X-ray peak profile analysis of solid-state sintered alumina doped zinc oxide ceramics by Williamson–Hall and size-strain plot methods
ZnO doped with different concentrations of Al2O3 (2, 4, 6, 8 and 10wt%) is prepared by conventional solid-state reaction method. X-ray diffraction results revealed that the samples were crystalline with a hexagonal wurtzite phase. As the concentration of alumina (Al2O3) increases in ZnO, the X-ray d...
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| Published in | Journal of Asian Ceramic Societies Vol. 5; no. 2; pp. 94 - 103 |
|---|---|
| Main Authors | , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
01.06.2017
Taylor & Francis Taylor & Francis Group |
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| Online Access | Get full text |
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| Abstract | ZnO doped with different concentrations of Al2O3 (2, 4, 6, 8 and 10wt%) is prepared by conventional solid-state reaction method. X-ray diffraction results revealed that the samples were crystalline with a hexagonal wurtzite phase. As the concentration of alumina (Al2O3) increases in ZnO, the X-ray diffraction peaks shifts towards higher angle. This shifting in peak position and decrease in intensity reflect that Al is successfully replaced Zn in ZnO matrix. X-ray peak broadening analysis was used to evaluate the crystallite size and lattice strain by the Williamson–Hall (W–H) method and size-strain plot (SSP) method. The physical parameters such as strain, stress, and energy density values were also calculated using W–H method with different models namely uniform deformation model, uniform stress deformation model and uniform deformation energy density model. The surface morphology and elemental analysis of the prepared samples were characterized by field emission scanning electron microscopy and energy dispersive spectra. |
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| AbstractList | ZnO doped with different concentrations of Al2O3 (2, 4, 6, 8 and 10wt%) is prepared by conventional solid-state reaction method. X-ray diffraction results revealed that the samples were crystalline with a hexagonal wurtzite phase. As the concentration of alumina (Al2O3) increases in ZnO, the X-ray diffraction peaks shifts towards higher angle. This shifting in peak position and decrease in intensity reflect that Al is successfully replaced Zn in ZnO matrix. X-ray peak broadening analysis was used to evaluate the crystallite size and lattice strain by the Williamson–Hall (W–H) method and size-strain plot (SSP) method. The physical parameters such as strain, stress, and energy density values were also calculated using W–H method with different models namely uniform deformation model, uniform stress deformation model and uniform deformation energy density model. The surface morphology and elemental analysis of the prepared samples were characterized by field emission scanning electron microscopy and energy dispersive spectra. ZnO doped with different concentrations of Al2O3 (2, 4, 6, 8 and 10 wt%) is prepared by conventional solid-state reaction method. X-ray diffraction results revealed that the samples were crystalline with a hexagonal wurtzite phase. As the concentration of alumina (Al2O3) increases in ZnO, the X-ray diffraction peaks shifts towards higher angle. This shifting in peak position and decrease in intensity reflect that Al is successfully replaced Zn in ZnO matrix. X-ray peak broadening analysis was used to evaluate the crystallite size and lattice strain by the Williamson–Hall (W–H) method and size-strain plot (SSP) method. The physical parameters such as strain, stress, and energy density values were also calculated using W–H method with different models namely uniform deformation model, uniform stress deformation model and uniform deformation energy density model. The surface morphology and elemental analysis of the prepared samples were characterized by field emission scanning electron microscopy and energy dispersive spectra. ZnO doped with different concentrations of Al 2 O 3 (2, 4, 6, 8 and 10 wt%) is prepared by conventional solid-state reaction method. X-ray diffraction results revealed that the samples were crystalline with a hexagonal wurtzite phase. As the concentration of alumina (Al 2 O 3 ) increases in ZnO, the X-ray diffraction peaks shifts towards higher angle. This shifting in peak position and decrease in intensity reflect that Al is successfully replaced Zn in ZnO matrix. X-ray peak broadening analysis was used to evaluate the crystallite size and lattice strain by the Williamson-Hall (W-H) method and size-strain plot (SSP) method. The physical parameters such as strain, stress, and energy density values were also calculated using W-H method with different models namely uniform deformation model, uniform stress deformation model and uniform deformation energy density model. The surface morphology and elemental analysis of the prepared samples were characterized by field emission scanning electron microscopy and energy dispersive spectra. |
| Author | Hymavathi, B. Rajesh Kumar, B. |
| Author_xml | – sequence: 1 givenname: B. surname: Rajesh Kumar fullname: Rajesh Kumar, B. email: rajphyind@gmail.com organization: Department of Physics, GITAM Institute of Technology, GITAM University, Visakhapatnam 530045, AP, India – sequence: 2 givenname: B. surname: Hymavathi fullname: Hymavathi, B. organization: Department of Physics, Anil Neerukonda Institute of Technology and Sciences (Autonomous), Sangivalasa, Visakhapatnam 531162, AP, India |
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| Snippet | ZnO doped with different concentrations of Al2O3 (2, 4, 6, 8 and 10wt%) is prepared by conventional solid-state reaction method. X-ray diffraction results... ZnO doped with different concentrations of Al 2 O 3 (2, 4, 6, 8 and 10 wt%) is prepared by conventional solid-state reaction method. X-ray diffraction results... ZnO doped with different concentrations of Al2O3 (2, 4, 6, 8 and 10 wt%) is prepared by conventional solid-state reaction method. X-ray diffraction results... |
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| StartPage | 94 |
| SubjectTerms | Scanning electron microscopy Solid-state reaction XRD |
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| Title | X-ray peak profile analysis of solid-state sintered alumina doped zinc oxide ceramics by Williamson–Hall and size-strain plot methods |
| URI | https://dx.doi.org/10.1016/j.jascer.2017.02.001 https://www.tandfonline.com/doi/abs/10.1016/j.jascer.2017.02.001 https://doaj.org/article/43aa10a32d874aecac8efad97e166387 |
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