Porphyrinic Zirconium Metal–Organic Frameworks (MOFs) as Heterogeneous Photocatalysts for PET‐RAFT Polymerization and Stereolithography
In this study, porphyrinic zirconium (Zr) MOFs were investigated as heterogeneous photocatalysts for photoinduced electron transfer‐reversible addition‐fragmentation chain transfer (PET‐RAFT) polymerization of various monomers under a broad range of wavelengths, producing polymers with high monomer...
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| Published in | Angewandte Chemie International Edition Vol. 60; no. 10; pp. 5489 - 5496 |
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| Main Authors | , , , , , , , , |
| Format | Journal Article |
| Language | English |
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Wiley Subscription Services, Inc
01.03.2021
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| Edition | International ed. in English |
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| Abstract | In this study, porphyrinic zirconium (Zr) MOFs were investigated as heterogeneous photocatalysts for photoinduced electron transfer‐reversible addition‐fragmentation chain transfer (PET‐RAFT) polymerization of various monomers under a broad range of wavelengths, producing polymers with high monomer conversions, narrow molecular weight distributions, low dispersity and good chain‐end fidelity. Screening of various porphyrinic Zr‐MOFs (Zn) containing Zn‐metalled porphyrinic ligands demonstrated that MOF‐525 (Zn) with the smallest size had the best photocatalytic activity in PET‐RAFT polymerization, due to enhanced dispersion and light penetration. Oxygen tolerance and temporal control were also demonstrated during MOF catalysed PET‐RAFT. Results suggested that the polymerization rates were significantly affected by changing the size and surface area of MOFs, and the heterogeneous MOF photocatalysts could be easily separated and recycled for up to five independent PET‐RAFT polymerizations without an obvious decrease in efficiency. Finally, the MOF photocatalysts were utilized to create three‐dimensional polymeric objects with high resolution via visible light mediated stereolithography in an open‐air environment.
Porphyrinic zirconium MOFs act as heterogeneous photocatalysts for photoinduced electron transfer‐reversible addition‐fragmentation chain transfer (PET‐RAFT) polymerization of various monomers under a broad range of wavelengths, producing polymers with high monomer conversions, narrow molecular weight distributions, low dispersity and good chain‐end fidelity |
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| AbstractList | In this study, porphyrinic zirconium (Zr) MOFs were investigated as heterogeneous photocatalysts for photoinduced electron transfer-reversible addition-fragmentation chain transfer (PET-RAFT) polymerization of various monomers under a broad range of wavelengths, producing polymers with high monomer conversions, narrow molecular weight distributions, low dispersity and good chain-end fidelity. Screening of various porphyrinic Zr-MOFs (Zn) containing Zn-metalled porphyrinic ligands demonstrated that MOF-525 (Zn) with the smallest size had the best photocatalytic activity in PET-RAFT polymerization, due to enhanced dispersion and light penetration. Oxygen tolerance and temporal control were also demonstrated during MOF catalysed PET-RAFT. Results suggested that the polymerization rates were significantly affected by changing the size and surface area of MOFs, and the heterogeneous MOF photocatalysts could be easily separated and recycled for up to five independent PET-RAFT polymerizations without an obvious decrease in efficiency. Finally, the MOF photocatalysts were utilized to create three-dimensional polymeric objects with high resolution via visible light mediated stereolithography in an open-air environment.In this study, porphyrinic zirconium (Zr) MOFs were investigated as heterogeneous photocatalysts for photoinduced electron transfer-reversible addition-fragmentation chain transfer (PET-RAFT) polymerization of various monomers under a broad range of wavelengths, producing polymers with high monomer conversions, narrow molecular weight distributions, low dispersity and good chain-end fidelity. Screening of various porphyrinic Zr-MOFs (Zn) containing Zn-metalled porphyrinic ligands demonstrated that MOF-525 (Zn) with the smallest size had the best photocatalytic activity in PET-RAFT polymerization, due to enhanced dispersion and light penetration. Oxygen tolerance and temporal control were also demonstrated during MOF catalysed PET-RAFT. Results suggested that the polymerization rates were significantly affected by changing the size and surface area of MOFs, and the heterogeneous MOF photocatalysts could be easily separated and recycled for up to five independent PET-RAFT polymerizations without an obvious decrease in efficiency. Finally, the MOF photocatalysts were utilized to create three-dimensional polymeric objects with high resolution via visible light mediated stereolithography in an open-air environment. In this study, porphyrinic zirconium (Zr) MOFs were investigated as heterogeneous photocatalysts for photoinduced electron transfer‐reversible addition‐fragmentation chain transfer (PET‐RAFT) polymerization