Molecular sieving of ethylene from ethane using a rigid metal–organic framework
There are great challenges in developing efficient adsorbents to replace the currently used and energy-intensive cryogenic distillation processes for olefin/paraffin separation, owing to the similar physical properties of the two molecules. Here we report an ultramicroporous metal–organic framework...
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| Published in | Nature materials Vol. 17; no. 12; pp. 1128 - 1133 |
|---|---|
| Main Authors | , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
London
Nature Publishing Group UK
01.12.2018
Nature Publishing Group |
| Subjects | |
| Online Access | Get full text |
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| Abstract | There are great challenges in developing efficient adsorbents to replace the currently used and energy-intensive cryogenic distillation processes for olefin/paraffin separation, owing to the similar physical properties of the two molecules. Here we report an ultramicroporous metal–organic framework [Ca(C
4
O
4
)(H
2
O)], synthesized from calcium nitrate and squaric acid, that possesses rigid one-dimensional channels. These apertures are of a similar size to ethylene molecules, but owing to the size, shape and rigidity of the pores, act as molecular sieves to prevent the transport of ethane. The efficiency of this molecular sieve for the separation of ethylene/ethane mixtures is validated by breakthrough experiments with high ethylene productivity under ambient conditions. This material can be easily synthesized at the kilogram scale using an environmentally friendly method and is water-stable, which is important for potential industrial implementation. The strategy of using highly rigid metal–organic frameworks with well defined and rigid pores could also be extended to other porous materials for chemical separation processes.
Separating ethylene from ethane is highly challenging as they have very similar physical properties. Here, a metal–organic framework is reported that, owing to its pore size and rigidity, adsorbs ethylene but almost completely excludes ethane under ambient conditions. |
|---|---|
| AbstractList | There are great challenges in developing efficient adsorbents to replace the currently used and energy-intensive cryogenic distillation processes for olefin/paraffin separation, owing to the similar physical properties of the two molecules. Here we report an ultramicroporous metal–organic framework [Ca(C4O4)(H2O)], synthesized from calcium nitrate and squaric acid, that possesses rigid one-dimensional channels. These apertures are of a similar size to ethylene molecules, but owing to the size, shape and rigidity of the pores, act as molecular sieves to prevent the transport of ethane. The efficiency of this molecular sieve for the separation of ethylene/ethane mixtures is validated by breakthrough experiments with high ethylene productivity under ambient conditions. This material can be easily synthesized at the kilogram scale using an environmentally friendly method and is water-stable, which is important for potential industrial implementation. The strategy of using highly rigid metal–organic frameworks with well defined and rigid pores could also be extended to other porous materials for chemical separation processes. There are great challenges in developing efficient adsorbents to replace the currently used and energy-intensive cryogenic distillation processes for olefin/paraffin separation, owing to the similar physical properties of the two molecules. Here we report an ultramicroporous metal–organic framework [Ca(C 4 O 4 )(H 2 O)], synthesized from calcium nitrate and squaric acid, that possesses rigid one-dimensional channels. These apertures are of a similar size to ethylene molecules, but owing to the size, shape and rigidity of the pores, act as molecular sieves to prevent the transport of ethane. The efficiency of this molecular sieve for the separation of ethylene/ethane mixtures is validated by breakthrough experiments with high ethylene productivity under ambient conditions. This material can be easily synthesized at the kilogram scale using an environmentally friendly method and is water-stable, which is important for potential industrial implementation. The strategy of using highly rigid metal–organic frameworks with well defined and rigid pores could also be extended to other porous materials for chemical separation processes. Separating ethylene from ethane is highly challenging as they have very similar physical properties. Here, a metal–organic framework is reported that, owing to its pore size and rigidity, adsorbs ethylene but almost completely excludes ethane under ambient conditions. There are great challenges in developing efficient adsorbents to replace the currently used and energy-intensive cryogenic distillation processes for olefin/paraffin separation, owing to the similar physical properties of the two molecules. Here we report an ultramicroporous metal-organic framework [Ca(C4O4)(H2O)], synthesized from calcium nitrate and squaric acid, that possesses rigid one-dimensional channels. These apertures are of a similar size to ethylene molecules, but owing to the size, shape and rigidity of the pores, act as molecular sieves to prevent the transport of ethane. The efficiency of this molecular sieve for the separation of