Lithium Nitrate Solvation Chemistry in Carbonate Electrolyte Sustains High‐Voltage Lithium Metal Batteries
The lithium metal anode is regarded as a promising candidate in next‐generation energy storage devices. Lithium nitrate (LiNO3) is widely applied as an effective additive in ether electrolyte to increase the interfacial stability in batteries containing lithium metal anodes. However, because of its...
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| Published in | Angewandte Chemie International Edition Vol. 57; no. 43; pp. 14055 - 14059 |
|---|---|
| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Germany
Wiley Subscription Services, Inc
22.10.2018
|
| Edition | International ed. in English |
| Subjects | |
| Online Access | Get full text |
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| Abstract | The lithium metal anode is regarded as a promising candidate in next‐generation energy storage devices. Lithium nitrate (LiNO3) is widely applied as an effective additive in ether electrolyte to increase the interfacial stability in batteries containing lithium metal anodes. However, because of its poor solubility LiNO3 is rarely utilized in the high‐voltage window provided by carbonate electrolyte. Dissolution of LiNO3 in carbonate electrolyte is realized through an effective solvation regulation strategy. LiNO3 can be directly dissolved in an ethylene carbonate/diethyl carbonate electrolyte mixture by adding trace amounts of copper fluoride as a dissolution promoter. LiNO3 protects the Li metal anode in a working high‐voltage Li metal battery. When a LiNi0.80Co0.15Al0.05O2 cathode is paired with a Li metal anode, an extraordinary capacity retention of 53 % is achieved after 300 cycles (13 % after 200 cycles for LiNO3‐free electrolyte) and a very high average Coulombic efficiency above 99.5 % is achieved at 0.5 C. The solvation chemistry of LiNO3‐containing carbonate electrolyte may sustain high‐voltage Li metal anodes operating in corrosive carbonate electrolytes.
Liquid assets: LiNO3 can be dissolved directly in an ethylene carbonate/diethyl carbonate electrolyte mixture by adding a trace amount of copper fluoride to promote dissolution. The solvation structure of the electrolyte system protects the lithium metal anode in a working high‐voltage lithium metal battery. NCA=LiNi0.80Co0.15Al0.05O2. |
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| AbstractList | The lithium metal anode is regarded as a promising candidate in next-generation energy storage devices. Lithium nitrate (LiNO
) is widely applied as an effective additive in ether electrolyte to increase the interfacial stability in batteries containing lithium metal anodes. However, because of its poor solubility LiNO
is rarely utilized in the high-voltage window provided by carbonate electrolyte. Dissolution of LiNO
in carbonate electrolyte is realized through an effective solvation regulation strategy. LiNO
can be directly dissolved in an ethylene carbonate/diethyl carbonate electrolyte mixture by adding trace amounts of copper fluoride as a dissolution promoter. LiNO
protects the Li metal anode in a working high-voltage Li metal battery. When a LiNi
Co
Al
O
cathode is paired with a Li metal anode, an extraordinary capacity retention of 53 % is achieved after 300 cycles (13 % after 200 cycles for LiNO
-free electrolyte) and a very high average Coulombic efficiency above 99.5 % is achieved at 0.5 C. The solvation chemistry of LiNO
-containing carbonate electrolyte may sustain high-voltage Li metal anodes operating in corrosive carbonate electrolytes. The lithium metal anode is regarded as a promising candidate in next‐generation energy storage devices. Lithium nitrate (LiNO3) is widely applied as an effective additive in ether electrolyte to increase the interfacial stability in batteries containing lithium metal anodes. However, because of its poor solubility LiNO3 is rarely utilized in the high‐voltage window provided by carbonate electrolyte. Dissolution of LiNO3 in carbonate electrolyte is realized through an effective solvation regulation strategy. LiNO3 can be directly dissolved in an ethylene carbonate/diethyl