Understanding and Calibration of Charge Storage Mechanism in Cyclic Voltammetry Curves
Noticeable pseudo‐capacitance behavior out of charge storage mechanism (CSM) has attracted intensive studies because it can provide both high energy density and large output power. Although cyclic voltammetry is recognized as the feasible electrochemical technique to determine it quantitatively in t...
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| Published in | Angewandte Chemie International Edition Vol. 60; no. 39; pp. 21310 - 21318 |
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| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Weinheim
Wiley Subscription Services, Inc
20.09.2021
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| Edition | International ed. in English |
| Subjects | |
| Online Access | Get full text |
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| Abstract | Noticeable pseudo‐capacitance behavior out of charge storage mechanism (CSM) has attracted intensive studies because it can provide both high energy density and large output power. Although cyclic voltammetry is recognized as the feasible electrochemical technique to determine it quantitatively in the previous works, the results are inferior due to uncertainty in the definitions and application conditions. Herein, three successive treatments, including de‐polarization, de‐residual and de‐background, as well as a non‐linear fitting algorithm are employed for the first time to calibrate the different CSM contribution of three typical cathode materials, LiFePO4, LiMn2O4 and Na4Fe3(PO4)2P2O7, and achieve well‐separated physical capacitance, pseudo‐capacitance and diffusive contributions to the total capacity. This work can eliminate misunderstanding concepts and correct ambiguous results of the pseudo‐capacitance contribution and recognize the essence of CSM in electrode materials.
Well‐separated physical capacitance, pseudo‐capacitance, and diffusive capacity are achieved from the CV curves of typical electrode materials for metal‐ion batteries after three successive treatments including de‐polarization, de‐residual and de‐background as well as non‐linear fitting calculation, offering a more rational and reliable method to calculate the pseudo‐capacitance contribution. |
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| AbstractList | Noticeable pseudo‐capacitance behavior out of charge storage mechanism (CSM) has attracted intensive studies because it can provide both high energy density and large output power. Although cyclic voltammetry is recognized as the feasible electrochemical technique to determine it quantitatively in the previous works, the results are inferior due to uncertainty in the definitions and application conditions. Herein, three successive treatments, including de‐polarization, de‐residual and de‐background, as well as a non‐linear fitting algorithm are employed for the first time to calibrate the different CSM contribution of three typical cathode materials, LiFePO 4 , LiMn 2 O 4 and Na 4 Fe 3 (PO 4 ) 2 P 2 O 7 , and achieve well‐separated physical capacitance, pseudo‐capacitance and diffusive contributions to the total capacity. This work can eliminate misunderstanding concepts and correct ambiguous results of the pseudo‐capacitance contribution and recognize the essence of CSM in electrode materials. Noticeable pseudo-capacitance behavior out of charge storage mechanism (CSM) has attracted intensive studies because it can provide both high energy density and large output power. Although cyclic voltammetry is recognized as the feasible electrochemical technique to determine it quantitatively in the previous works, the results are inferior due to uncertainty in the definitions and application conditions. Herein, three successive treatments, including de-polarization, de-residual and de-background, as well as a non-linear fitting algorithm are employed for the first time to calibrate the different CSM contribution of three typical cathode materials, LiFePO4 , LiMn2 O4 and Na4 Fe3 (PO4 )2 P2 O7 , and achieve well-separated physical capacitance, pseudo-capacitance and diffusive contributions to the total capacity. This work can eliminate misunderstanding concepts and correct ambiguous results of the pseudo-capacitance contribution and recognize the essence of CSM in electrode materials.Noticeable pseudo-capacitance behavior out of charge storage mechanism (CSM) has attracted intensive studies because it can provide both high energy density and large output power. Although cyclic voltammetry is recognized as the feasible electrochemical technique to determine it quantitatively in the previous works, the results are inferior due to uncertainty in the definitions and application