ethylene/ethane mixtures is validated by breakthrough experiments with high ethylene productivity under ambient conditions. This material can be easily synthesized at the kilogram scale using an environmentally friendly method and is water-stable, which is important for potential industrial implementation. The strategy of using highly rigid metal-organic frameworks with well defined and rigid pores could also be extended to other porous materials for chemical separation processes.There are great challenges in developing efficient adsorbents to replace the currently used and energy-intensive cryogenic distillation processes for olefin/paraffin separation, owing to the similar physical properties of the two molecules. Here we report an ultramicroporous metal-organic framework [Ca(C4O4)(H2O)], synthesized from calcium nitrate and squaric acid, that possesses rigid one-dimensional channels. These apertures are of a similar size to ethylene molecules, but owing to the size, shape and rigidity of the pores, act as molecular sieves to prevent the transport of ethane. The efficiency of this molecular sieve for the separation of ethylene/ethane mixtures is validated by breakthrough experiments with high ethylene productivity under ambient conditions. This material can be easily synthesized at the kilogram scale using an environmentally friendly method and is water-stable, which is important for potential industrial implementation. The strategy of using highly rigid metal-organic frameworks with well defined and rigid pores could also be extended to other porous materials for chemical separation processes. There are great challenges in developing efficient adsorbents to replace the currently used and energy-intensive cryogenic distillation processes for olefin/paraffin separation, owing to the similar physical properties of the two molecules. Here we report an ultramicroporous metal-organic framework [Ca(C O )(H O)], synthesized from calcium nitrate and squaric acid, that possesses rigid one-dimensional channels. These apertures are of a similar size to ethylene molecules, but owing to the size, shape and rigidity of the pores, act as molecular sieves to prevent the transport of ethane. The efficiency of this molecular sieve for the separation of ethylene/ethane mixtures is validated by breakthrough experiments with high ethylene productivity under ambient conditions. This material can be easily synthesized at the kilogram scale using an environmentally friendly method and is water-stable, which is important for potential industrial implementation. The strategy of using highly rigid metal-organic frameworks with well defined and rigid pores could also be extended to other porous materials for chemical separation processes. |
| Author | Chen, Banglin He, Chaohui Lin, Rui-Biao Krishna, Rajamani Li, Libo Li, Shun Li, Jinping Wu, Hui Zhou, Wei Zhou, Hao-Long |
| Author_xml | – sequence: 1 givenname: Rui-Biao surname: Lin fullname: Lin, Rui-Biao organization: Department of Chemistry, University of Texas at San Antonio – sequence: 2 givenname: Libo surname: Li fullname: Li, Libo organization: Department of Chemistry, University of Texas at San Antonio, Research Institute of Special Chemicals, Taiyuan University of Technology – sequence: 3 givenname: Hao-Long orcidid: 0000-0002-5007-6535 surname: Zhou fullname: Zhou, Hao-Long organization: School of Physical Science and Technology, ShanghaiTech University – sequence: 4 givenname: Hui orcidid: 0000-0003-0296-5204 surname: Wu fullname: Wu, Hui organization: NIST Center for Neutron Research, National Institute of Standards and Technology – sequence: 5 givenname: Chaohui surname: He fullname: He, Chaohui organization: Research Institute of Special Chemicals, Taiyuan University of Technology – sequence: 6 givenname: Shun surname: Li fullname: Li, Shun organization: Research Institute of Special Chemicals, Taiyuan University of Technology – sequence: 7 givenname: Rajamani orcidid: 0000-0002-4784-8530 surname: Krishna fullname: Krishna, Rajamani organization: Van’t Hoff Institute for Molecular Sciences, University of Amsterdam – sequence: 8 givenname: Jinping surname: Li fullname: Li, Jinping organization: Research Institute of Special Chemicals, Taiyuan University of Technology – sequence: 9 givenname: Wei orcidid: 0000-0002-5461-3617 surname: Zhou fullname: Zhou, Wei email: wzhou@nist.gov organization: NIST Center for Neutron Research, National Institute of Standards and Technology – sequence: 10 givenname: Banglin orcidid: 0000-0001-8707-8115 surname: Chen fullname: Chen, Banglin email: banglin.chen@utsa.edu organization: Department of Chemistry, University of Texas at San Antonio |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/30397312$$D View this record in MEDLINE/PubMed |
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| SubjectTerms | 639/301 639/301/299/1013 639/301/299/921 639/638 Apertures Biomaterials Calcium nitrate Chemical separation Chemistry and Materials Science Condensed Matter Physics Distillation Ethane Ethylene Materials Science Metal-organic frameworks Molecular sieves Nanotechnology Optical and Electronic Materials Organic chemistry Paraffins Physical properties Pores Porous materials Rigidity Separation processes Synthesis |
| Title | Molecular sieving of ethylene from ethane using a rigid metal–organic framework |
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