Molecularly imprinted silica as a selective SPE sorbent for triazine herbicides
A molecularly imprinted organically modified silica was prepared through a simple sol-gel procedure and evaluated as a specific sorbent for SPE of triazine herbicides. The material proved to be highly selective for the template molecule, atrazine, as well as for other structurally related species su...
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| Published in | Journal of separation science Vol. 33; no. 9; pp. 1319 - 1324 |
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| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Weinheim
Wiley-VCH Verlag
01.05.2010
WILEY-VCH Verlag WILEY‐VCH Verlag Wiley |
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| Abstract | A molecularly imprinted organically modified silica was prepared through a simple sol-gel procedure and evaluated as a specific sorbent for SPE of triazine herbicides. The material proved to be highly selective for the template molecule, atrazine, as well as for other structurally related species such as simazine and propazine. The performance of this material was shown to be comparable with commercial acrylate-based molecularly imprinted polymers. The molecularly imprinted silica was applied for the determination of trace levels of the target triazine analytes in sugar cane juice (locally called "garapa"). |
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| AbstractList | A molecularly imprinted organically modified silica was prepared through a simple sol-gel procedure and evaluated as a specific sorbent for SPE of triazine herbicides. The material proved to be highly selective for the template molecule, atrazine, as well as for other structurally related species such as simazine and propazine. The performance of this material was shown to be comparable with commercial acrylate-based molecularly imprinted polymers. The molecularly imprinted silica was applied for the determination of trace levels of the target triazine analytes in sugar cane juice (locally called "garapa"). Abstract A molecularly imprinted organically modified silica was prepared through a simple sol‐gel procedure and evaluated as a specific sorbent for SPE of triazine herbicides. The material proved to be highly selective for the template molecule, atrazine, as well as for other structurally related species such as simazine and propazine. The performance of this material was shown to be comparable with commercial acrylate‐based molecularly imprinted polymers. The molecularly imprinted silica was applied for the determination of trace levels of the target triazine analytes in sugar cane juice (locally called “garapa”). |
| Author | Rosa Morais Vigna, Camila Collins, Carol H. Augusto, Fabio Bottoli, Carla B. G. Gomes Costa Silva, Raquel |
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| Cites_doi | 10.1021/cr990099w 10.1002/anie.200352298 10.1016/j.aca.2005.11.081 10.1016/S0021-9673(03)00552-1 10.1016/S0021-9673(03)00529-6 10.1016/S0003-2670(01)01421-0 10.1007/s00216-006-1004-2 10.1016/j.chroma.2006.02.051 10.1021/bk-1989-0414 10.1016/j.chroma.2006.08.095 10.1007/s00216-009-2930-6 10.1007/BF02493006 10.1007/s00216-003-1915-0 10.1016/j.bios.2006.05.014 10.1016/j.chroma.2006.09.076 10.1021/cr980039a 10.1016/j.chroma.2006.01.051 10.1016/j.chroma.2005.09.035 10.1007/s00216-006-0406-5 10.1021/ac010642k 10.1021/ac0105538 10.1016/j.chroma.2004.09.016 10.1016/j.snb.2006.07.022 10.1016/j.snb.2006.10.026 |
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| Keywords | Solid phase extraction Chemical analysis HPLC chromatography Silica Chemical enrichment Surface structure Affinity adsorbent Characterization Sample preparation Ormosils Quantitative analysis Trace analysis Scanning electron microscopy Sol-gel Pesticides Sugar juice Contamination Herbicide Ultraviolet detector Sol gel process Residue Morphology Preparation Triazine derivatives Sugar cane Molecular imprinting Molecularly imprinted sorbents Atrazine |
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| Snippet | A molecularly imprinted organically modified silica was prepared through a simple sol-gel procedure and evaluated as a specific sorbent for SPE of triazine... A molecularly imprinted organically modified silica was prepared through a simple sol‐gel procedure and evaluated as a specific sorbent for SPE of triazine... Abstract A molecularly imprinted organically modified silica was prepared through a simple sol‐gel procedure and evaluated as a specific sorbent for SPE of... |
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| SubjectTerms | Analytical chemistry Atrazine Biological and medical sciences Chemistry Chromatographic methods and physical methods associated with chromatography Exact sciences and technology Food industries Fundamental and applied biological sciences. Psychology Herbicides Imprinted polymers Juices Materials selection Molecularly imprinted sorbents Ormosils Other chromatographic methods Silicon dioxide Sol gel process Sol-gel Sorbents Sugar industries |
| Title | Molecularly imprinted silica as a selective SPE sorbent for triazine herbicides |
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