Surface modification of nanosatrch using nano silver: a potential antibacterial for food package coating
Starch nanocrystal was prepared using weak sulfuric acid hydrolysis at 40 °C. Transmission electron micrographs of dilute suspensions of starch nanocrystals showed round particles with a diameter ranging from 20 to 40 nm. SEM of freeze dried samples showed separated particles between 40 and 100 nm a...
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| Published in | Journal of food science and technology Vol. 55; no. 3; pp. 899 - 904 |
|---|---|
| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
New Delhi
Springer India
01.03.2018
Springer Nature B.V |
| Subjects | |
| Online Access | Get full text |
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| Abstract | Starch nanocrystal was prepared using weak sulfuric acid hydrolysis at 40 °C. Transmission electron micrographs of dilute suspensions of starch nanocrystals showed round particles with a diameter ranging from 20 to 40 nm. SEM of freeze dried samples showed separated particles between 40 and 100 nm and confirmed production of starch nano particles. XRD patterns obtained for the prepared nanostarch and raw starch sample showed no special pattern of crystallinity for starch sample. Extracted nanostarch showed pattern of crystallinity with the peaks at Bragg angles (2θ) at about 15° and 23°, and a doublet at 17° and 18°. The crystalline structure of prepared sample was A-type. FTIR spectra confirmed the particles oxidation. Nano silver particle was precipitated on the starch nano particle. UV spectra confirmed the presence of silver particle on the starch particles. Inhibitions tests of nanostarch bearing nano silver on three types of bacteria was investigated. The inhibition test results were 25 µg/mL for
S. aureus
, and
S. typhi
, and 12.5 µg/mL for
E. coli
. |
|---|---|
| AbstractList | Starch nanocrystal was prepared using weak sulfuric acid hydrolysis at 40 °C. Transmission electron micrographs of dilute suspensions of starch nanocrystals showed round particles with a diameter ranging from 20 to 40 nm. SEM of freeze dried samples showed separated particles between 40 and 100 nm and confirmed production of starch nano particles. XRD patterns obtained for the prepared nanostarch and raw starch sample showed no special pattern of crystallinity for starch sample. Extracted nanostarch showed pattern of crystallinity with the peaks at Bragg angles (2θ) at about 15° and 23°, and a doublet at 17° and 18°. The crystalline structure of prepared sample was A-type. FTIR spectra confirmed the particles oxidation. Nano silver particle was precipitated on the starch nano particle. UV spectra confirmed the presence of silver particle on the starch particles. Inhibitions tests of nanostarch bearing nano silver on three types of bacteria was investigated. The inhibition test results were 25 µg/mL for
, and
, and 12.5 µg/mL for
. Starch nanocrystal was prepared using weak sulfuric acid hydrolysis at 40 °C. Transmission electron micrographs of dilute suspensions of starch nanocrystals showed round particles with a diameter ranging from 20 to 40 nm. SEM of freeze dried samples showed separated particles between 40 and 100 nm and confirmed production of starch nano particles. XRD patterns obtained for the prepared nanostarch and raw starch sample showed no special pattern of crystallinity for starch sample. Extracted nanostarch showed pattern of crystallinity with the peaks at Bragg angles (2θ) at about 15° and 23°, and a doublet at 17° and 18°. The crystalline structure of prepared sample was A-type. FTIR spectra confirmed the particles oxidation. Nano silver particle was precipitated on the starch nano particle. UV spectra confirmed the presence of silver particle on the starch particles. Inhibitions tests of nanostarch bearing nano silver on three types of bacteria was investigated. The inhibition test results were 25 µg/mL for S. aureus, and S. typhi, and 12.5 µg/mL for E. coli. Starch nanocrystal was prepared using weak sulfuric acid hydrolysis at 40 °C. Transmission electron micrographs of