conditions. Herein, three successive treatments, including de-polarization, de-residual and de-background, as well as a non-linear fitting algorithm are employed for the first time to calibrate the different CSM contribution of three typical cathode materials, LiFePO4 , LiMn2 O4 and Na4 Fe3 (PO4 )2 P2 O7 , and achieve well-separated physical capacitance, pseudo-capacitance and diffusive contributions to the total capacity. This work can eliminate misunderstanding concepts and correct ambiguous results of the pseudo-capacitance contribution and recognize the essence of CSM in electrode materials. Noticeable pseudo‐capacitance behavior out of charge storage mechanism (CSM) has attracted intensive studies because it can provide both high energy density and large output power. Although cyclic voltammetry is recognized as the feasible electrochemical technique to determine it quantitatively in the previous works, the results are inferior due to uncertainty in the definitions and application conditions. Herein, three successive treatments, including de‐polarization, de‐residual and de‐background, as well as a non‐linear fitting algorithm are employed for the first time to calibrate the different CSM contribution of three typical cathode materials, LiFePO4, LiMn2O4 and Na4Fe3(PO4)2P2O7, and achieve well‐separated physical capacitance, pseudo‐capacitance and diffusive contributions to the total capacity. This work can eliminate misunderstanding concepts and correct ambiguous results of the pseudo‐capacitance contribution and recognize the essence of CSM in electrode materials. Noticeable pseudo‐capacitance behavior out of charge storage mechanism (CSM) has attracted intensive studies because it can provide both high energy density and large output power. Although cyclic voltammetry is recognized as the feasible electrochemical technique to determine it quantitatively in the previous works, the results are inferior due to uncertainty in the definitions and application conditions. Herein, three successive treatments, including de‐polarization, de‐residual and de‐background, as well as a non‐linear fitting algorithm are employed for the first time to calibrate the different CSM contribution of three typical cathode materials, LiFePO4, LiMn2O4 and Na4Fe3(PO4)2P2O7, and achieve well‐separated physical capacitance, pseudo‐capacitance and diffusive contributions to the total capacity. This work can eliminate misunderstanding concepts and correct ambiguous results of the pseudo‐capacitance contribution and recognize the essence of CSM in electrode materials. Well‐separated physical capacitance, pseudo‐capacitance, and diffusive capacity are achieved from the CV curves of typical electrode materials for metal‐ion batteries after three successive treatments including de‐polarization, de‐residual and de‐background as well as non‐linear fitting calculation, offering a more rational and reliable method to calculate the pseudo‐capacitance contribution. |
| Author | Wang, Chunsheng Pu, Xiangjun Cao, Yuliang Cao, Shunan Zhao, Dong Chen, Zhongxue Fu, Chenglong |
| Author_xml | – sequence: 1 givenname: Xiangjun surname: Pu fullname: Pu, Xiangjun organization: Wuhan University – sequence: 2 givenname: Dong surname: Zhao fullname: Zhao, Dong organization: Wuhan University – sequence: 3 givenname: Chenglong surname: Fu fullname: Fu, Chenglong organization: Wuhan University – sequence: 4 givenname: Zhongxue orcidid: 0000-0002-1526-7336 surname: Chen fullname: Chen, Zhongxue email: zxchen_pmc@whu.edu.cn organization: Wuhan University – sequence: 5 givenname: Shunan surname: Cao fullname: Cao, Shunan email: shunancao@163.com organization: Wuhan University – sequence: 6 givenname: Chunsheng surname: Wang fullname: Wang, Chunsheng organization: University of Maryland – sequence: 7 givenname: Yuliang orcidid: 0000-0001-6092-5652 surname: Cao fullname: Cao, Yuliang email: ylcao@whu.edu.cn organization: Wuhan University |
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| Snippet | Noticeable pseudo‐capacitance behavior out of charge storage mechanism (CSM) has attracted intensive studies because it can provide both high energy density... Noticeable pseudo-capacitance behavior out of charge storage mechanism (CSM) has attracted intensive studies because it can provide both high energy density... |
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| SubjectTerms | Algorithms calibration Capacitance charge storage mechanism Electrochemistry Electrode materials Flux density Lithium manganese oxides non-linear fitting physical capacitance pseudo-capacitance Voltammetry |
| Title | Understanding and Calibration of Charge Storage Mechanism in Cyclic Voltammetry Curves |
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