Crosslinked P(VDF‐CTFE)/PS‐COOH nanocomposites for high‐energy‐density capacitor application
High‐capacity or high‐power‐density capacitors are being actively investigated for portable electronics, electric vehicles, and electric power systems. The dielectric nanocomposite with a small loading of carboxylic polystyrene (PS‐COOH) nanoparticles in poly(vinylidene fluoride‐chlorotrifluoroethyl...
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| Published in | Journal of polymer science. Part B, Polymer physics Vol. 54; no. 12; pp. 1160 - 1169 |
|---|---|
| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
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Hoboken
Wiley
15.06.2016
Blackwell Publishing Ltd Wiley Subscription Services, Inc |
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| Abstract | High‐capacity or high‐power‐density capacitors are being actively investigated for portable electronics, electric vehicles, and electric power systems. The dielectric nanocomposite with a small loading of carboxylic polystyrene (PS‐COOH) nanoparticles in poly(vinylidene fluoride‐chlorotrifluoroethylene) [P(VDF‐CTFE)] matrix, followed by chemical crosslinking has been described. Combination of these two methods significantly improved the capacity of electric energy storage at low electric field. Specially, the nanocomposite with 2 wt % nanoparticles and 15 wt % crosslinking agent achieved a dielectric constant of 17.2 and a discharged energy density of 17.5 J/cm³ (4.9 Wh/L) at an electric field as high as 324 MV/m, while corresponding values for pristine P(VDF‐CTFE) are 9.6 and 13.3 J/cm³ (3.7 Wh/L), respectively. Fundamental physics underlying the enhancement in the performance of the nanocomposites with respect to P(VDF‐CTFE) is illustrated by solid‐state ¹⁹F nuclear magnetic resonance of direct excitation or ¹⁹F{¹H} cross polarization. It revealed different dynamics behavior between crystalline/amorphous regions, and PS‐COOH nanoparticles favored the formation of polar γ‐form crystals. Small‐angle X‐ray scattering studies revealed the contribution of the interface to the extraordinary storage of electric energies in the nanocomposites. This approach provided a facile and straightforward way to design or understand PVDF‐based polymers for their practical applications in high‐energy‐density capacitors. © 2016 Wiley Periodicals, Inc. J. Polym. Sci., Part B: Polym. Phys. 2016, 54, 1160–1169 |
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| AbstractList | High-capacity or high-power-density capacitors are being actively investigated for portable electronics, electric vehicles, and electric power systems. The dielectric nanocomposite with a small loading of carboxylic polystyrene (PS-COOH) nanoparticles in poly(vinylidene fluoride-chlorotrifluoroethylene) [P(VDF-CTFE)] matrix, followed by chemical crosslinking has been described. Combination of these two methods significantly improved the capacity of electric energy storage at low electric field. Specially, the nanocomposite with 2 wt % nanoparticles and 15 wt % crosslinking agent achieved a dielectric constant of 17.2 and a discharged energy density of 17.5 J/cm super(3) (4.9 Wh/L) at an electric field as high as 324 MV/m, while corresponding values for pristine P(VDF-CTFE) are 9.6 and 13.3 J/cm super(3) (3.7 Wh/L), respectively. Fundamental physics underlying the enhancement in the performance of the nanocomposites with respect to P(VDF-CTFE) is illustrated by solid-state super(19)F nuclear magnetic resonance of direct excitation or super(1)9{ super(1) H}cross polarization. It revealed different dynamics behavior between crystalline/amorphous regions, and PS-COOH nanoparticles favored the formation of polar gamma -form crystals. Small-angle X-ray scattering studies revealed the contribution of the interface to the extraordinary storage of electric energies in the nanocomposites. This approach provided a facile and straightforward way to design or understand PVDF-based polymers for their practical applications in high-energy-density capacitors. J. Polym. Sci., Part B: Polym. Phys. 2016, 54, 1160-1169 Concurrent improvements in dielectric constant and energy density are attained in the crosslinked nanocomposite incorporated with the PS-COOH nanoparticles, and followed by chemical crosslinking. Fundamental physics underlying the enhancement in the performance of the nanocomposites with respect to P(VDF-CTFE) is illustrated by solid-state super(19)F nuclear magnetic resonance of direct excitation or super(1)9{ super(1) H}cross polarization. High-capacity or high-power-density capacitors are being actively investigated for portable electronics, electric vehicles, and electric power systems. The dielectric nanocomposite with a small loading of carboxylic polystyrene (PS-COOH) nanoparticles in poly(vinylidene fluoride-chlorotrifluoroethylene) [P(VDF-CTFE)] matrix, followed by chemical crosslinking has been described. Combination of these two methods significantly improved the capacity of electric energy storage at low electric field. Specially, the nanocomposite with 2 wt % nanoparticles and 15 wt % crosslinking agent achieved a dielectric constant of 17.2 and a discharged energy