Molybdenum arsenate crystal: A highly efficient and recyclable catalyst for hydrolysis of ethylene carbonate
•The molybdenum arsenate crystal can provide a suitable catalyst for hydrolysis of ester reactions.•The heterogeneous catalyst displayed high catalytic activity for hydrolysis of ethylene carbonate reactions.•The catalyst can be simply recovered and reused without significant loss of catalytic activ...
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Published in | Applied catalysis. A, General Vol. 471; pp. 50 - 55 |
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Main Authors | , , , , , , |
Format | Journal Article |
Language | English |
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10.02.2014
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Abstract | •The molybdenum arsenate crystal can provide a suitable catalyst for hydrolysis of ester reactions.•The heterogeneous catalyst displayed high catalytic activity for hydrolysis of ethylene carbonate reactions.•The catalyst can be simply recovered and reused without significant loss of catalytic activity.•The catalyst gave 96.5% conversion under optimized conditions.
A simple one-step hydrothermal reaction was employed to synthesize the molybdenum arsenate crystallite catalyst, [{Cu(imi)2}3As3Mo3O15]·H2O (1) (imi=imidazole). The catalyst was characterized using X-ray crystallographic analyses, FT-IR, TGA, XRD, ICP-AES, NH3-TPD and BET techniques. Moreover, we performed evaluation on its catalytic activity towards the hydrolysis of ethylene carbonate to produce ethylene glycol. Interestingly, the conversion of this reaction reaches 96.5% and the selectivity is close to 100% at optimum conditions. No polyoxometalate leaching or framework decomposition was observed and the catalyst can be recovered and reused with slight loss of reactivity under identical reaction conditions. |
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AbstractList | A simple one-step hydrothermal reaction was employed to synthesize the molybdenum arsenate crystallite catalyst, [{Cu(imi)2}3As3Mo3O15].H2O (1) (imi = imidazole). The catalyst was characterized using X-ray crystallographic analyses, FT-IR, TGA, XRD, ICP-AES, NH3-TPD and BET techniques. Moreover, we performed evaluation on its catalytic activity towards the hydrolysis of ethylene carbonate to produce ethylene glycol. Interestingly, the conversion of this reaction reaches 96.5% and the selectivity is close to 100% at optimum conditions. No polyoxometalate leaching or framework decomposition was observed and the catalyst can be recovered and reused with slight loss of reactivity under identical reaction conditions. A simple one-step hydrothermal reaction was employed to synthesize the molybdenum arsenate crystallite catalyst, [{Cu(imi) sub(2)} sub(3)As sub(3)Mo sub(3)O sub(15)][middot]H sub(2)O (1) (imi = imidazole). The catalyst was characterized using X-ray crystallographic analyses, FT-IR, TGA, XRD, ICP-AES, NH sub(3)-TPD and BET techniques. Moreover, we performed evaluation on its catalytic activity towards the hydrolysis of ethylene carbonate to produce ethylene glycol. Interestingly, the conversion of this reaction reaches 96.5% and the selectivity is close to 100% at optimum conditions. No polyoxometalate leaching or framework decomposition was observed and the catalyst can be recovered and reused with slight loss of reactivity under identical reaction conditions. •The molybdenum arsenate crystal can provide a suitable catalyst for hydrolysis of ester reactions.•The heterogeneous catalyst displayed high catalytic activity for hydrolysis of ethylene carbonate reactions.•The catalyst can be simply recovered and reused without significant loss of catalytic activity.•The catalyst gave 96.5% conversion under optimized conditions. A simple one-step hydrothermal reaction was employed to synthesize the molybdenum arsenate crystallite catalyst, [{Cu(imi)2}3As3Mo3O15]·H2O (1) (imi=imidazole). The catalyst was characterized using X-ray crystallographic analyses, FT-IR, TGA, XRD, ICP-AES, NH3-TPD and BET techniques. Moreover, we performed evaluation on its catalytic activity towards the hydrolysis of ethylene carbonate to produce ethylene glycol. Interestingly, the conversion of this reaction reaches 96.5% and the selectivity is close to 100% at optimum conditions. No polyoxometalate leaching or framework decomposition was observed and the catalyst can be recovered and reused with slight loss of reactivity under identical reaction conditions. |