carbonate electrolyte mixture by adding trace amounts of copper fluoride as a dissolution promoter. LiNO3 protects the Li metal anode in a working high‐voltage Li metal battery. When a LiNi0.80Co0.15Al0.05O2 cathode is paired with a Li metal anode, an extraordinary capacity retention of 53 % is achieved after 300 cycles (13 % after 200 cycles for LiNO3‐free electrolyte) and a very high average Coulombic efficiency above 99.5 % is achieved at 0.5 C. The solvation chemistry of LiNO3‐containing carbonate electrolyte may sustain high‐voltage Li metal anodes operating in corrosive carbonate electrolytes. Liquid assets: LiNO3 can be dissolved directly in an ethylene carbonate/diethyl carbonate electrolyte mixture by adding a trace amount of copper fluoride to promote dissolution. The solvation structure of the electrolyte system protects the lithium metal anode in a working high‐voltage lithium metal battery. NCA=LiNi0.80Co0.15Al0.05O2. The lithium metal anode is regarded as a promising candidate in next‐generation energy storage devices. Lithium nitrate (LiNO 3 ) is widely applied as an effective additive in ether electrolyte to increase the interfacial stability in batteries containing lithium metal anodes. However, because of its poor solubility LiNO 3 is rarely utilized in the high‐voltage window provided by carbonate electrolyte. Dissolution of LiNO 3 in carbonate electrolyte is realized through an effective solvation regulation strategy. LiNO 3 can be directly dissolved in an ethylene carbonate/diethyl carbonate electrolyte mixture by adding trace amounts of copper fluoride as a dissolution promoter. LiNO 3 protects the Li metal anode in a working high‐voltage Li metal battery. When a LiNi 0.80 Co 0.15 Al 0.05 O 2 cathode is paired with a Li metal anode, an extraordinary capacity retention of 53 % is achieved after 300 cycles (13 % after 200 cycles for LiNO 3 ‐free electrolyte) and a very high average Coulombic efficiency above 99.5 % is achieved at 0.5 C. The solvation chemistry of LiNO 3 ‐containing carbonate electrolyte may sustain high‐voltage Li metal anodes operating in corrosive carbonate electrolytes. The lithium metal anode is regarded as a promising candidate in next-generation energy storage devices. Lithium nitrate (LiNO3 ) is widely applied as an effective additive in ether electrolyte to increase the interfacial stability in batteries containing lithium metal anodes. However, because of its poor solubility LiNO3 is rarely utilized in the high-voltage window provided by carbonate electrolyte. Dissolution of LiNO3 in carbonate electrolyte is realized through an effective solvation regulation strategy. LiNO3 can be directly dissolved in an ethylene carbonate/diethyl carbonate electrolyte mixture by adding trace amounts of copper fluoride as a dissolution promoter. LiNO3 protects the Li metal anode in a working high-voltage Li metal battery. When a LiNi0.80 Co0.15 Al0.05 O2 cathode is paired with a Li metal anode, an extraordinary capacity retention of 53 % is achieved after 300 cycles (13 % after 200 cycles for LiNO3 -free electrolyte) and a very high average Coulombic efficiency above 99.5 % is achieved at 0.5 C. The solvation chemistry of LiNO3 -containing carbonate electrolyte may sustain high-voltage Li metal anodes operating in corrosive carbonate electrolytes.The lithium metal anode is regarded as a promising candidate in next-generation energy storage devices. Lithium nitrate (LiNO3 ) is widely applied as an effective additive in ether electrolyte to increase the interfacial stability in batteries containing lithium metal anodes. However, because of its poor solubility LiNO3 is rarely utilized in the high-voltage window provided by carbonate electrolyte. Dissolution of LiNO3 in carbonate electrolyte is realized through an effective solvation regulation strategy. LiNO3 can be directly dissolved in an ethylene carbonate/diethyl carbonate electrolyte mixture by adding trace amounts of copper fluoride as a dissolution promoter. LiNO3 protects the Li metal anode in a working high-voltage Li metal battery. When a LiNi0.80 Co0.15 Al0.05 O2 cathode is paired with a Li metal anode, an