Activating Inert Metallic Compounds for High‐Rate Lithium–Sulfur Batteries Through In Situ Etching of Extrinsic Metal
Surface reactions constitute the foundation of various energy conversion/storage technologies, such as the lithium–sulfur (Li‐S) batteries. To expedite surface reactions for high‐rate battery applications demands in‐depth understanding of reaction kinetics and rational catalyst design. Now an in sit...
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| Published in | Angewandte Chemie International Edition Vol. 58; no. 12; pp. 3779 - 3783 |
|---|---|
| Main Authors | , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Germany
Wiley Subscription Services, Inc
18.03.2019
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| Edition | International ed. in English |
| Subjects | |
| Online Access | Get full text |
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| Abstract | Surface reactions constitute the foundation of various energy conversion/storage technologies, such as the lithium–sulfur (Li‐S) batteries. To expedite surface reactions for high‐rate battery applications demands in‐depth understanding of reaction kinetics and rational catalyst design. Now an in situ extrinsic‐metal etching strategy is used to activate an inert monometal nitride of hexagonal Ni3N through iron‐incorporated cubic Ni3FeN. In situ etched Ni3FeN regulates polysulfide‐involving surface reactions at high rates. Electron microscopy was used to unveil the mechanism of in situ catalyst transformation. The Li‐S batteries modified with Ni3FeN exhibited superb rate capability, remarkable cycling stability at a high sulfur loading of 4.8 mg cm−2, and lean‐electrolyte operability. This work opens up the exploration of multimetallic alloys and compounds as kinetic regulators for high‐rate Li‐S batteries and also elucidates catalytic surface reactions and the role of defect chemistry.
Inert hexagonal Ni3N can be activated by an extrinsic metal‐incorporating strategy with in situ etching that uses cubic Ni3FeN. Vacancy‐rich Ni3FeN catalysts kinetically regulate polysulfide‐involving reactions at high rates for use in advanced lithium–sulfur batteries. |
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| AbstractList | Surface reactions constitute the foundation of various energy conversion/storage technologies, such as the lithium–sulfur (Li‐S) batteries. To expedite surface reactions for high‐rate battery applications demands in‐depth understanding of reaction kinetics and rational catalyst design. Now an in situ extrinsic‐metal etching strategy is used to activate an inert monometal nitride of hexagonal Ni
3
N through iron‐incorporated cubic Ni
3
FeN. In situ etched Ni
3
FeN regulates polysulfide‐involving surface reactions at high rates. Electron microscopy was used to unveil the mechanism of in situ catalyst transformation. The Li‐S batteries modified with Ni
3
FeN exhibited superb rate capability, remarkable cycling stability at a high sulfur loading of 4.8 mg cm
−2
, and lean‐electrolyte operability. This work opens up the exploration of multimetallic alloys and compounds as kinetic regulators for high‐rate Li‐S batteries and also elucidates catalytic surface reactions and the role of defect chemistry. Surface reactions constitute the foundation of various energy conversion/storage technologies, such as the lithium–sulfur (Li‐S) batteries. To expedite surface reactions for high‐rate battery applications demands in‐depth understanding of reaction kinetics and rational catalyst design. Now an in situ extrinsic‐metal etching strategy is used to activate an inert monometal nitride of hexagonal Ni3N through iron‐incorporated cubic Ni3FeN. In situ etched Ni3FeN regulates polysulfide‐involving surface reactions at high rates. Electron microscopy was used to unveil the mechanism of in situ catalyst transformation. The Li‐S batteries modified with Ni3FeN exhibited superb rate capability, remarkable cycling stability at a high sulfur loading of 4.8 mg cm−2, and lean‐electrolyte operability. This work opens up the exploration of multimetallic alloys and compounds as kinetic regulators for high‐rate Li‐S batteries and also elucidates catalytic surface reactions and the role of defect chemistry. Surface reactions constitute the foundation of various energy conversion/storage technologies, such as the lithium-sulfur (Li-S) batteries. To expedite surface reactions for high-rate battery applications demands in-depth understanding of reaction kinetics and rational catalyst design. Now an in situ extrinsic-metal etching strategy is used to activate an inert monometal nitride of hexagonal Ni N through iron-incorporated cubic Ni FeN. In situ etched Ni FeN regulates polysulfide-involving surface reactions at high rates. Electron microscopy was used to unveil the mechanism of in situ catalyst transformation. The Li-S batteries modified with Ni FeN exhibited superb rate capability, remarkable cycling stability at a high sulfur loading of 4.8 mg cm , and lean-electrolyte operability. This work opens up the exploration of multimetallic alloys and compounds as kinetic regulators for high-rate Li-S batteries and also elucidates catalytic surface reactions and the role of defect chemistry. Surface reactions constitute the foundation of various energy conversion/storage technologies, such