Elucidation of the effect of hybrid copper/selenium nanofiller on the optical, thermal, electrical, mechanical properties and antibacterial activity of polyvinyl alcohol/carboxymethyl cellulose blend
Polymer nanocomposite samples of a polyvinyl alcohol (PVA)/carboxymethyl cellulose (CMC) blend doped with copper nanoparticles and selenium nanoparticles (Cu NPs/Se NPs) were prepared by the casting method. X‐ray diffraction analysis (XRD) patterns showed an increase in the degree of amorphous natur...
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| Published in | Polymer engineering and science Vol. 63; no. 7; pp. 1974 - 1988 |
|---|---|
| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Hoboken, USA
John Wiley & Sons, Inc
01.07.2023
Society of Plastics Engineers, Inc Blackwell Publishing Ltd |
| Subjects | |
| Online Access | Get full text |
| ISSN | 0032-3888 1548-2634 |
| DOI | 10.1002/pen.26339 |
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| Abstract | Polymer nanocomposite samples of a polyvinyl alcohol (PVA)/carboxymethyl cellulose (CMC) blend doped with copper nanoparticles and selenium nanoparticles (Cu NPs/Se NPs) were prepared by the casting method. X‐ray diffraction analysis (XRD) patterns showed an increase in the degree of amorphous nature of the host polymeric matrix with increasing content of Cu/Se nanoparticles. The addition of 1.60 wt.%, Cu/Se NPs narrowed the indirect optical energy gap value of the nanocomposite from 3.97 to 2.39 eV. In addition, the differential scanning calorimetry (DSC) curve of the pure blend displays the miscibility of the blend components, confirmed by the presence of a single glass transition. Transmission electron microscopy (TEM) micrographs showed that the average sizes of Cu and Se nanoparticles are about 11 and 41 nm, respectively. The maximum values of AC and DC conductivity were 6.76 × 10−6 S.cm−1 and 5.49 × 10−10 for a PVA/CMC film filled with 1.60 wt.% of Cu‐Se NPs. The mechanical properties of the PVA/CMC blend improved after adding the hybrid NPs. Moreover, the antibacterial activity of the prepared samples was increased due to the filling of Cu‐Se nanoparticles to the films. Therefore, these results indicate the multifunctionality of PVA/CMC/Cu‐Se nanocomposite samples for use in electrical energy storage, solid‐polymer electrolytes, and food packaging industry.
Preparation and characterization of nanocomposite samples. |
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| AbstractList | Polymer nanocomposite samples of a polyvinyl alcohol (PVA)/carboxymethyl cellulose (CMC) blend doped with copper nanoparticles and selenium nanoparticles (Cu NPs/Se NPs) were prepared by the casting method. X‐ray diffraction analysis (XRD) patterns showed an increase in the degree of amorphous nature of the host polymeric matrix with increasing content of Cu/Se nanoparticles. The addition of 1.60 wt.%, Cu/Se NPs narrowed the indirect optical energy gap value of the nanocomposite from 3.97 to 2.39 eV. In addition, the differential scanning calorimetry (DSC) curve of the pure blend displays the miscibility of the blend components, confirmed by the presence of a single glass transition. Transmission electron microscopy (TEM) micrographs showed that the average sizes of Cu and Se nanoparticles are about 11 and 41 nm, respectively. The maximum values of AC and DC conductivity were 6.76 × 10−6 S.cm−1 and 5.49 × 10−10 for a PVA/CMC film filled with 1.60 wt.% of Cu‐Se NPs. The mechanical properties of the PVA/CMC blend improved after adding the hybrid NPs. Moreover, the antibacterial activity of the prepared samples was increased due to the filling of Cu‐Se nanoparticles to the films. Therefore, these results indicate the multifunctionality of PVA/CMC/Cu‐Se nanocomposite samples for use in electrical energy storage, solid‐polymer electrolytes, and food packaging industry.
