Retention behavior of isomeric polycyclic aromatic sulfur heterocycles in gas chromatography on stationary phases of different selectivity
•GC retention indices for 48 PASHs.•Detailed comparison of three GC stationary phases with different selectivities for PASHs.•First reported separations of PASH isomers via GC on a 50% liquid crystalline DMPS phase.•Correlations are presented between the GC retention of PASHs and their L/B. Retentio...
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| Published in | Journal of Chromatography A Vol. 1485; pp. 120 - 130 |
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| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
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17.02.2017
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| Abstract | •GC retention indices for 48 PASHs.•Detailed comparison of three GC stationary phases with different selectivities for PASHs.•First reported separations of PASH isomers via GC on a 50% liquid crystalline DMPS phase.•Correlations are presented between the GC retention of PASHs and their L/B.
Retention indices for 48 polycyclic aromatic sulfur heterocycles (PASHs) were determined using gas chromatography with three different stationary phases: a 50% phenyl phase, a 50% liquid crystalline dimethylpolysiloxane (LC-DMPS) phase, and an ionic liquid (IL) phase. Correlations between the retention behavior on the three stationary phases and PASH geometry (L/B and T, i.e., length-to-breadth ratio and thickness, respectively) were investigated for the following four isomer sets: (1) 4 three-ring molecular mass (MM) 184Da PASHs, (2) 13 four-ring MM 234Da PASHs, (3) 10 five-ring MM 258Da PASHs, and (4) 20 five-ring MM 284Da PASHs. Correlation coefficients for retention on the 50% LC-DMPS vs L/B ranged from r=0.50 (MM 284Da) to r=0.77 (MM 234Da). Correlation coefficients for retention on the IL phase vs L/B ranged from r=0.31 (MM 234Da) to r=0.54 (MM 284Da). Correlation coefficients for retention on the 50% phenyl vs L/B ranged from r=0.14 (MM 258Da) to r=0.59 (MM 284Da). Several correlation trends are discussed in detail for the retention behavior of PASH on the three stationary phases. |
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| AbstractList | Retention indices for 48 polycyclic aromatic sulfur heterocycles (PASHs) were determined using gas chromatography with three different stationary phases: a 50% phenyl phase, a 50% liquid crystalline dimethylpolysiloxane (LC-DMPS) phase, and an ionic liquid (IL) phase. Correlations between the retention behavior on the three stationary phases and PASH geometry (
L/B
and
T
, i.e., length-to-breadth ratio and thickness, respectively) were investigated for the following four isomer sets: (1) 4 three-ring molecular mass (MM) 184 Da PASHs, (2) 13 four-ring MM 234 Da PASHs, (3) 10 five-ring MM 258 Da PASHs, and (4) 20 five-ring MM 284 Da PASHs. Correlation coefficients for retention on the 50% LC-DMPS vs
L/B
ranged from
r
= 0.50 (MM 284 Da) to
r
= 0.77 (MM 234 Da). Correlation coefficients for retention on the IL phase vs
L/B
ranged from
r
= 0.31 (MM 234 Da) to
r
= 0.54 (MM 284 Da). Correlation coefficients for retention on the 50% phenyl vs
L/B
ranged from
r
= 0.14 (MM 258 Da) to
r
= 0.59 (MM 284 Da). Several correlation trends are discussed in detail for the retention behavior of PASH on the three stationary phases. Retention indices for 48 polycyclic aromatic sulfur heterocycles (PASHs) were determined using gas chromatography with three different stationary phases: a 50% phenyl phase, a 50% liquid crystalline dimethylpolysiloxane (LC-DMPS) phase, and an ionic liquid (IL) phase. Correlations between the retention behavior on the three stationary phases and PASH geometry (L/B and T, i.e., length-to-breadth ratio and thickness, respectively) were investigated for the following four isomer sets: (1) 4 three-ring molecular mass (MM) 184Da PASHs, (2) 13 four-ring MM 234Da PASHs, (3) 10 five-ring MM 258Da PASHs, and (4) 20 five-ring MM 284Da PASHs. Correlation coefficients for retention on the 50% LC-DMPS vs L/B ranged from r=0.50 (MM 284Da) to r=0.77 (MM 234Da). Correlation coefficients for retention on the IL phase vs L/B ranged from r=0.31 (MM 234Da) to r=0.54 (MM 284Da). Correlation coefficients for retention on the 50% phenyl vs L/B ranged from r=0.14 (MM 258Da) to r=0.59 (MM 284Da). Several correlation trends are discussed in detail for the retention behavior of PASH on the three stationary phases. •GC retention indices for 48 PASHs.•Detailed comparison of three GC stationary phases with different selectivities for PASHs.•First reported separations of PASH isomers via GC on a 50% liquid crystalline DMPS phase.