Author | Gao, Limin Su, Zhanhua Cai, Qinghai Bi, Jiancong Zhao, Zhifeng Zhou, Baibin Ding, Yuanzhu |
Author_xml | – sequence: 1 givenname: Zhifeng surname: Zhao fullname: Zhao, Zhifeng email: zhifengzhao1980@163.com organization: College of Materials Science and Engineering, University of Science and Technology Heilongjiang, Harbin 150022, PR China – sequence: 2 givenname: Yuanzhu surname: Ding fullname: Ding, Yuanzhu organization: College of Materials Science and Engineering, University of Science and Technology Heilongjiang, Harbin 150022, PR China – sequence: 3 givenname: Jiancong surname: Bi fullname: Bi, Jiancong organization: College of Materials Science and Engineering, University of Science and Technology Heilongjiang, Harbin 150022, PR China – sequence: 4 givenname: Zhanhua surname: Su fullname: Su, Zhanhua email: su_zhan_hua@163.com organization: Key Laboratory of Synthesis of Functional Materials and Green Catalysis, Colleges of Heilongjiang Province, Harbin Normal University, Harbin 150025, PR China – sequence: 5 givenname: Qinghai surname: Cai fullname: Cai, Qinghai organization: Key Laboratory of Synthesis of Functional Materials and Green Catalysis, Colleges of Heilongjiang Province, Harbin Normal University, Harbin 150025, PR China – sequence: 6 givenname: Limin surname: Gao fullname: Gao, Limin organization: College of Materials Science and Engineering, University of Science and Technology Heilongjiang, Harbin 150022, PR China – sequence: 7 givenname: Baibin surname: Zhou fullname: Zhou, Baibin organization: Key Laboratory of Synthesis of Functional Materials and Green Catalysis, Colleges of Heilongjiang Province, Harbin Normal University, Harbin 150025, PR China |
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CitedBy_id | crossref_primary_10_1002_cctc_202300504 crossref_primary_10_1039_C7GC03773B crossref_primary_10_1016_j_cep_2023_109519 crossref_primary_10_1007_s10876_018_1390_6 crossref_primary_10_1016_j_inoche_2015_09_008 crossref_primary_10_1016_j_inoche_2017_05_024 |
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Keywords | Hydrolysis Heterogeneous catalysis Ethylene glycol POMs crystal Arsenates Crystals Recyclable catalyst Transition metal Carbonates Molybdenum Glycol |
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Snippet | •The molybdenum arsenate crystal can provide a suitable catalyst for hydrolysis of ester reactions.•The heterogeneous catalyst displayed high catalytic... A simple one-step hydrothermal reaction was employed to synthesize the molybdenum arsenate crystallite catalyst, [{Cu(imi)2}3As3Mo3O15].H2O (1) (imi =... A simple one-step hydrothermal reaction was employed to synthesize the molybdenum arsenate crystallite catalyst, [{Cu(imi) sub(2)} sub(3)As sub(3)Mo sub(3)O... |
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SubjectTerms | Arsenates Carbonates Catalysis Catalysts Chemistry Emission analysis Ethylene Ethylene glycol Exact sciences and technology General and physical chemistry Heterogeneous catalysis Hydrolysis Inductively coupled plasma Molybdenum POMs crystal Spectroscopy Theory of reactions, general kinetics. Catalysis. Nomenclature, chemical documentation, computer chemistry |
Title | Molybdenum arsenate crystal: A highly efficient and recyclable catalyst for hydrolysis of ethylene carbonate |
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