Preparation and characterization of nanocomposite samples. Polymer nanocomposite samples of a polyvinyl alcohol (PVA)/carboxymethyl cellulose (CMC) blend doped with copper nanoparticles and selenium nanoparticles (Cu NPs/Se NPs) were prepared by the casting method. X‐ray diffraction analysis (XRD) patterns showed an increase in the degree of amorphous nature of the host polymeric matrix with increasing content of Cu/Se nanoparticles. The addition of 1.60 wt.%, Cu/Se NPs narrowed the indirect optical energy gap value of the nanocomposite from 3.97 to 2.39 eV. In addition, the differential scanning calorimetry (DSC) curve of the pure blend displays the miscibility of the blend components, confirmed by the presence of a single glass transition. Transmission electron microscopy (TEM) micrographs showed that the average sizes of Cu and Se nanoparticles are about 11 and 41 nm, respectively. The maximum values of AC and DC conductivity were 6.76 × 10−6 S.cm−1 and 5.49 × 10−10 for a PVA/CMC film filled with 1.60 wt.% of Cu‐Se NPs. The mechanical properties of the PVA/CMC blend improved after adding the hybrid NPs. Moreover, the antibacterial activity of the prepared samples was increased due to the filling of Cu‐Se nanoparticles to the films. Therefore, these results indicate the multifunctionality of PVA/CMC/Cu‐Se nanocomposite samples for use in electrical energy storage, solid‐polymer electrolytes, and food packaging industry. Polymer nanocomposite samples of a polyvinyl alcohol (PVA)/carboxymethyl cellulose (CMC) blend doped with copper nanoparticles and selenium nanoparticles (Cu NPs/Se NPs) were prepared by the casting method. X-ray diffraction analysis (XRD) patterns showed an increase in the degree of amorphous nature of the host polymeric matrix with increasing content of Cu/Se nanoparticles. The addition of 1.60 wt.%, Cu/Se NPs narrowed the indirect optical energy gap value of the nanocomposite from 3.97 to 2.39 eV. In addition, the differential scanning calorimetry (DSC) curve of the pure blend displays the miscibility of the blend components, confirmed by the presence of a single glass transition. Transmission electron microscopy (TEM) micrographs showed that the average sizes of Cu and Se nanoparticles are about 11 and 41 nm, respectively. The maximum values of AC and DC conductivity were 6.76 * [10.sup.-6] S.[cm.sup.-1] and 5.49 * [10.sup.-10] for a PVA/CMC film filled with 1.60 wt.% of Cu-Se NPs. The mechanical properties of the PVA/CMC blend improved after adding the hybrid NPs. Moreover, the antibacterial activity of the prepared samples was increased due to the filling of Cu-Se nanoparticles to the films. Therefore, these results indicate the multifunctionality of PVA/CMC/Cu-Se nanocomposite samples for use in electrical energy storage, solid-polymer electrolytes, and food packaging industry. KEYWORDS AC conductivity, antibacterial activity, Cu NPs, mechanical properties, Se NPs Polymer nanocomposite samples of a polyvinyl alcohol (PVA)/carboxymethyl cellulose (CMC) blend doped with copper nanoparticles and selenium nanoparticles (Cu NPs/Se NPs) were prepared by the casting method. X‐ray diffraction analysis (XRD) patterns showed an increase in the degree of amorphous nature of the host polymeric matrix with increasing content of Cu/Se nanoparticles. The addition of 1.60 wt.%, Cu/Se NPs narrowed the indirect optical energy gap value of the nanocomposite from 3.97 to 2.39 eV. In addition, the differential scanning calorimetry (DSC) curve of the pure blend displays the miscibility of the blend components, confirmed by the presence of a single glass transition. Transmission electron microscopy (TEM) micrographs showed that the average sizes of Cu and Se nanoparticles are about 11 and 41 nm, respectively. The maximum values of AC and DC conductivity were 6.76 × 10 −6 S.cm −1 and 5.49 × 10 −10 for a PVA/CMC film filled with 1.60 wt.