density of 17.5 J/cm3 (4.9 Wh/L) at an electric field as high as 324 MV/m, while corresponding values for pristine P(VDF-CTFE) are 9.6 and 13.3 J/cm3 (3.7 Wh/L), respectively. Fundamental physics underlying the enhancement in the performance of the nanocomposites with respect to P(VDF-CTFE) is illustrated by solid-state 19F nuclear magnetic resonance of direct excitation or 19F{1H} cross polarization. It revealed different dynamics behavior between crystalline/amorphous regions, and PS-COOH nanoparticles favored the formation of polar [gamma]-form crystals. Small-angle X-ray scattering studies revealed the contribution of the interface to the extraordinary storage of electric energies in the nanocomposites. This approach provided a facile and straightforward way to design or understand PVDF-based polymers for their practical applications in high-energy-density capacitors. © 2016 Wiley Periodicals, Inc. J. Polym. Sci., Part B: Polym. Phys. 2016, 54, 1160-1169 ABSTRACT High‐capacity or high‐power‐density capacitors are being actively investigated for portable electronics, electric vehicles, and electric power systems. The dielectric nanocomposite with a small loading of carboxylic polystyrene (PS‐COOH) nanoparticles in poly(vinylidene fluoride‐chlorotrifluoroethylene) [P(VDF‐CTFE)] matrix, followed by chemical crosslinking has been described. Combination of these two methods significantly improved the capacity of electric energy storage at low electric field. Specially, the nanocomposite with 2 wt % nanoparticles and 15 wt % crosslinking agent achieved a dielectric constant of 17.2 and a discharged energy density of 17.5 J/cm3 (4.9 Wh/L) at an electric field as high as 324 MV/m, while corresponding values for pristine P(VDF‐CTFE) are 9.6 and 13.3 J/cm3 (3.7 Wh/L), respectively. Fundamental physics underlying the enhancement in the performance of the nanocomposites with respect to P(VDF‐CTFE) is illustrated by solid‐state 19F nuclear magnetic resonance of direct excitation or 19F{1H} cross polarization. It revealed different dynamics behavior between crystalline/amorphous regions, and PS‐COOH nanoparticles favored the formation of polar γ‐form crystals. Small‐angle X‐ray scattering studies revealed the contribution of the interface to the extraordinary storage of electric energies in the nanocomposites. This approach provided a facile and straightforward way to design or understand PVDF‐based polymers for their practical applications in high‐energy‐density capacitors. © 2016 Wiley Periodicals, Inc. J. Polym. Sci., Part B: Polym. Phys. 2016, 54, 1160–1169 Concurrent improvements in dielectric constant and energy density are attained in the crosslinked nanocomposite incorporated with the PS‐COOH nanoparticles, and followed by chemical crosslinking. Fundamental physics underlying the enhancement in the performance of the nanocomposites with respect to P(VDF‐CTFE) is illustrated by solid‐state 19F nuclear magnetic resonance of direct excitation or 19F{1H} cross polarization. High‐capacity or high‐power‐density capacitors are being actively investigated for portable electronics, electric vehicles, and electric power systems. The dielectric nanocomposite with a small loading of carboxylic polystyrene (PS‐COOH) nanoparticles in poly(vinylidene fluoride‐chlorotrifluoroethylene) [P(VDF‐CTFE)] matrix, followed by chemical crosslinking has been described. Combination of these two methods significantly improved the capacity of electric energy storage at low electric field. Specially, the nanocomposite with 2 wt % nanoparticles and 15 wt % crosslinking agent achieved a dielectric constant of 17.2 and a discharged energy density of 17.5 J/cm³ (4.9 Wh/L) at an electric field as high as 324 MV/m, while corresponding values for pristine P(VDF‐CTFE) are 9.6 and 13.3 J/cm³ (3.7 Wh/L), respectively. Fundamental physics underlying the enhancement in the performance of the nanocomposites with respect to P(VDF‐CTFE) is illustrated by solid‐state ¹⁹F nuclear magnetic resonance of direct excitation or ¹⁹F{¹H} cross polarization. It revealed different dynamics behavior between crystalline/amorphous regions, and PS‐COOH nanoparticles favored the formation of polar γ‐form crystals. Small‐angle X‐ray scattering studies revealed the contribution of the interface to the extraordinary storage of electric energies in the nanocomposites. This approach provided a facile and straightforward way to design or understand PVDF‐based polymers for their practical applications in high‐energy‐density capacitors. © 2016 Wiley Periodicals, Inc. J. Polym. Sci., Part B: Polym. Phys. 2016, 54, 1160–1169 |
| Author | Hu, Wenbing Tang, Xin Shen, Qun-Dong Shu, Jie Chen, Yingxin Wang, Xiaoliang |
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| SubjectTerms | Capacitors carboxylic polystyrene nanoparticles Cross polarization crosslinked nanocomposites Crosslinking dielectric permittivity Electric fields Energy density Excitation high-power-density capacitor Nanocomposites Nanoparticles poly(vinylidene fluoride-chlorotrifluoroethylene) |
| Title | Crosslinked P(VDF‐CTFE)/PS‐COOH nanocomposites for high‐energy‐density capacitor application |
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