Preparation and Characterization of a Novel Sulfonated Titanium Oxide Incorporated Chitosan Nanocomposite Membranes for Fuel Cell Application

In this study, nano-TiO2 sulfonated with 1,3-propane sultone (STiO2) was incorporated into the chitosan (CS) matrix for the preparation of CS/STiO2 nanocomposite membranes for fuel cell applications. The grafting of sulfonic acid (–SO3H) groups was confirmed by Fourier transform infrared spectroscop...

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Published inMembranes (Basel) Vol. 11; no. 6; p. 450
Main Authors Ahmed, Saad, Arshad, Tasleem, Zada, Amir, Afzal, Annum, Khan, Muhammad, Hussain, Amjad, Hassan, Muhammad, Ali, Muhammad, Xu, Shiai
Format Journal Article
LanguageEnglish
Published Basel MDPI AG 17.06.2021
MDPI
Subjects
Biosensors
Chain mobility
Chitosan
Conductivity
Fourier analysis
Fourier transforms
Fuel cells
Fuel technology
Infrared analysis
Infrared spectroscopy
Interface stability
Ion exchange
Membranes
nanocomposite membrane
Nanocomposites
Physicochemical properties
Polymers
proton exchange membrane fuel cell
Proton exchange membrane fuel cells
Protons
Scanning electron microscopy
Spectrum analysis
sulfonated TiO2
Sulfonic acid
Sulfur
Swelling ratio
Thermogravimetric analysis
Titanium dioxide
Titanium oxide
Titanium oxides
Water uptake
X-ray spectroscopy
United States > US
China
Japan
Online AccessGet full text

