Structure, properties and potential applications of phytoglycogen and waxy starch subjected to carboxymethylation
•Structure and properties for different CM-starches were investigated.•DS of CM-PG was higher than that of CM-WS under equivalent modification conditions.•The Mw increased for CM-PG with increasing DS whereas Rz was nearly constant.•Carboxymethylation modification resulted in a greater increase of S...
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| Published in | Carbohydrate polymers Vol. 234; p. 115908 |
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| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
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Elsevier Ltd
15.04.2020
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| Abstract | •Structure and properties for different CM-starches were investigated.•DS of CM-PG was higher than that of CM-WS under equivalent modification conditions.•The Mw increased for CM-PG with increasing DS whereas Rz was nearly constant.•Carboxymethylation modification resulted in a greater increase of SDS and RS.•Tailor-made CM-PG can be used as a potential carrier for bioactive ingredients.
The structure and properties of phytoglycogen (PG) and waxy starch (WS) from different mutants subjected to carboxymethylation (CM) were investigated. FT-IR analysis confirmed the carboxymethylation of PG and WS. The degree of substitution (DS) increased with increasing of the ratio of monochloroacetic acid to anhydroglucose unit, while DS of CM-PG was higher than that of CM-WS using equivalent modification conditions. The weight-average molecular weight (Mw) and radius of gyration (Rz) of CM-WS increased with the DS, whereas the Mw increased and Rz was nearly constant for CM-PG. The zeta-potential of CM-WS reduced and the viscosity increased significantly as DS increased, while the viscosity of CM-PG was remarkably lower than that of CM-WS with equivalent of DS. The increase of DS in CM-starches resulted in a substantial reduction of RDS accompanied by the increase of SDS and RS. The results revealed the promising application of CM-PG as a potential carrier system for bioactive ingredients. |
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| AbstractList | The structure and properties of phytoglycogen (PG) and waxy starch (WS) from different mutants subjected to carboxymethylation (CM) were investigated. FT-IR analysis confirmed the carboxymethylation of PG and WS. The degree of substitution (DS) increased with increasing of the ratio of monochloroacetic acid to anhydroglucose unit, while DS of CM-PG was higher than that of CM-WS using equivalent modification conditions. The weight-average molecular weight (Mw) and radius of gyration (Rz) of CM-WS increased with the DS, whereas the Mw increased and Rz was nearly constant for CM-PG. The zeta-potential of CM-WS reduced and the viscosity increased significantly as DS increased, while the viscosity of CM-PG was remarkably lower than that of CM-WS with equivalent of DS. The increase of DS in CM-starches resulted in a substantial reduction of RDS accompanied by the increase of SDS and RS. The results revealed the promising application of CM-PG as a potential carrier system for bioactive ingredients. •Structure and properties for different CM-starches were investigated.•DS of CM-PG was higher than that of CM-WS under equivalent modification conditions.•The Mw increased for CM-PG with increasing DS whereas Rz was nearly constant.•Carboxymethylation modification resulted in a greater increase of SDS and RS.•Tailor-made CM-PG can be used as a potential carrier for bioactive ingredients. The structure and properties of phytoglycogen (PG) and waxy starch (WS) from different mutants subjected to carboxymethylation (CM) were investigated. FT-IR analysis confirmed the carboxymethylation of PG and WS. The degree of substitution (DS) increased with increasing of the ratio of monochloroacetic acid to anhydroglucose unit, while DS of CM-PG was higher than that of CM-WS using equivalent modification conditions. The weight-average molecular weight (Mw) and radius of gyration (Rz) of CM-WS increased with the DS, whereas the Mw increased and Rz was nearly constant for CM-PG. The zeta-potential of CM-WS reduced and the viscosity increased significantly as DS increased, while the viscosity of CM-PG was remarkably lower than that of CM-WS with equivalent of DS. The increase of DS in CM-starches resulted in a substantial reduction of RDS accompanied by the increase of SDS and RS. The results revealed the promising application of CM-PG as a potential carrier system for bioactive ingredients. The structure