of various monomers under a broad range of wavelengths, producing polymers with high monomer conversions, narrow molecular weight distributions, low dispersity and good chain‐end fidelity. Screening of various porphyrinic Zr‐MOFs (Zn) containing Zn‐metalled porphyrinic ligands demonstrated that MOF‐525 (Zn) with the smallest size had the best photocatalytic activity in PET‐RAFT polymerization, due to enhanced dispersion and light penetration. Oxygen tolerance and temporal control were also demonstrated during MOF catalysed PET‐RAFT. Results suggested that the polymerization rates were significantly affected by changing the size and surface area of MOFs, and the heterogeneous MOF photocatalysts could be easily separated and recycled for up to five independent PET‐RAFT polymerizations without an obvious decrease in efficiency. Finally, the MOF photocatalysts were utilized to create three‐dimensional polymeric objects with high resolution via visible light mediated stereolithography in an open‐air environment. In this study, porphyrinic zirconium (Zr) MOFs were investigated as heterogeneous photocatalysts for photoinduced electron transfer‐reversible addition‐fragmentation chain transfer (PET‐RAFT) polymerization of various monomers under a broad range of wavelengths, producing polymers with high monomer conversions, narrow molecular weight distributions, low dispersity and good chain‐end fidelity. Screening of various porphyrinic Zr‐MOFs (Zn) containing Zn‐metalled porphyrinic ligands demonstrated that MOF‐525 (Zn) with the smallest size had the best photocatalytic activity in PET‐RAFT polymerization, due to enhanced dispersion and light penetration. Oxygen tolerance and temporal control were also demonstrated during MOF catalysed PET‐RAFT. Results suggested that the polymerization rates were significantly affected by changing the size and surface area of MOFs, and the heterogeneous MOF photocatalysts could be easily separated and recycled for up to five independent PET‐RAFT polymerizations without an obvious decrease in efficiency. Finally, the MOF photocatalysts were utilized to create three‐dimensional polymeric objects with high resolution via visible light mediated stereolithography in an open‐air environment. Porphyrinic zirconium MOFs act as heterogeneous photocatalysts for photoinduced electron transfer‐reversible addition‐fragmentation chain transfer (PET‐RAFT) polymerization of various monomers under a broad range of wavelengths, producing polymers with high monomer conversions, narrow molecular weight distributions, low dispersity and good chain‐end fidelity |
| Author | Shi, Xiaobing Namivandi‐Zangeneh, Rashin Liang, Kang Kuchel, Rhiannon P Corrigan, Nathaniel Jung, Kenward Boyer, Cyrille Zhang, Liwen Zhang, Zhiheng |
| Author_xml | – sequence: 1 givenname: Liwen surname: Zhang fullname: Zhang, Liwen organization: The University of New South Wales – sequence: 2 givenname: Xiaobing surname: Shi fullname: Shi, Xiaobing organization: The University of New South Wales – sequence: 3 givenname: Zhiheng surname: Zhang fullname: Zhang, Zhiheng organization: The University of New South Wales – sequence: 4 givenname: Rhiannon P surname: Kuchel fullname: Kuchel, Rhiannon P organization: The University of New South Wales – sequence: 5 givenname: Rashin surname: Namivandi‐Zangeneh fullname: Namivandi‐Zangeneh, Rashin organization: The University of New South Wales – sequence: 6 givenname: Nathaniel surname: Corrigan fullname: Corrigan, Nathaniel organization: The University of New South Wales – sequence: 7 givenname: Kenward surname: Jung fullname: Jung, Kenward organization: The University of New South Wales – sequence: 8 givenname: Kang surname: Liang fullname: Liang, Kang email: kang.liang@unsw.edu.au organization: The University of New South Wales – sequence: 9 givenname: Cyrille orcidid: 0000-0002-4564-4702 surname: Boyer fullname: Boyer, Cyrille email: cboyer@unsw.edu.au organization: The University of New South Wales |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/33179352$$D View this record in MEDLINE/PubMed |
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| Snippet | In this study, porphyrinic zirconium (Zr) MOFs were investigated as heterogeneous photocatalysts for photoinduced electron transfer‐reversible... In this study, porphyrinic zirconium (Zr) MOFs were investigated as heterogeneous photocatalysts for photoinduced electron transfer-reversible... |
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| SubjectTerms | 3D printing Addition polymerization Catalytic activity Chain transfer Electron transfer green chemistry Light penetration Lithography Metal-organic frameworks metal–organic frameworks (MOFs) Molecular weight Molecular weight distribution Monomers Photocatalysis Photocatalysts photopolymerization Polymerization Polymers stereolithography Wavelengths Zinc Zirconium |
| Title | Porphyrinic Zirconium Metal–Organic Frameworks (MOFs) as Heterogeneous Photocatalysts for PET‐RAFT Polymerization and Stereolithography |
| URI | https://onlinelibrary.wiley.com/doi/abs/10.1002%2Fanie.202014208 https://www.ncbi.nlm.nih.gov/pubmed/33179352 https://www.proquest.com/docview/2491851545 https://www.proquest.com/docview/2460082511 |
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