A microwave irradiation-persulfate-formate system for achieving the detoxification and alkali-activated composite geopolymerization of the chromate-contaminated soil

A microwave (MA) irradiation-persulfate-formate system was constructed to detoxify Cr contamination and solidify the geopolymerization of the alkali-activated composite material. Three series of experiments were correspondingly conducted to evaluate the treatment for the chromate-contaminated soil....

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Published inEcotoxicology and environmental safety Vol. 217; p. 112233
Main Authors Huang, Tao, Zhou, Lulu, Cao, Zhenxing, Zhang, Shuwen, Liu, Longfei
Format Journal Article
LanguageEnglish
Published Netherlands Elsevier Inc 01.07.2021
Elsevier
Subjects
Alkali activation
Chromate-contaminated soil
Composite geopolymerization
Microwave irradiation
Persulfate
Microwave irradiation
Composite geopolymerization
Chromate-contaminated soil
Alkali activation
Persulfate
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Abstract A microwave (MA) irradiation-persulfate-formate system was constructed to detoxify Cr contamination and solidify the geopolymerization of the alkali-activated composite material. Three series of experiments were correspondingly conducted to evaluate the treatment for the chromate-contaminated soil. The changes in the molar ratios of formate to persulfate and the mass rates of fortifier to soil led to a significantly greater reduction of CrVI in the detoxification experiments. The increase of blast furnace slag from 50% to 80% in the composite cementitious materials (CCM) intensified the immobilization efficiencies of chromate and the compressive strengths of geopolymer blocks. MA irradiation potentially enhanced the binding of Ca cations to the aluminosilicate compounds. The degree of reaction in the phenomenological kinetics model mathematically verified the geopolymerization process. Ettringite was formed within the structure of the geopolymer in the coupling system. Sulfate radicals released from persulfate not only contributed to the detoxification process but also strengthened the immobilization process. [Display omitted] •A microwave irradiation-persulfate-formate system was constructed to solve drawbacks.•Sulfate radicals contributed to detoxification and participated in solidification.•The catalytic production of CO2•− and the reduction of CrVI to CrIII were confirmed.•The formation of ettringite induced by sulfate radical enhanced geopolymerization.•The study expands the application of radicals and MA irradiation on the geopolymers.
AbstractList A microwave (MA) irradiation-persulfate-formate system was constructed to detoxify Cr contamination and solidify the geopolymerization of the alkali-activated composite material. Three series of experiments were correspondingly conducted to evaluate the treatment for the chromate-contaminated soil. The changes in the molar ratios of formate to persulfate and the mass rates of fortifier to soil led to a significantly greater reduction of CrVI in the detoxification experiments. The increase of blast furnace slag from 50% to 80% in the composite cementitious materials (CCM) intensified the immobilization efficiencies of chromate and the compressive strengths of geopolymer blocks. MA irradiation potentially enhanced the binding of Ca cations to the aluminosilicate compounds. The degree of reaction in the phenomenological kinetics model mathematically verified the geopolymerization process. Ettringite was formed within the structure of the geopolymer in the coupling system. Sulfate radicals released from persulfate not only contributed to the detoxification process but also strengthened the immobilization process.
A microwave (MA) irradiation-persulfate-formate system was constructed to detoxify Cr contamination and solidify the geopolymerization of the alkali-activated composite material. Three series of experiments were correspondingly conducted to evaluate the treatment for the chromate-contaminated soil. The changes in the molar ratios of formate to persulfate and the mass rates of fortifier to soil led to a significantly greater reduction of CrVI in the detoxification experiments. The increase of blast furnace slag from 50% to 80% in the composite cementitious materials (CCM) intensified the immobilization efficiencies of chromate and the compressive strengths of geopolymer blocks. MA irradiation potentially enhanced the binding of Ca cations to the aluminosilicate compounds. The degree of reaction in the phenomenological kinetics model mathematically verified the geopolymerization process. Ettringite was formed within the structure of the geopolymer in the coupling system. Sulfate radicals released from persulfate not only contributed to the detoxification process but also strengthened the immobilization process.A microwave (MA) irradiation-persulfate-formate system was constructed to detoxify Cr contamination and solidify the geopolymerization of the alkali-activated composite material. Three series of experiments were correspondingly conducted to evaluate the treatment for the chromate-contaminated soil. The changes in the molar ratios of formate to persulfate and the mass rates of fortifier to soil led to a significantly greater reduction of CrVI in the detoxification experiments. The increase of blast furnace slag from 50% to 80% in the composite cementitious materials (CCM) intensified the immobilization efficiencies of chromate and the compressive strengths of geopolymer blocks. MA irradiation potentially enhanced the binding of Ca cations to the aluminosilicate compounds. The degree of reaction in the phenomenological kinetics model mathematically verified the geopolymerization process. Ettringite was formed within the structure of the geopolymer in the coupling system. Sulfate radicals released from persulfate not only contributed to the detoxification process but also strengthened the immobilization process.