•Correlations are presented between the GC retention of PASHs and their L/B. Retention indices for 48 polycyclic aromatic sulfur heterocycles (PASHs) were determined using gas chromatography with three different stationary phases: a 50% phenyl phase, a 50% liquid crystalline dimethylpolysiloxane (LC-DMPS) phase, and an ionic liquid (IL) phase. Correlations between the retention behavior on the three stationary phases and PASH geometry (L/B and T, i.e., length-to-breadth ratio and thickness, respectively) were investigated for the following four isomer sets: (1) 4 three-ring molecular mass (MM) 184Da PASHs, (2) 13 four-ring MM 234Da PASHs, (3) 10 five-ring MM 258Da PASHs, and (4) 20 five-ring MM 284Da PASHs. Correlation coefficients for retention on the 50% LC-DMPS vs L/B ranged from r=0.50 (MM 284Da) to r=0.77 (MM 234Da). Correlation coefficients for retention on the IL phase vs L/B ranged from r=0.31 (MM 234Da) to r=0.54 (MM 284Da). Correlation coefficients for retention on the 50% phenyl vs L/B ranged from r=0.14 (MM 258Da) to r=0.59 (MM 284Da). Several correlation trends are discussed in detail for the retention behavior of PASH on the three stationary phases. |
| Author | Lee, Milton L. Mössner, Stephanie G. Oña-Ruales, Jorge O. Sander, Lane C. Sidisky, Leonard M. Wilson, Walter B. Wise, Stephen A. |
| AuthorAffiliation | d Department of Chemistry and Biochemistry, Brigham Young University, Provo, Utah 84602 a Chemical Sciences Division, Material Measurement Laboratory, National Institute of Standards and Technology, Gaithersburg, Maryland 20899 c MilliporeSigma, A business of Merck KGaA, Bellefonte, Pennsylvania 16823 |
| AuthorAffiliation_xml | – name: d Department of Chemistry and Biochemistry, Brigham Young University, Provo, Utah 84602 – name: c MilliporeSigma, A business of Merck KGaA, Bellefonte, Pennsylvania 16823 – name: a Chemical Sciences Division, Material Measurement Laboratory, National Institute of Standards and Technology, Gaithersburg, Maryland 20899 |
| Author_xml | – sequence: 1 givenname: Walter B. surname: Wilson fullname: Wilson, Walter B. email: walter.wilson@nist.gov organization: Chemical Sciences Division, Material Measurement Laboratory, National Institute of Standards and Technology, Gaithersburg, MD 20899, United States – sequence: 2 givenname: Lane C. surname: Sander fullname: Sander, Lane C. organization: Chemical Sciences Division, Material Measurement Laboratory, National Institute of Standards and Technology, Gaithersburg, MD 20899, United States – sequence: 3 givenname: Jorge O. surname: Oña-Ruales fullname: Oña-Ruales, Jorge O. organization: Chemical Sciences Division, Material Measurement Laboratory, National Institute of Standards and Technology, Gaithersburg, MD 20899, United States – sequence: 4 givenname: Stephanie G. surname: Mössner fullname: Mössner, Stephanie G. organization: Chemical Sciences Division, Material Measurement Laboratory, National Institute of Standards and Technology, Gaithersburg, MD 20899, United States – sequence: 5 givenname: Leonard M. surname: Sidisky fullname: Sidisky, Leonard M. organization: MilliporeSigma, A business of Merck KGaA, Bellefonte, PA 16823, United States – sequence: 6 givenname: Milton L. surname: Lee fullname: Lee, Milton L. organization: Department of Chemistry and Biochemistry, Brigham Young University, Provo, UT 84602, United States – sequence: 7 givenname: Stephen A. surname: Wise fullname: Wise, Stephen A. organization: Chemical Sciences Division, Material Measurement Laboratory, National Institute of Standards and Technology, Gaithersburg, MD 20899, United States |
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| Notes | Current Address: Department of Chemical Engineering, Nazarbayev University, Astana, Kazakhstan 010000. |
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| Snippet | •GC retention indices for 48 PASHs.•Detailed comparison of three GC stationary phases with different selectivities for PASHs.•First reported separations of... Retention indices for 48 polycyclic aromatic sulfur heterocycles (PASHs) were determined using gas chromatography with three different stationary phases: a 50%... |
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| SubjectTerms | Chromatography, Gas - methods Dimethylpolysiloxanes Heterocyclic Compounds, 3-Ring - chemistry Heterocyclic Compounds, 4 or More Rings - chemistry Ionic Liquids Isomerism Molecular Weight Thiophenes - chemistry |
| Title | Retention behavior of isomeric polycyclic aromatic sulfur heterocycles in gas chromatography on stationary phases of different selectivity |
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