dilute suspensions of starch nanocrystals showed round particles with a diameter ranging from 20 to 40 nm. SEM of freeze dried samples showed separated particles between 40 and 100 nm and confirmed production of starch nano particles. XRD patterns obtained for the prepared nanostarch and raw starch sample showed no special pattern of crystallinity for starch sample. Extracted nanostarch showed pattern of crystallinity with the peaks at Bragg angles (2θ) at about 15° and 23°, and a doublet at 17° and 18°. The crystalline structure of prepared sample was A-type. FTIR spectra confirmed the particles oxidation. Nano silver particle was precipitated on the starch nano particle. UV spectra confirmed the presence of silver particle on the starch particles. Inhibitions tests of nanostarch bearing nano silver on three types of bacteria was investigated. The inhibition test results were 25 µg/mL for S. aureus , and S. typhi , and 12.5 µg/mL for E. coli . |
| Author | Khalilzadeh, Mohammad A. Sadeghifar, Hasan Amirsoleimani, Mina Sadeghifar, Fatemeh |
| Author_xml | – sequence: 1 givenname: Mina surname: Amirsoleimani fullname: Amirsoleimani, Mina organization: Department of Phytochemistry, Qaemshahr Branch, Islamic Azad University – sequence: 2 givenname: Mohammad A. surname: Khalilzadeh fullname: Khalilzadeh, Mohammad A. organization: Department of Phytochemistry, Qaemshahr Branch, Islamic Azad University – sequence: 3 givenname: Fatemeh surname: Sadeghifar fullname: Sadeghifar, Fatemeh organization: Department of Biology, North Carolina State University – sequence: 4 givenname: Hasan surname: Sadeghifar fullname: Sadeghifar, Hasan email: hsadegh@ncsu.edu organization: Department of Wood and Paper Science, Sari Branch, Islamic Azad University, Department of Forest Biomaterials, North Carolina State University |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/29487431$$D View this record in MEDLINE/PubMed |
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| Cites_doi | 10.1016/j.cocis.2014.06.001 10.1016/j.carbpol.2010.10.011 10.1016/j.carbpol.2012.11.022 10.1016/j.carbpol.2007.07.025 10.1039/C4RA14090G 10.1016/j.foodchem.2014.04.068 10.1016/j.reactfunctpolym.2014.09.020 10.1016/S0008-6215(00)90933-9 10.1021/ma00138a009 10.1021/la047530j 10.1016/S0141-8130(98)00040-3 10.1021/bm901428y 10.1016/j.ijbiomac.2015.12.040 10.1016/j.carbpol.2011.02.016 10.1002/star.19880400102 10.1039/c3ra41610k 10.1016/j.carbpol.2011.07.012 10.1016/j.foodchem.2006.01.060 10.1016/B978-0-12-746270-7.50013-6 |
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| Copyright | Association of Food Scientists & Technologists (India) 2018 Journal of Food Science and Technology is a copyright of Springer, (2018). All Rights Reserved. |
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| Keywords | Nanoparticles Surface modification Nano silver Nanostarch Antibacterial |
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| Snippet | Starch nanocrystal was prepared using weak sulfuric acid hydrolysis at 40 °C. Transmission electron micrographs of dilute suspensions of starch nanocrystals... Starch nanocrystal was prepared using weak sulfuric acid hydrolysis at 40 °C. Transmission electron micrographs of dilute suspensions of starch nanocrystals... |
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| SubjectTerms | Chemistry Chemistry and Materials Science Chemistry/Food Science Crystal structure Crystallinity Dilution E coli Electron micrographs Food packaging Food Science Freeze drying Nanocrystals Nanoparticles Nutrition Original Original Article Oxidation Protective coatings Silver Starch Studies Sulfuric acid |
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| Title | Surface modification of nanosatrch using nano silver: a potential antibacterial for food package coating |
| URI | https://link.springer.com/article/10.1007/s13197-017-2996-7 https://www.ncbi.nlm.nih.gov/pubmed/29487431 https://www.proquest.com/docview/2000802610 https://search.proquest.com/docview/2009212509 https://pubmed.ncbi.nlm.nih.gov/PMC5821645 |
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