Crystallization Kinetics of LaF3 Nanocrystals in an Oxyfluoride Glass
Nanocrystallization of LaF3 in a glass of composition 55SiO2–20Al2O3–15Na2O–10LaF3 (mol%) has been achieved by heat treatment above the glass transition temperature. A maximum crystal size of 14 nm has been attained, with the crystalline fraction and crystal size dependent on the time and temperatur...
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Published in | Journal of the American Ceramic Society Vol. 94; no. 8; pp. 2420 - 2428 |
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Main Authors | , , , , , , , , , |
Format | Journal Article |
Language | English |
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Malden, USA
Blackwell Publishing Inc
01.08.2011
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Abstract | Nanocrystallization of LaF3 in a glass of composition 55SiO2–20Al2O3–15Na2O–10LaF3 (mol%) has been achieved by heat treatment above the glass transition temperature. A maximum crystal size of 14 nm has been attained, with the crystalline fraction and crystal size dependent on the time and temperature of thermal treatment. The effect of lanthanum fluoride crystallization is noticeable from the microstructural and compositional changes in the glass matrix, which have been studied using several techniques, including viscosity, dilatometry, X‐ray diffraction, and quantitative Rietveld refinement, transmission electron microscopy, and differential scanning calorimetry. The crystallization mechanism is shown to occur via regions of La‐ and Si‐phase separation in the glass, from which the fluoride crystals develop during heat treatment. The interface between the glass matrix and the crystals in the demixed ranges is enriched in network formers, mainly SiO2, creating a viscous barrier, which inhibits further crystal growth and limits the crystal size to the nanometric range. |
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AbstractList | Nanocrystallization of LaF3 in a glass of composition 55SiO2-20Al2O3-15Na2O-10LaF3 (mol%) has been achieved by heat treatment above the glass transition temperature. A maximum crystal size of 14 nm has been attained, with the crystalline fraction and crystal size dependent on the time and temperature of thermal treatment. The effect of lanthanum fluoride crystallization is noticeable from the microstructural and compositional changes in the glass matrix, which have been studied using several techniques, including viscosity, dilatometry, X-ray diffraction, and quantitative Rietveld refinement, transmission electron microscopy, and differential scanning calorimetry. The crystallization mechanism is shown to occur via regions of La- and Si-phase separation in the glass, from which the fluoride crystals develop during heat treatment. The interface between the glass matrix and the crystals in the demixed ranges is enriched in network formers, mainly SiO2, creating a viscous barrier, which inhibits further crystal growth and limits the crystal size to the nanometric range. Nanocrystallisation of LaF3 in 55SiO2-20Al2O3-15Na2O-10LaF3 (mol%) glass was achieved by heat treatment above the glass transition temperature. A maximum crystal size of 14 nm was attained, with the crystalline fraction and crystal size dependent on the time and temperature of the thermal treatment. The effect of lanthanum fluoride crystallisation was noticeable from the microstructural and compositional changes in the glass matrix, which were studied by viscosity, dilatometry, XRD, Rietveld refinement, TEM, and DSC. The crystallisation mechanism occurred via regions of La- and Si-phase separation in the glass, from which the fluoride crystals developed during heat treatment. The interface between the glass matrix and the crystals in the de-mixed range was enriched with network formers, mainly SiO2, creating a viscous barrier, which inhibited further crystal growth and limited the crystal size to the nanometric range. |
Author | Mather, Glenn C. Muñoz, Francisco Bhattacharyya, Sommnath Deubener, Joachim Durán, Alicia Hémono, Nicolas Bornhöft, Hansjörg de Pablos-Martín, Araceli Höche, Thomas Pascual, Maria J. |
Author_xml | – sequence: 1 givenname: Araceli surname: de Pablos-Martín fullname: de Pablos-Martín, Araceli organization: Instituto de Cerámica y Vidrio (CSIC), Kelsen 5, Madrid 28049, Spain – sequence: 2 givenname: Nicolas surname: Hémono fullname: Hémono, Nicolas organization: Instituto de Cerámica y Vidrio (CSIC), Kelsen 5, Madrid 28049, Spain – sequence: 3 givenname: Glenn C. surname: Mather fullname: Mather, Glenn C. organization: Instituto de Cerámica y Vidrio (CSIC), Kelsen 5, Madrid 28049, Spain – sequence: 4 givenname: Sommnath surname: Bhattacharyya fullname: Bhattacharyya, Sommnath organization: Leibniz-Institut für Oberfläcgenmodifizierung e.V., Permoserstraβe 15, Leipzig D-04318, Germany – sequence: 5 givenname: Thomas surname: Höche fullname: Höche, Thomas organization: Fraunhofer-Institute für Werkstoffmechanik, Walter- Hülse-Straβe 1, D-06120, Halle, Germany – sequence: 6 givenname: Hansjörg surname: Bornhöft fullname: Bornhöft, Hansjörg organization: Institut für Nichtmetallische Werkstoffe, TU-Clausthal, Clausthal-Zellerfeld D-38678, Germany – sequence: 7 givenname: Joachim surname: Deubener fullname: Deubener, Joachim organization: Institut für Nichtmetallische Werkstoffe, TU-Clausthal, Clausthal-Zellerfeld D-38678, Germany – sequence: 8 givenname: Francisco surname: Muñoz fullname: Muñoz, Francisco organization: Instituto de Cerámica y Vidrio (CSIC), Kelsen 5, Madrid 28049, Spain – sequence: 9 givenname: Alicia surname: Durán fullname: Durán, Alicia organization: Instituto de Cerámica y Vidrio (CSIC), Kelsen 5, Madrid 28049, Spain – sequence: 10 givenname: Maria J. surname: Pascual fullname: Pascual, Maria J. email: mpascual@icv.csic.es organization: Instituto de Cerámica y Vidrio (CSIC), Kelsen 5, Madrid 28049, Spain |
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Snippet | Nanocrystallization of LaF3 in a glass of composition 55SiO2–20Al2O3–15Na2O–10LaF3 (mol%) has been achieved by heat treatment above the glass transition... Nanocrystallisation of LaF3 in 55SiO2-20Al2O3-15Na2O-10LaF3 (mol%) glass was achieved by heat treatment above the glass transition temperature. A maximum... Nanocrystallization of LaF3 in a glass of composition 55SiO2-20Al2O3-15Na2O-10LaF3 (mol%) has been achieved by heat treatment above the glass transition... |
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SubjectTerms | Crystallization Crystals Enrichment Glass Heat treatment Lanthanum fluorides Nanocrystals Networks |
Title | Crystallization Kinetics of LaF3 Nanocrystals in an Oxyfluoride Glass |
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