A microwave (MA) irradiation-persulfate-formate system was constructed to detoxify Cr contamination and solidify the geopolymerization of the alkali-activated composite material. Three series of experiments were correspondingly conducted to evaluate the treatment for the chromate-contaminated soil. The changes in the molar ratios of formate to persulfate and the mass rates of fortifier to soil led to a significantly greater reduction of Cr in the detoxification experiments. The increase of blast furnace slag from 50% to 80% in the composite cementitious materials (CCM) intensified the immobilization efficiencies of chromate and the compressive strengths of geopolymer blocks. MA irradiation potentially enhanced the binding of Ca cations to the aluminosilicate compounds. The degree of reaction in the phenomenological kinetics model mathematically verified the geopolymerization process. Ettringite was formed within the structure of the geopolymer in the coupling system. Sulfate radicals released from persulfate not only contributed to the detoxification process but also strengthened the immobilization process.
A microwave (MA) irradiation-persulfate-formate system was constructed to detoxify Cr contamination and solidify the geopolymerization of the alkali-activated composite material. Three series of experiments were correspondingly conducted to evaluate the treatment for the chromate-contaminated soil. The changes in the molar ratios of formate to persulfate and the mass rates of fortifier to soil led to a significantly greater reduction of CrVI in the detoxification experiments. The increase of blast furnace slag from 50% to 80% in the composite cementitious materials (CCM) intensified the immobilization efficiencies of chromate and the compressive strengths of geopolymer blocks. MA irradiation potentially enhanced the binding of Ca cations to the aluminosilicate compounds. The degree of reaction in the phenomenological kinetics model mathematically verified the geopolymerization process. Ettringite was formed within the structure of the geopolymer in the coupling system. Sulfate radicals released from persulfate not only contributed to the detoxification process but also strengthened the immobilization process. [Display omitted] •A microwave irradiation-persulfate-formate system was constructed to solve drawbacks.•Sulfate radicals contributed to detoxification and participated in solidification.•The catalytic production of CO2•− and the reduction of CrVI to CrIII were confirmed.•The formation of ettringite induced by sulfate radical enhanced geopolymerization.•The study expands the application of radicals and MA irradiation on the geopolymers.
ArticleNumber 112233
Author Zhang, Shuwen
Cao, Zhenxing
Huang, Tao
Zhou, Lulu
Liu, Longfei
Author_xml – sequence: 1
  givenname: Tao
  surname: Huang
  fullname: Huang, Tao
  organization: School of Materials Engineering, Changshu Institute of Technology, 215500, China
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  givenname: Lulu
  surname: Zhou
  fullname: Zhou, Lulu
  email: luluzhou_work@163.com
  organization: School of Materials Engineering, Changshu Institute of Technology, 215500, China
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  givenname: Zhenxing
  surname: Cao
  fullname: Cao, Zhenxing
  organization: School of Materials Engineering, Changshu Institute of Technology, 215500, China
– sequence: 4
  givenname: Shuwen
  surname: Zhang
  fullname: Zhang, Shuwen
  organization: Nuclear Resources Engineering College, University of South China, 421001, China
– sequence: 5
  givenname: Longfei
  surname: Liu
  fullname: Liu, Longfei
  organization: School of Materials Engineering, Changshu Institute of Technology, 215500, China
BackLink https://www.ncbi.nlm.nih.gov/pubmed/33862430$$D View this record in MEDLINE/PubMed
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Keywords Microwave irradiation
Composite geopolymerization
Chromate-contaminated soil
Alkali activation
Persulfate
Language English
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Snippet A microwave (MA) irradiation-persulfate-formate system was constructed to detoxify Cr contamination and solidify the geopolymerization of the alkali-activated...
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StartPage 112233
SubjectTerms Alkali activation
Chromate-contaminated soil
Composite geopolymerization
Microwave irradiation
Persulfate
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Title A microwave irradiation-persulfate-formate system for achieving the detoxification and alkali-activated composite geopolymerization of the chromate-contaminated soil
URI https://dx.doi.org/10.1016/j.ecoenv.2021.112233
https://www.ncbi.nlm.nih.gov/pubmed/33862430
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