Synthesis and characterization of a binary noble metal nitride
There has been considerable interest in the synthesis of new nitrides because of their technological and fundamental importance 1 , 2 . Although numerous metals react with nitrogen there are no known binary nitrides of the noble metals. We report the discovery and characterization of platinum nitrid...
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| Published in | Nature materials Vol. 3; no. 5; pp. 294 - 297 |
|---|---|
| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
London
Nature Publishing Group UK
01.05.2004
Nature Publishing Group |
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| Online Access | Get full text |
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| Abstract | There has been considerable interest in the synthesis of new nitrides because of their technological and fundamental importance
1
,
2
. Although numerous metals react with nitrogen there are no known binary nitrides of the noble metals. We report the discovery and characterization of platinum nitride (PtN), the first binary nitride of the noble metals group. This compound can be formed above 45–50 GPa and temperatures exceeding 2,000 K, and is stable after quenching to room pressure and temperature. It is characterized by a very high Raman-scattering cross-section with easily observed second- and third-order Raman bands. Synchrotron X-ray diffraction shows that the new phase is cubic with a remarkably high bulk modulus of 372(±5) GPa. |
|---|---|
| AbstractList | There has been considerable interest in the synthesis of new nitrides because of their technological and fundamental importance
1
,
2
. Although numerous metals react with nitrogen there are no known binary nitrides of the noble metals. We report the discovery and characterization of platinum nitride (PtN), the first binary nitride of the noble metals group. This compound can be formed above 45–50 GPa and temperatures exceeding 2,000 K, and is stable after quenching to room pressure and temperature. It is characterized by a very high Raman-scattering cross-section with easily observed second- and third-order Raman bands. Synchrotron X-ray diffraction shows that the new phase is cubic with a remarkably high bulk modulus of 372(±5) GPa. There has been considerable interest in the synthesis of new nitrides because of their technological and fundamental importance. Although numerous metals react with nitrogen there are no known binary nitrides of the noble metals. We report the discovery and characterization of platinum nitride (PtN), the first binary nitride of the noble metals group. This compound can be formed above 45-50 GPa and temperatures exceeding 2,000 K, and is stable after quenching to room pressure and temperature. It is characterized by a very high Raman-scattering cross-section with easily observed second- and third-order Raman bands. Synchrotron X-ray diffraction shows that the new phase is cubic with a remarkably high bulk modulus of 372(+/-5) GPa. There has been considerable interest in the synthesis of new nitrides because of their technological and fundamental importance. Although numerous metals react with nitrogen there are no known binary nitrides of the noble metals. We report the discovery and characterization of platinum nitride (PtN), the first binary nitride of the noble metals group. This compound can be formed above 45-50 GPa and temperatures exceeding 2,000 K, and is stable after quenching to room pressure and temperature. It is characterized by a very high Raman-scattering cross-section with easily observed second- and third-order Raman bands. Synchrotron X-ray diffraction shows that the new phase is cubic with a remarkably high bulk modulus of 372(+/-5) GPa.There has been considerable interest in the synthesis of new nitrides because of their technological and fundamental importance. Although numerous metals react with nitrogen there are no known binary nitrides of the noble metals. We report the discovery and characterization of platinum nitride (PtN), the first binary nitride of the noble metals group. This compound can be formed above 45-50 GPa and temperatures exceeding 2,000 K, and is stable after quenching to room pressure and temperature. It is characterized by a very high Raman-scattering cross-section with easily observed second- and third-order Raman bands. Synchrotron X-ray diffraction shows that the new phase is cubic with a remarkably high bulk modulus of 372(+/-5) GPa. There