Triptycene‐based Chiral Porous Polyimides for Enantioselective Membrane Separation

Enantiomers of 2, 6‐diaminotriptycene (R, R‐1 and S, S‐1) are split by chiral‐phase HPLC and their absolute configurations are identified by single‐crystal X‐ray diffraction technology. Using the enantiomers as monomers, a couple of chiral porous polyimides (R‐FTPI and S‐FTPI) are prepared by polyco...

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Published inAngewandte Chemie International Edition Vol. 60; no. 23; pp. 12781 - 12785
Main Authors Zhang, Qing‐Pu, Wang, Zhen, Zhang, Zhe‐Wen, Zhai, Tian‐Long, Chen, Jing‐Jing, Ma, Hui, Tan, Bien, Zhang, Chun
Format Journal Article
LanguageEnglish
Published Germany Wiley Subscription Services, Inc 01.06.2021
EditionInternational ed. in English
Subjects
chiral microporous polymers
enantioelective separation
Enantiomers
High-performance liquid chromatography
Liquid chromatography
Membrane separation
membranes
Monomers
Organic solvents
Polycondensation reactions
Polyimide resins
Selectivity
Separation
Surface stability
triptycene
membranes
enantioelective separation
chiral microporous polymers
triptycene
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Abstract Enantiomers of 2, 6‐diaminotriptycene (R, R‐1 and S, S‐1) are split by chiral‐phase HPLC and their absolute configurations are identified by single‐crystal X‐ray diffraction technology. Using the enantiomers as monomers, a couple of chiral porous polyimides (R‐FTPI and S‐FTPI) are prepared by polycondensation reactions and display good heat stability, high BET surface area and good solubility in organic solvents. Moreover, both of R‐FTPI and S‐FTPI can be cast into robust, free‐standing films suitable for enantioselective separation with symmetrical chiral selectivity. Chiral porous polyimides (FTPI) were synthesized using monomers of chiral 2,6‐diaminotriptycene. The absolute configurations were identified by single‐crystal X‐ray diffraction. The obtained R‐FTPI and S‐FTPI can be cast into robust, free‐standing films suitable for enantioselective separation with high permeation rates.
AbstractList Enantiomers of 2, 6-diaminotriptycene (R, R-1 and S, S-1) are split by chiral-phase HPLC and their absolute configurations are identified by single-crystal X-ray diffraction technology. Using the enantiomers as monomers, a couple of chiral porous polyimides (R-FTPI and S-FTPI) are prepared by polycondensation reactions and display good heat stability, high BET surface area and good solubility in organic solvents. Moreover, both of R-FTPI and S-FTPI can be cast into robust, free-standing films suitable for enantioselective separation with symmetrical chiral selectivity.Enantiomers of 2, 6-diaminotriptycene (R, R-1 and S, S-1) are split by chiral-phase HPLC and their absolute configurations are identified by single-crystal X-ray diffraction technology. Using the enantiomers as monomers, a couple of chiral porous polyimides (R-FTPI and S-FTPI) are prepared by polycondensation reactions and display good heat stability, high BET surface area and good solubility in organic solvents. Moreover, both of R-FTPI and S-FTPI can be cast into robust, free-standing films suitable for enantioselective separation with symmetrical chiral selectivity.
Enantiomers of 2, 6-diaminotriptycene (R, R-1 and S, S-1) are split by chiral-phase HPLC and their absolute configurations are identified by single-crystal X-ray diffraction technology. Using the enantiomers as monomers, a couple of chiral porous polyimides (R-FTPI and S-FTPI) are prepared by polycondensation reactions and display good heat stability, high BET surface area and good solubility in organic solvents. Moreover, both of R-FTPI and S-FTPI can be cast into robust, free-standing films suitable for enantioselective separation with symmetrical chiral selectivity.
Enantiomers of 2, 6‐diaminotriptycene (R, R‐1 and S, S‐1) are split by chiral‐phase HPLC and their absolute configurations are identified by single‐crystal X‐ray diffraction technology. Using the enantiomers as monomers, a couple of chiral porous polyimides (R‐FTPI and S‐FTPI) are prepared by polycondensation reactions and display good heat stability, high BET surface area and good solubility in organic solvents. Moreover, both of R‐FTPI and S‐FTPI can be cast into robust, free‐standing films suitable for enantioselective separation with symmetrical chiral selectivity. Chiral porous polyimides (FTPI) were synthesized using monomers of chiral 2,6‐diaminotriptycene. The absolute configurations were identified by single‐crystal X‐ray diffraction. The obtained R‐FTPI and S‐FTPI can be cast into robust, free‐standing films suitable for enantioselective separation with high permeation rates.
Enantiomers of 2, 6‐diaminotriptycene (R, R‐ 1 and S, S‐ 1 ) are split by chiral‐phase HPLC and their absolute configurations are identified by single‐crystal X‐ray diffraction technology. Using the enantiomers as monomers, a couple of chiral porous polyimides (R‐FTPI and S‐FTPI) are prepared by polycondensation reactions and display good heat stability, high BET surface area and good solubility in organic solvents. Moreover, both of R‐FTPI and S‐FTPI can be cast into robust, free‐standing films suitable for enantioselective separation with symmetrical chiral selectivity.
Author Zhai, Tian‐Long
Ma, Hui
Wang, Zhen
Zhang, Chun
Zhang, Qing‐Pu
Chen, Jing‐Jing
Zhang, Zhe‐Wen
Tan, Bien
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  organization: Huazhong University of Science and Technology
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  surname: Zhang
  fullname: Zhang, Chun
  email: chunzhang@hust.edu.cn
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Keywords membranes
enantioelective separation
chiral microporous polymers
triptycene
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Snippet Enantiomers of 2, 6‐diaminotriptycene (R, R‐1 and S, S‐1) are split by chiral‐phase HPLC and their absolute configurations are identified by single‐crystal...
Enantiomers of 2, 6‐diaminotriptycene (R, R‐ 1 and S, S‐ 1 ) are split by chiral‐phase HPLC and their absolute configurations are identified by single‐crystal...
Enantiomers of 2, 6-diaminotriptycene (R, R-1 and S, S-1) are split by chiral-phase HPLC and their absolute configurations are identified by single-crystal...
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SubjectTerms chiral microporous polymers
enantioelective separation
Enantiomers
High-performance liquid chromatography
Liquid chromatography
Membrane separation
membranes
Monomers
Organic solvents
Polycondensation reactions
Polyimide resins
Selectivity
Separation
Surface stability
triptycene
Title Triptycene‐based Chiral Porous Polyimides for Enantioselective Membrane Separation
URI https://onlinelibrary.wiley.com/doi/abs/10.1002%2Fanie.202102350
https://www.ncbi.nlm.nih.gov/pubmed/33792135
https://www.proquest.com/docview/2532084978
https://www.proquest.com/docview/2507733897
Volume 60
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