and properties of phytoglycogen (PG) and waxy starch (WS) from different mutants subjected to carboxymethylation (CM) were investigated. FT-IR analysis confirmed the carboxymethylation of PG and WS. The degree of substitution (DS) increased with increasing of the ratio of monochloroacetic acid to anhydroglucose unit, while DS of CM-PG was higher than that of CM-WS using equivalent modification conditions. The weight-average molecular weight (Mw) and radius of gyration (R ) of CM-WS increased with the DS, whereas the Mw increased and R was nearly constant for CM-PG. The zeta-potential of CM-WS reduced and the viscosity increased significantly as DS increased, while the viscosity of CM-PG was remarkably lower than that of CM-WS with equivalent of DS. The increase of DS in CM-starches resulted in a substantial reduction of RDS accompanied by the increase of SDS and RS. The results revealed the promising application of CM-PG as a potential carrier system for bioactive ingredients. The structure and properties of phytoglycogen (PG) and waxy starch (WS) from different mutants subjected to carboxymethylation (CM) were investigated. FT-IR analysis confirmed the carboxymethylation of PG and WS. The degree of substitution (DS) increased with increasing of the ratio of monochloroacetic acid to anhydroglucose unit, while DS of CM-PG was higher than that of CM-WS using equivalent modification conditions. The weight-average molecular weight (Mw) and radius of gyration (Rz) of CM-WS increased with the DS, whereas the Mw increased and Rz was nearly constant for CM-PG. The zeta-potential of CM-WS reduced and the viscosity increased significantly as DS increased, while the viscosity of CM-PG was remarkably lower than that of CM-WS with equivalent of DS. The increase of DS in CM-starches resulted in a substantial reduction of RDS accompanied by the increase of SDS and RS. The results revealed the promising application of CM-PG as a potential carrier system for bioactive ingredients.The structure and properties of phytoglycogen (PG) and waxy starch (WS) from different mutants subjected to carboxymethylation (CM) were investigated. FT-IR analysis confirmed the carboxymethylation of PG and WS. The degree of substitution (DS) increased with increasing of the ratio of monochloroacetic acid to anhydroglucose unit, while DS of CM-PG was higher than that of CM-WS using equivalent modification conditions. The weight-average molecular weight (Mw) and radius of gyration (Rz) of CM-WS increased with the DS, whereas the Mw increased and Rz was nearly constant for CM-PG. The zeta-potential of CM-WS reduced and the viscosity increased significantly as DS increased, while the viscosity of CM-PG was remarkably lower than that of CM-WS with equivalent of DS. The increase of DS in CM-starches resulted in a substantial reduction of RDS accompanied by the increase of SDS and RS. The results revealed the promising application of CM-PG as a potential carrier system for bioactive ingredients. |
| ArticleNumber | 115908 |
| Author | Miao, Ming Liu, Yao Hu, Xiuting Jin, Zhengyu Lu, Keyu |
| Author_xml | – sequence: 1 givenname: Yao surname: Liu fullname: Liu, Yao – sequence: 2 givenname: Keyu surname: Lu fullname: Lu, Keyu – sequence: 3 givenname: Xiuting surname: Hu fullname: Hu, Xiuting – sequence: 4 givenname: Zhengyu surname: Jin fullname: Jin, Zhengyu – sequence: 5 givenname: Ming orcidid: 0000-0001-8389-1125 surname: Miao fullname: Miao, Ming email: miaoming@jiangnan.edu.cn |
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| Keywords | Degradation Phytoglycogen Waxy starch Carboxymethylation Carrier Structure |
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| Snippet | •Structure and properties for different CM-starches were investigated.•DS of CM-PG was higher than that of CM-WS under equivalent modification conditions.•The... The structure and properties of phytoglycogen (PG) and waxy starch (WS) from different mutants subjected to carboxymethylation (CM) were investigated. FT-IR... |
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| SubjectTerms | Carboxymethylation Carrier Degradation Fourier transform infrared spectroscopy ingredients molecular weight monochloroacetic acid mutants Phytoglycogen Structure viscosity Waxy starch zeta potential |
| Title | Structure, properties and potential applications of phytoglycogen and waxy starch subjected to carboxymethylation |
| URI | https://dx.doi.org/10.1016/j.carbpol.2020.115908 https://www.ncbi.nlm.nih.gov/pubmed/32070527 https://www.proquest.com/docview/2358599004 https://www.proquest.com/docview/2440696883 |
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