Thermal characterization of 3D printable multifunctional graphene‐reinforced polyethylene terephthalate glycol (PETG) composite filaments enabled for smart structural applications

The focus on fillers' influence in high‐performance polymer composites has undergone a transformation. Additionally, the utilization of additive manufacturing (AM) in this venture has aroused the curiosity of investigators to empirically enumerate the characteristics of such composites for nume...

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Published inPolymer engineering and science Vol. 63; no. 9; pp. 2841 - 2856
Main Authors Bedi, Surjeet Singh, Mallesha, Vasu, Mahesh, Vinyas, Mahesh, Vishwas, Mukunda, Sriram, Negi, Sushanth, Ponnusami, Sathiskumar Anusuya
Format Journal Article
LanguageEnglish
Published Hoboken, USA John Wiley & Sons, Inc 01.09.2023
Society of Plastics Engineers, Inc
Blackwell Publishing Ltd
Subjects
3D printing
differential scanning calorimetry
differential thermogravimetric
Filaments
Fourier transforms
fourier transform‐infrared spectroscopy
Glycols
Graphene
Graphite
Infrared analysis
Infrared spectroscopy
Polyethylene terephthalate
polyethylene terephthalate glycol
Polymer matrix composites
Polymeric composites
Production processes
Technology application
Thermodynamic properties
Thermogravimetric analysis
Three dimensional printing
India
Online AccessGet full text
ISSN0032-3888
1548-2634
DOI10.1002/pen.26409

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Abstract The focus on fillers' influence in high‐performance polymer composites has undergone a transformation. Additionally, the utilization of additive manufacturing (AM) in this venture has aroused the curiosity of investigators to empirically enumerate the characteristics of such composites for numerous applications. Consequently, this investigation aims to assess the thermal behavior of polyethylene terephthalate glycol (PETG) polymers reinforced with graphene flakes. As mentioned above, various weight ratios of the constituents are manufactured, blended, and extruded into six distinct varieties of 3D‐printable filaments utilizing a twin‐screw extruder. In accordance with the relevant American Society for Testing and Materials (ASTM) standards, we perform the thermal characterization of the compounded PETG/graphene pellets using Fourier transform‐infrared (FTIR) spectroscopy, thermogravimetric analysis (TGA), and differential scanning calorimetry (DSC). The results reveal that enhancing the concentration of graphene augments the thermal properties of the composites. Furthermore, the FTIR investigation contributes to graphene's proficiency in absorbing infrared radiation and curbing micro‐vibrations. Additionally, the study highlights the way in which chemical interactions between graphene and PETG impact the general effectiveness of the composites. Thermal characterization of PETG/graphene composites.
AbstractList The focus on fillers' influence in high‐performance polymer composites has undergone a transformation. Additionally, the utilization of additive manufacturing (AM) in this venture has aroused the curiosity of investigators to empirically enumerate the characteristics of such composites for numerous applications. Consequently, this investigation aims to assess the thermal behavior of polyethylene terephthalate glycol (PETG) polymers reinforced with graphene flakes. As mentioned above, various weight ratios of the constituents are manufactured, blended, and extruded into six distinct varieties of 3D‐printable filaments utilizing a twin‐screw extruder. In accordance with the relevant American Society for Testing and Materials (ASTM) standards, we perform the thermal characterization of the compounded PETG/graphene pellets using Fourier transform‐infrared (FTIR) spectroscopy, thermogravimetric analysis (TGA), and differential scanning calorimetry (DSC). The results reveal that enhancing the concentration of graphene augments the thermal properties of the composites. Furthermore, the FTIR investigation contributes to graphene's proficiency in absorbing infrared radiation and curbing micro‐vibrations. Additionally, the study highlights the way in which chemical interactions between graphene and PETG impact the general effectiveness of the composites.
The focus on fillers' influence in high‐performance polymer composites has undergone a transformation. Additionally, the utilization of additive manufacturing (AM) in this venture has aroused the curiosity of investigators to empirically enumerate the characteristics of such composites for numerous applications. Consequently, this investigation aims to assess the thermal behavior of polyethylene terephthalate glycol (PETG) polymers reinforced with graphene flakes. As mentioned above, various weight ratios of the constituents are manufactured, blended, and extruded into six distinct varieties of 3D‐printable filaments utilizing a twin‐screw extruder. In accordance with the relevant American Society for Testing and Materials (ASTM) standards, we perform the thermal characterization of the compounded PETG/graphene pellets using Fourier transform‐infrared (FTIR) spectroscopy, thermogravimetric analysis (TGA), and differential scanning calorimetry (DSC). The results reveal that enhancing the concentration of graphene augments the thermal properties of the composites. Furthermore, the FTIR investigation contributes to graphene's proficiency in absorbing infrared radiation and curbing micro‐vibrations. Additionally, the study highlights the way in which chemical interactions between graphene and PETG impact the general effectiveness of the composites. Thermal characterization of PETG/graphene composites.
Audience Academic
Author Ponnusami, Sathiskumar Anusuya
Mahesh, Vinyas
Mahesh, Vishwas
Mukunda, Sriram
Bedi, Surjeet Singh
Mallesha, Vasu
Negi, Sushanth
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Snippet The focus on fillers' influence in high‐performance polymer composites has undergone a transformation. Additionally, the utilization of additive manufacturing...
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SubjectTerms 3D printing
differential scanning calorimetry
differential thermogravimetric
Filaments
Fourier transforms
fourier transform‐infrared spectroscopy
Glycols
Graphene
Graphite
Infrared analysis
Infrared spectroscopy
Polyethylene terephthalate
polyethylene terephthalate glycol
Polymer matrix composites
Polymeric composites
Production processes
Technology application
Thermodynamic properties
Thermogravimetric analysis
Three dimensional printing
Title Thermal characterization of 3D printable multifunctional graphene‐reinforced polyethylene terephthalate glycol (PETG) composite filaments enabled for smart structural applications
URI https://onlinelibrary.wiley.com/doi/abs/10.1002%2Fpen.26409
https://www.proquest.com/docview/2862608415
Volume 63
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