Tea saponin additive to extract eleutheroside B and E from Eleutherococcus senticosus by ultrasonic mediation and its application in a semi-pilot scale
•Use ultrasonic-assisted extraction of eleutheroside B and E from E. senticosus.•Tea saponin was first added to extract eleutherosides in the process.•Dynamic models under powers, temperatures were considered.•Determine optimum conditions of eleutheroside B and E by response surface method.•A 200-fo...
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Published in | Ultrasonics sonochemistry Vol. 86; p. 106039 |
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Main Authors | , , , , , |
Format | Journal Article |
Language | English |
Published |
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Elsevier B.V
01.05.2022
Elsevier |
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Online Access | Get full text |
ISSN | 1350-4177 1873-2828 1873-2828 |
DOI | 10.1016/j.ultsonch.2022.106039 |
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Abstract | •Use ultrasonic-assisted extraction of eleutheroside B and E from E. senticosus.•Tea saponin was first added to extract eleutherosides in the process.•Dynamic models under powers, temperatures were considered.•Determine optimum conditions of eleutheroside B and E by response surface method.•A 200-fold expansion of the semi-pilot test was carried out.
The safety of ethanol in operations and its effects on human health are gradually being questioned. Under this premise, we attempted to use the natural surfactant tea saponin, which originates from the processing residues of camellia oil, as the additive of the extraction solvent and to extract eleutheroside B and eleutheroside E in the roots and rhizomes of E. senticosus by ultrasonic mediation. After a single-factor experiment, extraction kinetics at different powers and reaction temperatures, and Box–Behnken design optimization, the optimal conditions obtained were 0.3% tea saponin solution as the extraction solvent, 20 mL/g liquid–solid ratio, 250 W ultrasonic irradiation power (43.4 mW/g ultrasonic power density) and 40 min ultrasonic irradiation time. Under optimal conditions, satisfactory yields of eleutheroside B (1.06 ± 0.04 mg/g) and eleutheroside E (2.65 ± 0.12 mg/g) were obtained with semi pilot scale ultrasonic extraction equipment. The experiments showed that compared with the traditional thermal extraction process, the extraction time is significantly reduced at lower operating temperatures. |
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AbstractList | The safety of ethanol in operations and its effects on human health are gradually being questioned. Under this premise, we attempted to use the natural surfactant tea saponin, which originates from the processing residues of camellia oil, as the additive of the extraction solvent and to extract eleutheroside B and eleutheroside E in the roots and rhizomes of E. senticosus by ultrasonic mediation. After a single-factor experiment, extraction kinetics at different powers and reaction temperatures, and Box–Behnken design optimization, the optimal conditions obtained were 0.3% tea saponin solution as the extraction solvent, 20 mL/g liquid–solid ratio, 250 W ultrasonic irradiation power (43.4 mW/g ultrasonic power density) and 40 min ultrasonic irradiation time. Under optimal conditions, satisfactory yields of eleutheroside B (1.06 ± 0.04 mg/g) and eleutheroside E (2.65 ± 0.12 mg/g) were obtained with semi pilot scale ultrasonic extraction equipment. The experiments showed that compared with the traditional thermal extraction process, the extraction time is significantly reduced at lower operating temperatures. • Use ultrasonic-assisted extraction of eleutheroside B and E from E. senticosus. • Tea saponin was first added to extract eleutherosides in the process. • Dynamic models under powers, temperatures were considered. • Determine optimum conditions of eleutheroside B and E by response surface method. • A 200-fold expansion of the semi-pilot test was carried out. The safety of ethanol in operations and its effects on human health are gradually being questioned. Under this premise, we attempted to use the natural surfactant tea saponin, which originates from the processing residues of camellia oil, as the additive of the extraction solvent and to extract eleutheroside B and eleutheroside E in the roots and rhizomes of E. senticosus by ultrasonic mediation. After a single-factor experiment, extraction kinetics at different powers and reaction temperatures, and Box–Behnken design optimization, the optimal conditions obtained were 0.3% tea saponin solution as the extraction solvent, 20 mL/g liquid–solid ratio, 250 W ultrasonic irradiation power (43.4 mW/g ultrasonic power density) and 40 min ultrasonic irradiation time. Under optimal conditions, satisfactory yields of eleutheroside B (1.06 ± 0.04 mg/g) and eleutheroside E (2.65 ± 0.12 mg/g) were obtained with semi pilot scale ultrasonic extraction equipment. The experiments showed that compared with the traditional thermal extraction process, the extraction time is significantly reduced at lower operating temperatures. The safety of ethanol in operations and its effects on human health are gradually being questioned. Under this premise, we attempted to use the natural surfactant tea saponin, which originates from the processing residues of camellia oil, as the additive of the extraction solvent and to extract eleutheroside B and eleutheroside E in the roots and rhizomes of E. senticosus by ultrasonic mediation. After a single-factor experiment, extraction kinetics at different powers and reaction