalyst based on an earth‐abundant metal for the hydrogenation of organic carbonates to methanol and alcohols is reported.... The first example of a homogeneous catalyst based on an earth-abundant metal for the hydrogenation of organic carbonates to methanol and alcohols is reported.... Abstract The first example of a homogeneous catalyst based on an earth‐abundant metal for the hydrogenation of organic carbonates to methanol and alcohols is... |
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| SubjectTerms | Alcohol Alcohols Carbon dioxide Carbonates Catalysis Catalysts Chemistry Chemistry, Multidisciplinary Hydrogenation Intermediates Ligands Manganese Metals Methanol Physical Sciences Science & Technology |
| Title | Manganese Catalyzed Hydrogenation of Organic Carbonates to Methanol and Alcohols |
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