Evolution of nanoporosity in organic-rich shales during thermal maturation

•Laboratory-matured shale samples were produced by an anhydrous pyrolysis experiment.•Low-pressure gas adsorption was used to characterize the pore structure of laboratory-matured shales.•There are substantial differences in evolution of nanoporosity between organic-rich and organic-poor samples.•Ev...

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Bibliographic Details
Published in	Fuel (Guildford) Vol. 129; pp. 173 - 181
Main Authors	Chen, Ji, Xiao, Xianming
Format	Journal Article
Language	English
Published	Kidlington Elsevier Ltd 01.08.2014 Elsevier
Subjects	Anhydrous pyrolysis Applied sciences Carbon dioxide Energy Energy. Thermal use of fuels Equivalence Evolution Exact sciences and technology Fuels Gas shale Nanoporosity evolution Nanostructure Natural gas Porosity Reflectivity Shale Thermal maturation Anhydrous pyrolysis Thermal maturation Nanoporosity evolution Gas shale Pyrolysis Shale
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Abstract	•Laboratory-matured shale samples were produced by an anhydrous pyrolysis experiment.•Low-pressure gas adsorption was used to characterize the pore structure of laboratory-matured shales.•There are substantial differences in evolution of nanoporosity between organic-rich and organic-poor samples.•Evolution of organic matter-hosted nanopores of gas shales can be roughly divided into three stages. Artificial shale samples with equivalent vitrinite reflectance values (VRo) ranging from 0.69% to 4.19% were obtained from an anhydrous pyrolysis experiment. Microporous and mesoporous characteristics of these samples were investigated by low-pressure nitrogen and carbon dioxide adsorption techniques. The result shows that the nanoporosity (microporosity plus mesoporosity) increases with thermal maturity after the oil window stage, and this increase is attributed to the formation of porosity within organic matter and/or mineral–organic matter groundmass, rather than in the pure clay minerals. By combining the gas generation and porosity evolution of these shales, a general model for formation and development of the nanoporosity is proposed.
AbstractList	•Laboratory-matured shale samples were produced by an anhydrous pyrolysis experiment.•Low-pressure gas adsorption was used to characterize the pore structure of laboratory-matured shales.•There are substantial differences in evolution of nanoporosity between organic-rich and organic-poor samples.•Evolution of organic matter-hosted nanopores of gas shales can be roughly divided into three stages. Artificial shale samples with equivalent vitrinite reflectance values (VRo) ranging from 0.69% to 4.19% were obtained from an anhydrous pyrolysis experiment. Microporous and mesoporous characteristics of these samples were investigated by low-pressure nitrogen and carbon dioxide adsorption techniques. The result shows that the nanoporosity (microporosity plus mesoporosity) increases with thermal maturity after the oil window stage, and this increase is attributed to the formation of porosity within organic matter and/or mineral–organic matter groundmass, rather than in the pure clay minerals. By combining the gas generation and porosity evolution of these shales, a general model for formation and development of the nanoporosity is proposed. Artificial shale samples with equivalent vitrinite reflectance values (VRo) ranging from 0.69% to 4.19% were obtained from an anhydrous pyrolysis experiment. Microporous and mesoporous characteristics of these samples were investigated by low-pressure nitrogen and carbon dioxide adsorption techniques. The result shows that the nanoporosity (microporosity plus mesoporosity) increases with thermal maturity after the oil window stage, and this increase is attributed to the formation of porosity within organic matter and/or mineral-organic matter groundmass, rather than in the pure clay minerals. By combining the gas generation and porosity evolution of these shales, a general model for formation and development of the nanoporosity is proposed.
Author	Xiao, Xianming Chen, Ji
Author_xml	– sequence: 1 givenname: Ji surname: Chen fullname: Chen, Ji organization: State Key Laboratory of Organic Geochemistry, Guangzhou Institute of Geochemistry, Chinese Academy of Sciences, Guangzhou 510640, China – sequence: 2 givenname: Xianming surname: Xiao fullname: Xiao, Xianming email: xmxiao@gig.ac.cn organization: State Key Laboratory of Organic Geochemistry, Guangzhou Institute of Geochemistry, Chinese Academy of Sciences, Guangzhou 510640, China
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Snippet	•Laboratory-matured shale samples were produced by an anhydrous pyrolysis experiment.•Low-pressure gas adsorption was used to characterize the pore structure... Artificial shale samples with equivalent vitrinite reflectance values (VRo) ranging from 0.69% to 4.19% were obtained from an anhydrous pyrolysis experiment....
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StartPage	173
SubjectTerms	Anhydrous pyrolysis Applied sciences Carbon dioxide Energy Energy. Thermal use of fuels Equivalence Evolution Exact sciences and technology Fuels Gas shale Nanoporosity evolution Nanostructure Natural gas Porosity Reflectivity Shale Thermal maturation
Title	Evolution of nanoporosity in organic-rich shales during thermal maturation
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