Validation of QuEChERS-based method for determination of flusilazole residues in grape by high-performance liquid chromatography with photodiode array detector

• Published in: Toxicological and environmental chemistry Vol. 97; no. 9; pp. 1137 - 1144
• Main Authors: Malhat, Farag, Loutfy, Naglaa M., Ahmed, Mohamed Tawfic
• Format: Journal Article
• Language: English
• Published: Abingdon Taylor & Francis 21.10.2015; Taylor & Francis Ltd
• Subjects: Analytical chemistry; Arrays; Berries; Chromatography; Detectors; dissipation; Dosage; flusilazole; Food safety; Grapes; Health hazards; HPLC-DAD; Kinetics; Liquid chromatography; Mathematical analysis; Pesticides; Photodiodes; Residues; risk assessment; Vitaceae

A high-performance liquid chromatography with photodiode array detector analytical method was developed to determine the residue levels of flusilazole in grape and investigate the dissipation pattern and safety. The results showed that the mean recoveries were in the range of 86%-90%. Limits of dete...