Novel nanocrystalline PdNi alloy catalyst for methanol and ethanol electro-oxidation in alkaline media

► Nanocrystalline PdNi alloy can be fabricated by dealloying Al 75Pd 10Ni 15 precursor. ► PdNi alloy shows an enhanced catalytic activity towards alcohol electro-oxidation. ► The enhanced performance can be attributed to the alloying of Pd with Ni. Nanocrystalline Pd 40Ni 60 alloy catalyst has been...

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Published in	Journal of power sources Vol. 196; no. 14; pp. 5823 - 5828
Main Authors	Qi, Zhen, Geng, Haoran, Wang, Xiaoguang, Zhao, Changchun, Ji, Hong, Zhang, Chi, Xu, Junling, Zhang, Zhonghua
Format	Journal Article
Language	English
Published	Amsterdam Elsevier B.V 15.07.2011 Elsevier
Subjects	Alloy catalyst Applied sciences Catalysts Dealloying Direct alcohol fuel cells Direct energy conversion and energy accumulation Electrical engineering. Electrical power engineering Electrical power engineering Electro-oxidation Electrochemical conversion: primary and secondary batteries, fuel cells Energy Energy. Thermal use of fuels Equipments for energy generation and conversion: thermal, electrical, mechanical energy, etc Ethyl alcohol Exact sciences and technology Fuel cells Media Methyl alcohol Nanocrystals Nanoporous alloys Nanostructure Palladium Scanning electron microscopy Nanoporous alloys Alloy catalyst Dealloying Direct alcohol fuel cells Electro-oxidation Ethanol Alcohol fuel cells Nanoporous materials Oxidation Electrochemical reaction Catalyst Nanocrystal Methanol
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Abstract	► Nanocrystalline PdNi alloy can be fabricated by dealloying Al 75Pd 10Ni 15 precursor. ► PdNi alloy shows an enhanced catalytic activity towards alcohol electro-oxidation. ► The enhanced performance can be attributed to the alloying of Pd with Ni. Nanocrystalline Pd 40Ni 60 alloy catalyst has been fabricated by dealloying a ternary Al 75Pd 10Ni 15 alloy in a 20 wt.% NaOH aqueous solution under free corrosion conditions. The microstructure and catalytic performance of the catalyst have been characterized by X-ray diffraction, scanning electron microscopy, transmission electron microscopy, high-resolution transmission electron microscopy, and cyclic voltammetry. The Pd 40Ni 60 alloy consists of nanocrystals with sizes of 5–10 nm, and Pd/Ni elements exist in a solid solution form. Moreover, nanocrystalline zones, amorphous zones and lattice distortion can be observed in the Pd 40Ni 60 alloy. Electrochemical measurements demonstrate that, for equivalent mass Pd, Pd 40Ni 60 has an enhanced electrocatalytic performance towards methanol and ethanol oxidation in alkaline media than nanoporous Pd. The nanocrystalline Pd 40Ni 60 alloy is a promising catalyst towards alcohol oxidation in alkaline media for fuel cell applications.
AbstractList	► Nanocrystalline PdNi alloy can be fabricated by dealloying Al 75Pd 10Ni 15 precursor. ► PdNi alloy shows an enhanced catalytic activity towards alcohol electro-oxidation. ► The enhanced performance can be attributed to the alloying of Pd with Ni. Nanocrystalline Pd 40Ni 60 alloy catalyst has been fabricated by dealloying a ternary Al 75Pd 10Ni 15 alloy in a 20 wt.% NaOH aqueous solution under free corrosion conditions. The microstructure and catalytic performance of the catalyst have been characterized by X-ray diffraction, scanning electron microscopy, transmission electron microscopy, high-resolution transmission electron microscopy, and cyclic voltammetry. The Pd 40Ni 60 alloy consists of nanocrystals with sizes of 5–10 nm, and Pd/Ni elements exist in a solid solution form. Moreover, nanocrystalline zones, amorphous zones and lattice distortion can be observed in the Pd 40Ni 60 alloy. Electrochemical measurements demonstrate that, for equivalent mass Pd, Pd 40Ni 60 has an enhanced electrocatalytic performance towards methanol and ethanol oxidation in alkaline media than nanoporous Pd. The nanocrystalline Pd 40Ni 60 alloy is a promising catalyst towards alcohol oxidation in alkaline media for fuel cell applications. Nanocrystalline Pd sub(4)0Ni sub(60) alloy catalyst has been fabricated by dealloying a ternary Al sub(75)Pd sub(10)Ni sub(15) alloy in a 20 wt.% NaOH aqueous solution under free corrosion conditions. The microstructure and catalytic performance of the catalyst have been characterized by X-ray diffraction, scanning electron microscopy, transmission electron microscopy, high-resolution transmission electron microscopy, and cyclic voltammetry. The Pd sub(40)Ni sub(60) alloy consists of nanocrystals with sizes of 5-10 nm, and Pd/Ni elements exist in a solid solution form. Moreover, nanocrystalline zones, amorphous zones and lattice distortion can be observed in the Pd sub(40)Ni sub(60) alloy. Electrochemical measurements demonstrate that, for equivalent mass Pd, Pd sub(40)Ni sub(60) has an enhanced electrocatalytic performance towards methanol and ethanol oxidation in alkaline media than nanoporous Pd. The nanocrystalline Pd sub(40)Ni sub(60) alloy is a promising catalyst towards alcohol oxidation in alkaline media for fuel cell applications.
Author	Wang, Xiaoguang Qi, Zhen Xu, Junling Zhao, Changchun Zhang, Chi Zhang, Zhonghua Ji, Hong Geng, Haoran
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Snippet	► Nanocrystalline PdNi alloy can be fabricated by dealloying Al 75Pd 10Ni 15 precursor. ► PdNi alloy shows an enhanced catalytic activity towards alcohol... Nanocrystalline Pd sub(4)0Ni sub(60) alloy catalyst has been fabricated by dealloying a ternary Al sub(75)Pd sub(10)Ni sub(15) alloy in a 20 wt.% NaOH aqueous...
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SubjectTerms	Alloy catalyst Applied sciences Catalysts Dealloying Direct alcohol fuel cells Direct energy conversion and energy accumulation Electrical engineering. Electrical power engineering Electrical power engineering Electro-oxidation Electrochemical conversion: primary and secondary batteries, fuel cells Energy Energy. Thermal use of fuels Equipments for energy generation and conversion: thermal, electrical, mechanical energy, etc Ethyl alcohol Exact sciences and technology Fuel cells Media Methyl alcohol Nanocrystals Nanoporous alloys Nanostructure Palladium Scanning electron microscopy
Title	Novel nanocrystalline PdNi alloy catalyst for methanol and ethanol electro-oxidation in alkaline media
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