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Abstract In this study, nano-TiO2 sulfonated with 1,3-propane sultone (STiO2) was incorporated into the chitosan (CS) matrix for the preparation of CS/STiO2 nanocomposite membranes for fuel cell applications. The grafting of sulfonic acid (–SO3H) groups was confirmed by Fourier transform infrared spectroscopy, thermogravimetric analysis and energy-dispersive X-ray spectroscopy. The physicochemical properties of these prepared membranes, such as water uptake, swelling ratio, thermal and mechanical stability, ion exchange capacity and proton conductivity, were determined. The proton conducting groups on the surface of nano-TiO2 can form continuous proton conducting pathways along the CS/STiO2 interface and thus improve the proton conductivity of CS/STiO2 nanocomposite membranes. The CS/STiO2 nanocomposite membrane with 5 wt% of sulfonated TiO2 showed a proton conductivity (0.035 S·cm−1) equal to that of commercial Nafion 117 membrane (0.033 S·cm−1). The thermal and mechanical stability of the nanocomposite membranes were improved because the interfacial interaction between the -SO3H group of TiO2 and the –NH2 group of CS can restrict the mobility of CS chains to enhance the thermal and mechanical stability of the nanocomposite membranes. These CS/STiO2 nanocomposite membranes have promising applications in proton exchange membrane fuel cells.
AbstractList In this study, nano-TiO 2 sulfonated with 1,3-propane sultone (STiO 2 ) was incorporated into the chitosan (CS) matrix for the preparation of CS/STiO 2 nanocomposite membranes for fuel cell applications. The grafting of sulfonic acid (–SO 3 H) groups was confirmed by Fourier transform infrared spectroscopy, thermogravimetric analysis and energy-dispersive X-ray spectroscopy. The physicochemical properties of these prepared membranes, such as water uptake, swelling ratio, thermal and mechanical stability, ion exchange capacity and proton conductivity, were determined. The proton conducting groups on the surface of nano-TiO 2 can form continuous proton conducting pathways along the CS/STiO 2 interface and thus improve the proton conductivity of CS/STiO 2 nanocomposite membranes. The CS/STiO 2 nanocomposite membrane with 5 wt% of sulfonated TiO 2 showed a proton conductivity (0.035 S·cm −1 ) equal to that of commercial Nafion 117 membrane (0.033 S·cm −1 ). The thermal and mechanical stability of the nanocomposite membranes were improved because the interfacial interaction between the -SO 3 H group of TiO 2 and the –NH 2 group of CS can restrict the mobility of CS chains to enhance the thermal and mechanical stability of the nanocomposite membranes. These CS/STiO 2 nanocomposite membranes have promising applications in proton exchange membrane fuel cells.
In this study, nano-TiO2 sulfonated with 1,3-propane sultone (STiO2) was incorporated into the chitosan (CS) matrix for the preparation of CS/STiO2 nanocomposite membranes for fuel cell applications. The grafting of sulfonic acid (–SO3H) groups was confirmed by Fourier transform infrared spectroscopy, thermogravimetric analysis and energy-dispersive X-ray spectroscopy. The physicochemical properties of these prepared membranes, such as water uptake, swelling ratio, thermal and mechanical stability, ion exchange capacity and proton conductivity, were determined. The proton conducting groups on the surface of nano-TiO2 can form continuous proton conducting pathways along the CS/STiO2 interface and thus improve the proton conductivity of CS/STiO2 nanocomposite membranes. The CS/STiO2 nanocomposite membrane with 5 wt% of sulfonated TiO2 showed a proton conductivity (0.035 S·cm−1) equal to that of commercial Nafion 117 membrane (0.033 S·cm−1). The thermal and mechanical stability of the nanocomposite membranes were improved because the interfacial interaction between the -SO3H group of TiO2 and the –NH2 group of CS can restrict the mobility of CS chains to enhance the thermal and mechanical stability of the nanocomposite membranes. These CS/STiO2 nanocomposite membranes have promising applications in proton exchange membrane fuel cells.
Author Arshad, Tasleem
Hassan, Muhammad
Ali, Muhammad
Hussain, Amjad
Zada, Amir
Xu, Shiai
Ahmed, Saad
Afzal, Annum
Khan, Muhammad
AuthorAffiliation 1 School of Materials, East China University of Science and Technology, Shanghai 200237, China; saad_ahmad02@yahoo.com (S.A.); ali1095@gmail.com (M.A.)
3 Department of Chemistry, University of Okara, Okara 56300, Pakistan; tasleemarshad92@gmail.com (T.A.); anumafzal@mail.ustc.edu.cn (A.A.); mkhanchemistry@yahoo.com (M.K.); amjadhussain@uo.edu.pk (A.H.); mhassan@szu.edu.cn (M.H.)
4 Department of Chemistry, Abdul Wali Khan University Mardan, Mardan 23200, Pakistan; amistry009@yahoo.com
2 School of Chemical Engineering, Qinghai University, Xining 810016, China
AuthorAffiliation_xml – name: 3 Department of Chemistry, University of Okara, Okara 56300, Pakistan; tasleemarshad92@gmail.com (T.A.); anumafzal@mail.ustc.edu.cn (A.A.); mkhanchemistry@yahoo.com (M.K.); amjadhussain@uo.edu.pk (A.H.); mhassan@szu.edu.cn (M.H.)
– name: 2 School of Chemical Engineering, Qinghai University, Xining 810016, China
– name: 1 School of Materials, East China University of Science and Technology, Shanghai 200237, China; saad_ahmad02@yahoo.com (S.A.); ali1095@gmail.com (M.A.)
– name: 4 Department of Chemistry, Abdul Wali Khan University Mardan, Mardan 23200, Pakistan; amistry009@yahoo.com
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Snippet In this study, nano-TiO2 sulfonated with 1,3-propane sultone (STiO2) was incorporated into the chitosan (CS) matrix for the preparation of CS/STiO2...
In this study, nano-TiO 2 sulfonated with 1,3-propane sultone (STiO 2 ) was incorporated into the chitosan (CS) matrix for the preparation of CS/STiO 2...
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SubjectTerms Biosensors
Chain mobility
Chitosan
Conductivity
Fourier analysis
Fourier transforms
Fuel cells
Fuel technology
Infrared analysis
Infrared spectroscopy
Interface stability
Ion exchange
Membranes
nanocomposite membrane
Nanocomposites
Physicochemical properties
Polymers
proton exchange membrane fuel cell
Proton exchange membrane fuel cells
Protons
Scanning electron microscopy
Spectrum analysis
sulfonated TiO2
Sulfonic acid
Sulfur
Swelling ratio
Thermogravimetric analysis
Titanium dioxide
Titanium oxide
Titanium oxides
Water uptake
X-ray spectroscopy
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Title Preparation and Characterization of a Novel Sulfonated Titanium Oxide Incorporated Chitosan Nanocomposite Membranes for Fuel Cell Application
URI https://www.proquest.com/docview/2544893994
https://search.proquest.com/docview/2548397781
https://pubmed.ncbi.nlm.nih.gov/PMC8246320
https://doaj.org/article/03579d500899407aa9f05d1a23cdf0eb
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