% of Cu‐Se NPs. The mechanical properties of the PVA/CMC blend improved after adding the hybrid NPs. Moreover, the antibacterial activity of the prepared samples was increased due to the filling of Cu‐Se nanoparticles to the films. Therefore, these results indicate the multifunctionality of PVA/CMC/Cu‐Se nanocomposite samples for use in electrical energy storage, solid‐polymer electrolytes, and food packaging industry. Polymer nanocomposite samples of a polyvinyl alcohol (PVA)/carboxymethyl cellulose (CMC) blend doped with copper nanoparticles and selenium nanoparticles (Cu NPs/Se NPs) were prepared by the casting method. X-ray diffraction analysis (XRD) patterns showed an increase in the degree of amorphous nature of the host polymeric matrix with increasing content of Cu/Se nanoparticles. The addition of 1.60 wt.%, Cu/Se NPs narrowed the indirect optical energy gap value of the nanocomposite from 3.97 to 2.39 eV. In addition, the differential scanning calorimetry (DSC) curve of the pure blend displays the miscibility of the blend components, confirmed by the presence of a single glass transition. Transmission electron microscopy (TEM) micrographs showed that the average sizes of Cu and Se nanoparticles are about 11 and 41 nm, respectively. The maximum values of AC and DC conductivity were 6.76 * [10.sup.-6] S.[cm.sup.-1] and 5.49 * [10.sup.-10] for a PVA/CMC film filled with 1.60 wt.% of Cu-Se NPs. The mechanical properties of the PVA/CMC blend improved after adding the hybrid NPs. Moreover, the antibacterial activity of the prepared samples was increased due to the filling of Cu-Se nanoparticles to the films. Therefore, these results indicate the multifunctionality of PVA/CMC/Cu-Se nanocomposite samples for use in electrical energy storage, solid-polymer electrolytes, and food packaging industry. |
| Audience | Academic |
| Author | Asnag, G. M. Abdallah, E. M. Morsi, M. A. Aljohani, Marwah Yassin, A. Y. Albalwa, Aisha Nawaf |
| Author_xml | – sequence: 1 givenname: E. M. orcidid: 0000-0002-7692-7174 surname: Abdallah fullname: Abdallah, E. M. email: dr.e_abdallah91@yahoo.com organization: Delta University for Science and Technology – sequence: 2 givenname: G. M. surname: Asnag fullname: Asnag, G. M. email: g.asnag@yahoo.com organization: Azal University for Human Development – sequence: 3 givenname: M. A. surname: Morsi fullname: Morsi, M. A. organization: Egyptian Russian University – sequence: 4 givenname: Marwah surname: Aljohani fullname: Aljohani, Marwah organization: Imam Abdulrahman Bin Faisal University – sequence: 5 givenname: Aisha Nawaf surname: Albalwa fullname: Albalwa, Aisha Nawaf organization: University of Tabuk – sequence: 6 givenname: A. Y. surname: Yassin fullname: Yassin, A. Y. organization: Delta University for Science and Technology |
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| Copyright | 2023 Society of Plastics Engineers. COPYRIGHT 2023 Society of Plastics Engineers, Inc. 2023 Society of Plastics Engineers |
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| Snippet | Polymer nanocomposite samples of a polyvinyl alcohol (PVA)/carboxymethyl cellulose (CMC) blend doped with copper nanoparticles and selenium nanoparticles (Cu... |
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| SubjectTerms | AC conductivity Analysis antibacterial activity Antibacterial agents Calorimetry Carboxymethyl cellulose Carboxymethylcellulose Cellulose Copper Cu NPs Diffraction Diffraction patterns Electric properties Electrolytes Energy gap Energy storage Food packaging industry Founding Glass transition Mechanical properties Miscibility Molten salt electrolytes Nanocomposites Nanoparticles Optical properties Photomicrographs Polyelectrolytes Polymeric composites Polymers Polyvinyl alcohol Properties Se NPs Selenium Solid electrolytes X-rays |
| Title | Elucidation of the effect of hybrid copper/selenium nanofiller on the optical, thermal, electrical, mechanical properties and antibacterial activity of polyvinyl alcohol/carboxymethyl cellulose blend |
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