temperatures, and Box-Behnken design optimization, the optimal conditions obtained were 0.3% tea saponin solution as the extraction solvent, 20 mL/g liquid-solid ratio, 250 W ultrasonic irradiation power (43.4 mW/g ultrasonic power density) and 40 min ultrasonic irradiation time. Under optimal conditions, satisfactory yields of eleutheroside B (1.06 ± 0.04 mg/g) and eleutheroside E (2.65 ± 0.12 mg/g) were obtained with semi pilot scale ultrasonic extraction equipment. The experiments showed that compared with the traditional thermal extraction process, the extraction time is significantly reduced at lower operating temperatures.The safety of ethanol in operations and its effects on human health are gradually being questioned. Under this premise, we attempted to use the natural surfactant tea saponin, which originates from the processing residues of camellia oil, as the additive of the extraction solvent and to extract eleutheroside B and eleutheroside E in the roots and rhizomes of E. senticosus by ultrasonic mediation. After a single-factor experiment, extraction kinetics at different powers and reaction temperatures, and Box-Behnken design optimization, the optimal conditions obtained were 0.3% tea saponin solution as the extraction solvent, 20 mL/g liquid-solid ratio, 250 W ultrasonic irradiation power (43.4 mW/g ultrasonic power density) and 40 min ultrasonic irradiation time. Under optimal conditions, satisfactory yields of eleutheroside B (1.06 ± 0.04 mg/g) and eleutheroside E (2.65 ± 0.12 mg/g) were obtained with semi pilot scale ultrasonic extraction equipment. The experiments showed that compared with the traditional thermal extraction process, the extraction time is significantly reduced at lower operating temperatures. •Use ultrasonic-assisted extraction of eleutheroside B and E from E. senticosus.•Tea saponin was first added to extract eleutherosides in the process.•Dynamic models under powers, temperatures were considered.•Determine optimum conditions of eleutheroside B and E by response surface method.•A 200-fold expansion of the semi-pilot test was carried out. The safety of ethanol in operations and its effects on human health are gradually being questioned. Under this premise, we attempted to use the natural surfactant tea saponin, which originates from the processing residues of camellia oil, as the additive of the extraction solvent and to extract eleutheroside B and eleutheroside E in the roots and rhizomes of E. senticosus by ultrasonic mediation. After a single-factor experiment, extraction kinetics at different powers and reaction temperatures, and Box–Behnken design optimization, the optimal conditions obtained were 0.3% tea saponin solution as the extraction solvent, 20 mL/g liquid–solid ratio, 250 W ultrasonic irradiation power (43.4 mW/g ultrasonic power density) and 40 min ultrasonic irradiation time. Under optimal conditions, satisfactory yields of eleutheroside B (1.06 ± 0.04 mg/g) and eleutheroside E (2.65 ± 0.12 mg/g) were obtained with semi pilot scale ultrasonic extraction equipment. The experiments showed that compared with the traditional thermal extraction process, the extraction time is significantly reduced at lower operating temperatures. |
ArticleNumber | 106039 |
Author | Qi, Shuwen Yang, Xinyu Li, Jialei Gu, Huiyan Yang, Lei Liu, Tingting |
Author_xml | – sequence: 1 givenname: Xinyu surname: Yang fullname: Yang, Xinyu organization: Key Laboratory of Forest Plant Ecology, Ministry of Education, Northeast Forestry University, Harbin 150040, China – sequence: 2 givenname: Tingting surname: Liu fullname: Liu, Tingting organization: College of Pharmacy, Qiqihar Medical University, Qiqihar 161006, China – sequence: 3 givenname: Shuwen surname: Qi fullname: Qi, Shuwen organization: Key Laboratory of Forest Plant Ecology, Ministry of Education, Northeast Forestry University, Harbin 150040, China – sequence: 4 givenname: Huiyan surname: Gu fullname: Gu, Huiyan email: hygnefu@126.com organization: School of Forestry, Northeast Forestry University, Harbin 150040, China – sequence: 5 givenname: Jialei surname: Li fullname: Li, Jialei organization: Food Processing Institute, Heilongjiang Academy of Agricultural Sciences, Harbin 150086, China – sequence: 6 givenname: Lei surname: Yang fullname: Yang, Lei email: yanglei@nefu.edu.cn organization: Key Laboratory of Forest Plant Ecology, Ministry of Education, Northeast Forestry University, Harbin 150040, China |
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Keywords | Eleutheroside E Ultrasonic-assisted extraction Eleutheroside B Eleutherococcus senticosus Tea saponin |
Language | English |
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Snippet | •Use ultrasonic-assisted extraction of eleutheroside B and E from E. senticosus.•Tea saponin was first added to extract eleutherosides in the process.•Dynamic... The safety of ethanol in operations and its effects on human health are gradually being questioned. Under this premise, we attempted to use the natural... • Use ultrasonic-assisted extraction of eleutheroside B and E from E. senticosus. • Tea saponin was first added to extract eleutherosides in the process. •... |
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SubjectTerms | Eleutherococcus senticosus Eleutheroside B Eleutheroside E Short Communication Tea saponin Ultrasonic-assisted extraction |
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Title | Tea saponin additive to extract eleutheroside B and E from Eleutherococcus senticosus by ultrasonic mediation and its application in a semi-pilot scale |
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