Epitaxial growth and lithium ion conductivity of lithium-oxide garnet for an all solid-state battery electrolyte
Epitaxial thin films of Al-doped Li7La3Zr2O12 (LLZO) with a cubic garnet-type structure were successfully synthesized using pulsed laser deposition to investigate the lithium ion conduction in grains. Two orientations of the films were obtained depending on the Gd3Ga5O12 (GGG) substrate orientation,...
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| Published in | Dalton transactions : an international journal of inorganic chemistry Vol. 42; no. 36; pp. 13112 - 13117 |
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| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
England
28.09.2013
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| Abstract | Epitaxial thin films of Al-doped Li7La3Zr2O12 (LLZO) with a cubic garnet-type structure were successfully synthesized using pulsed laser deposition to investigate the lithium ion conduction in grains. Two orientations of the films were obtained depending on the Gd3Ga5O12 (GGG) substrate orientation, LLZO(001)/GGG(001) and LLZO(111)/GGG(111). The ionic conductivities in the grains of the (001) and (111) films were 2.5 × 10(-6) and 1.0 × 10(-5) S cm(-1) at 298 K, respectively, which were lower than those of polycrystalline LLZO of over 10(-4) S cm(-1). X-ray reflectometry and inductively coupled plasma mass spectrometry revealed a large amount of Al(3+) of over 0.6 moles substituted for Li(+). These results indicate that the Al(3+) substitution in the LLZO lattice decreases the number of movable lithium ions and blocks the three-dimensional lithium migration pathway. The lattice mismatch between the film and the substrate induced the lattice distortion of the LLZO, resulting in different conductivities between the (001) and (111) films. The epitaxial-film model system directly clarified a substantial impact of the Al substitution and the lattice distortion on the lithium ion conductivity in the LLZO. |
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| AbstractList | Epitaxial thin films of Al-doped Li7La3Zr2O12 (LLZO) with a cubic garnet-type structure were successfully synthesized using pulsed laser deposition to investigate the lithium ion conduction in grains. Two orientations of the films were obtained depending on the Gd3Ga5O12 (GGG) substrate orientation, LLZO(001)/GGG(001) and LLZO(111)/GGG(111). The ionic conductivities in the grains of the (001) and (111) films were 2.5 × 10(-6) and 1.0 × 10(-5) S cm(-1) at 298 K, respectively, which were lower than those of polycrystalline LLZO of over 10(-4) S cm(-1). X-ray reflectometry and inductively coupled plasma mass spectrometry revealed a large amount of Al(3+) of over 0.6 moles substituted for Li(+). These results indicate that the Al(3+) substitution in the LLZO lattice decreases the number of movable lithium ions and blocks the three-dimensional lithium migration pathway. The lattice mismatch between the film and the substrate induced the lattice distortion of the LLZO, resulting in different conductivities between the (001) and (111) films. The epitaxial-film model system directly clarified a substantial impact of the Al substitution and the lattice distortion on the lithium ion conductivity in the LLZO. Epitaxial thin films of Al-doped Li sub(7)La sub(3)Zr sub(2)O sub(12) (LLZO) with a cubic garnet-type structure were successfully synthesized using pulsed laser deposition to investigate the lithium ion conduction in grains. Two orientations of the films were obtained depending on the Gd sub(3)Ga sub(5)O sub(12) (GGG) substrate orientation, LLZO(001)/GGG(001) and LLZO(111)/GGG(111). The ionic conductivities in the grains of the (001) and (111) films were 2.5 10 super(-6) and 1.0 10 super(-5) S cm super(-1) at 298 K, respectively, which were lower than those of polycrystalline LLZO of over 10 super(-4) S cm super(-1). X-ray reflectometry and inductively coupled plasma mass spectrometry revealed a large amount of Al super(3+) of over 0.6 moles substituted for Li super(+). These results indicate that the Al super(3+) substitution in the LLZO lattice decreases the number of movable lithium ions and blocks the three-dimensional lithium migration pathway. The lattice mismatch between the film and the substrate induced the lattice distortion of the LLZO, resulting in different conductivities between the (001) and (111) films. The epitaxial-film model system directly clarified a substantial impact of the Al substitution and the lattice distortion on the lithium ion conductivity in the LLZO. |
| Author | Taminato, Sou Kim, Sangryun Hirayama, Masaaki Kanno, Ryoji |
| Author_xml | – sequence: 1 givenname: Sangryun surname: Kim fullname: Kim, Sangryun email: hirayama@echem.titech.ac.jp organization: Department of Electronic Chemistry, Interdisciplinary Graduate School of Science and Engineering, Tokyo Institute of Technology, 4259 Nagatsuta, Midori-ku, Yokohama 225-8502, Japan. hirayama@echem.titech.ac.jp – sequence: 2 givenname: Masaaki surname: Hirayama fullname: Hirayama, Masaaki – sequence: 3 givenname: Sou surname: Taminato fullname: Taminato, Sou – sequence: 4 givenname: Ryoji surname: Kanno fullname: Kanno, Ryoji |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/23877300$$D View this record in MEDLINE/PubMed |
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| Snippet | Epitaxial thin films of Al-doped Li7La3Zr2O12 (LLZO) with a cubic garnet-type structure were successfully synthesized using pulsed laser deposition to... Epitaxial thin films of Al-doped Li sub(7)La sub(3)Zr sub(2)O sub(12) (LLZO) with a cubic garnet-type structure were successfully synthesized using pulsed... |
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| SubjectTerms | Aluminum Distortion Epitaxy Grains Lattices Lithium Orientation Three dimensional |
| Title | Epitaxial growth and lithium ion conductivity of lithium-oxide garnet for an all solid-state battery electrolyte |
| URI | https://www.ncbi.nlm.nih.gov/pubmed/23877300 https://search.proquest.com/docview/1427007414 https://search.proquest.com/docview/1567064100 https://search.proquest.com/docview/1730097535 |
| Volume | 42 |
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| linkProvider | Royal Society of Chemistry |
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