extraordinary capacity retention of 53 % is achieved after 300 cycles (13 % after 200 cycles for LiNO3 -free electrolyte) and a very high average Coulombic efficiency above 99.5 % is achieved at 0.5 C. The solvation chemistry of LiNO3 -containing carbonate electrolyte may sustain high-voltage Li metal anodes operating in corrosive carbonate electrolytes. The lithium metal anode is regarded as a promising candidate in next‐generation energy storage devices. Lithium nitrate (LiNO3) is widely applied as an effective additive in ether electrolyte to increase the interfacial stability in batteries containing lithium metal anodes. However, because of its poor solubility LiNO3 is rarely utilized in the high‐voltage window provided by carbonate electrolyte. Dissolution of LiNO3 in carbonate electrolyte is realized through an effective solvation regulation strategy. LiNO3 can be directly dissolved in an ethylene carbonate/diethyl carbonate electrolyte mixture by adding trace amounts of copper fluoride as a dissolution promoter. LiNO3 protects the Li metal anode in a working high‐voltage Li metal battery. When a LiNi0.80Co0.15Al0.05O2 cathode is paired with a Li metal anode, an extraordinary capacity retention of 53 % is achieved after 300 cycles (13 % after 200 cycles for LiNO3‐free electrolyte) and a very high average Coulombic efficiency above 99.5 % is achieved at 0.5 C. The solvation chemistry of LiNO3‐containing carbonate electrolyte may sustain high‐voltage Li metal anodes operating in corrosive carbonate electrolytes. |
| Author | Huang, Jia‐Qi Yao, Yu‐Xing Zhang, Qiang Cheng, Xin‐Bing Zhang, Xue‐Qiang Yan, Chong Chen, Xiang |
| Author_xml | – sequence: 1 givenname: Chong orcidid: 0000-0001-9521-4981 surname: Yan fullname: Yan, Chong organization: Beijing Institute of Technology – sequence: 2 givenname: Yu‐Xing orcidid: 0000-0001-6350-1206 surname: Yao fullname: Yao, Yu‐Xing organization: Tsinghua University – sequence: 3 givenname: Xiang orcidid: 0000-0002-7686-6308 surname: Chen fullname: Chen, Xiang organization: Tsinghua University – sequence: 4 givenname: Xin‐Bing orcidid: 0000-0001-7567-1210 surname: Cheng fullname: Cheng, Xin‐Bing organization: Tsinghua University – sequence: 5 givenname: Xue‐Qiang orcidid: 0000-0003-2856-1881 surname: Zhang fullname: Zhang, Xue‐Qiang organization: Tsinghua University – sequence: 6 givenname: Jia‐Qi orcidid: 0000-0001-7394-9186 surname: Huang fullname: Huang, Jia‐Qi email: jqhuang@bit.edu.cn organization: Beijing Institute of Technology – sequence: 7 givenname: Qiang orcidid: 0000-0002-3929-1541 surname: Zhang fullname: Zhang, Qiang organization: Tsinghua University |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/30094909$$D View this record in MEDLINE/PubMed |
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| Keywords | lithium nitrate lithium deposition electrolyte additives lithium anodes high-voltage cathodes |
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| Snippet | The lithium metal anode is regarded as a promising candidate in next‐generation energy storage devices. Lithium nitrate (LiNO3) is widely applied as an... The lithium metal anode is regarded as a promising candidate in next‐generation energy storage devices. Lithium nitrate (LiNO 3 ) is widely applied as an... The lithium metal anode is regarded as a promising candidate in next-generation energy storage devices. Lithium nitrate (LiNO ) is widely applied as an... The lithium metal anode is regarded as a promising candidate in next-generation energy storage devices. Lithium nitrate (LiNO3 ) is widely applied as an... |
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| SubjectTerms | Anodes Anodic dissolution Anodic protection Batteries Copper fluorides Dissolution Electric potential electrolyte additives Electrolytes Energy storage Fluorides high-voltage cathodes Interface stability Lithium lithium anodes Lithium batteries lithium deposition lithium nitrate Metals Organic chemistry Solvation Voltage |
| Title | Lithium Nitrate Solvation Chemistry in Carbonate Electrolyte Sustains High‐Voltage Lithium Metal Batteries |
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