as the lithium–sulfur (Li‐S) batteries. To expedite surface reactions for high‐rate battery applications demands in‐depth understanding of reaction kinetics and rational catalyst design. Now an in situ extrinsic‐metal etching strategy is used to activate an inert monometal nitride of hexagonal Ni3N through iron‐incorporated cubic Ni3FeN. In situ etched Ni3FeN regulates polysulfide‐involving surface reactions at high rates. Electron microscopy was used to unveil the mechanism of in situ catalyst transformation. The Li‐S batteries modified with Ni3FeN exhibited superb rate capability, remarkable cycling stability at a high sulfur loading of 4.8 mg cm−2, and lean‐electrolyte operability. This work opens up the exploration of multimetallic alloys and compounds as kinetic regulators for high‐rate Li‐S batteries and also elucidates catalytic surface reactions and the role of defect chemistry. Inert hexagonal Ni3N can be activated by an extrinsic metal‐incorporating strategy with in situ etching that uses cubic Ni3FeN. Vacancy‐rich Ni3FeN catalysts kinetically regulate polysulfide‐involving reactions at high rates for use in advanced lithium–sulfur batteries. Surface reactions constitute the foundation of various energy conversion/storage technologies, such as the lithium-sulfur (Li-S) batteries. To expedite surface reactions for high-rate battery applications demands in-depth understanding of reaction kinetics and rational catalyst design. Now an in situ extrinsic-metal etching strategy is used to activate an inert monometal nitride of hexagonal Ni3 N through iron-incorporated cubic Ni3 FeN. In situ etched Ni3 FeN regulates polysulfide-involving surface reactions at high rates. Electron microscopy was used to unveil the mechanism of in situ catalyst transformation. The Li-S batteries modified with Ni3 FeN exhibited superb rate capability, remarkable cycling stability at a high sulfur loading of 4.8 mg cm-2 , and lean-electrolyte operability. This work opens up the exploration of multimetallic alloys and compounds as kinetic regulators for high-rate Li-S batteries and also elucidates catalytic surface reactions and the role of defect chemistry.Surface reactions constitute the foundation of various energy conversion/storage technologies, such as the lithium-sulfur (Li-S) batteries. To expedite surface reactions for high-rate battery applications demands in-depth understanding of reaction kinetics and rational catalyst design. Now an in situ extrinsic-metal etching strategy is used to activate an inert monometal nitride of hexagonal Ni3 N through iron-incorporated cubic Ni3 FeN. In situ etched Ni3 FeN regulates polysulfide-involving surface reactions at high rates. Electron microscopy was used to unveil the mechanism of in situ catalyst transformation. The Li-S batteries modified with Ni3 FeN exhibited superb rate capability, remarkable cycling stability at a high sulfur loading of 4.8 mg cm-2 , and lean-electrolyte operability. This work opens up the exploration of multimetallic alloys and compounds as kinetic regulators for high-rate Li-S batteries and also elucidates catalytic surface reactions and the role of defect chemistry. |
| Author | Zhao, Meng Huang, Jia‐Qi Zhang, Ze‐Wen Zhang, Qiang Wei, Jun‐Yu Li, Bo‐Quan Chen, Xiao Peng, Hong‐Jie Xie, Jin Chen, Xiang |
| Author_xml | – sequence: 1 givenname: Meng orcidid: 0000-0001-8402-7697 surname: Zhao fullname: Zhao, Meng organization: Beijing Institute of Technology – sequence: 2 givenname: Hong‐Jie orcidid: 0000-0002-4183-703X surname: Peng fullname: Peng, Hong‐Jie organization: Tsinghua University – sequence: 3 givenname: Ze‐Wen orcidid: 0000-0002-4909-4330 surname: Zhang fullname: Zhang, Ze‐Wen organization: Tsinghua University – sequence: 4 givenname: Bo‐Quan orcidid: 0000-0002-9544-5795 surname: Li fullname: Li, Bo‐Quan organization: Tsinghua University – sequence: 5 givenname: Xiao orcidid: 0000-0003-1104-6146 surname: Chen fullname: Chen, Xiao organization: Tsinghua University – sequence: 6 givenname: Jin orcidid: 0000-0002-4235-7441 surname: Xie fullname: Xie, Jin organization: Tsinghua University – sequence: 7 givenname: Xiang orcidid: 0000-0002-7686-6308 surname: Chen fullname: Chen, Xiang organization: Tsinghua University – sequence: 8 givenname: Jun‐Yu orcidid: 0000-0001-5775-3589 surname: Wei fullname: Wei, Jun‐Yu organization: Beijing Institute of Technology – sequence: 9 givenname: Qiang orcidid: 0000-0002-3929-1541 surname: Zhang fullname: Zhang, Qiang organization: Tsinghua University – sequence: 10 givenname: Jia‐Qi orcidid: 0000-0001-7394-9186 surname: Huang fullname: Huang, Jia‐Qi email: jqhuang@bit.edu.cn organization: Beijing Institute of Technology |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/30548388$$D View this record in MEDLINE/PubMed |
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| SubjectTerms | Catalysis Catalysts electrocatalysis Electron microscopy Energy conversion Energy storage Etching Lithium Lithium sulfur batteries Metal compounds metal nitrides Metal surfaces Organic chemistry polysulfide redox reaction Reaction kinetics Regulators separators Storage batteries Sulfur Surface reactions |
| Title | Activating Inert Metallic Compounds for High‐Rate Lithium–Sulfur Batteries Through In Situ Etching of Extrinsic Metal |
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