has been considerable interest in the synthesis of new nitrides because of their technological and fundamental importance1, 2. Although numerous metals react with nitrogen there are no known binary nitrides of the noble metals. We report the discovery and characterization of platinum nitride (PtN), the first binary nitride of the noble metals group. This compound can be formed above 45−50 GPa and temperatures exceeding 2,000 K, and is stable after quenching to room pressure and temperature. It is characterized by a very high Raman-scattering cross-section with easily observed second- and third-order Raman bands. Synchrotron X-ray diffraction shows that the new phase is cubic with a remarkably high bulk modulus of 372(plusminus5) GPa. There has been considerable interest in the synthesis of new nitrides because of their technological and fundamental importance. Although numerous metals react with nitrogen there are no known binary nitrides of the noble metals. We report the discovery and characterization of platinum nitride (PtN), the first binary nitride of the noble metals group. This compound can be formed above 45-50 GPa and temperatures exceeding 2,000 K, and is stable after quenching to room pressure and temperature. It is characterized by a very high Raman-scattering cross-section with easily observed second- and third-order Raman bands. Synchrotron X-ray diffraction shows that the new phase is cubic with a remarkably high bulk modulus of 372(c5) GPa. |
| Author | Badro, James Somayazulu, M. Fiquet, Guillaume Hemley, Russell J. Sanloup, Chrystele Gregoryanz, Eugene Mao, Ho-kwang |
| Author_xml | – sequence: 1 givenname: Eugene surname: Gregoryanz fullname: Gregoryanz, Eugene email: e.gregoryanz@gl.ciw.edu organization: Université Pierre et Marie Curie, LMCP, case 115, Geophysical Laboratory, Carnegie Institution of Washington, Geophysical Laboratory, Carnegie Institution of Washington – sequence: 2 givenname: Chrystele surname: Sanloup fullname: Sanloup, Chrystele organization: Université Pierre et Marie Curie, Laboratoire Magie, case 110 – sequence: 3 givenname: M. surname: Somayazulu fullname: Somayazulu, M. organization: HPCAT, Carnegie Institution of Washington, APS – sequence: 4 givenname: James surname: Badro fullname: Badro, James organization: Université Pierre et Marie Curie, LMCP, case 115 – sequence: 5 givenname: Guillaume surname: Fiquet fullname: Fiquet, Guillaume organization: Université Pierre et Marie Curie, LMCP, case 115 – sequence: 6 givenname: Ho-kwang surname: Mao fullname: Mao, Ho-kwang organization: Geophysical Laboratory, Carnegie Institution of Washington – sequence: 7 givenname: Russell J. surname: Hemley fullname: Hemley, Russell J. organization: Geophysical Laboratory, Carnegie Institution of Washington |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/15107839$$D View this record in MEDLINE/PubMed https://hal.science/hal-00085984$$DView record in HAL |
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| Snippet | There has been considerable interest in the synthesis of new nitrides because of their technological and fundamental importance
1
,
2
. Although numerous... There has been considerable interest in the synthesis of new nitrides because of their technological and fundamental importance. Although numerous metals react... There has been considerable interest in the synthesis of new nitrides because of their technological and fundamental importance1, 2. Although numerous metals... |
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| StartPage | 294 |
| SubjectTerms | Biomaterials Chemistry and Materials Science Computer Simulation Condensed Matter Physics Cross-sections letter Materials Science Materials Testing Metals Metals - chemical synthesis Metals - chemistry Models, Molecular Molecular Conformation Nanotechnology Nitrogen Nitrogen Compounds - chemical synthesis Nitrogen Compounds - chemistry Optical and Electronic Materials Platinum Platinum Compounds - chemical synthesis Platinum Compounds - chemistry Pressure Spectrum Analysis, Raman Surface Properties X-ray diffraction |
| Title | Synthesis and characterization of a binary noble metal nitride |
| URI | https://link.springer.com/article/10.1038/nmat1115 https://www.ncbi.nlm.nih.gov/pubmed/15107839 https://www.proquest.com/docview/222763187 https://www.proquest.com/docview/71903212 https://www.proquest.com/docview/743489512 https://hal.science/hal-00085984 |
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