Preparation of hybrid paper electrode based on hexagonal boron nitride integrated graphene nanocomposite for free-standing flexible supercapacitors
Flexible energy storage devices have received great interest due to the increasing demand for wearable and flexible electronic devices with high-power energy sources. Herein, a novel hybrid flexible hexagonal boron nitride integrated graphene paper (BN/GrP) is fabricated from 2D hexagonal boron nitr...
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| Published in | RSC advances Vol. 11; no. 6; pp. 3445 - 3451 |
|---|---|
| Main Authors | , , |
| Format | Journal Article |
| Language | English |
| Published |
England
Royal Society of Chemistry
15.01.2021
The Royal Society of Chemistry |
| Subjects | |
| Online Access | Get full text |
| ISSN | 2046-2069 2046-2069 |
| DOI | 10.1039/d0ra10735b |
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| Abstract | Flexible energy storage devices have received great interest due to the increasing demand for wearable and flexible electronic devices with high-power energy sources. Herein, a novel hybrid flexible hexagonal boron nitride integrated graphene paper (BN/GrP) is fabricated from 2D hexagonal boron nitride (h-BN) nanosheets integrated with graphene sheets dispersion
via
a simple vacuum filtration method. FE-SEM indicated that layered graphene nanosheets tightly confined with h-BN nanosheets. Further, the Raman spectroscopy confirmed successful integration of BN with graphene. As-prepared BN/GrP free-standing flexible conductive paper showed high electrical conductivity of 5.36 × 10
4
S m
−1
with the sheet resistance of 8.87 Ω sq
−1
. However, after 1000 continuous bending cycles, the BN/GrP sheet resistance increased just about 8.7% which indicated good flexibility of the paper. Furthermore, as-prepared BN/GrP showed excellent specific capacitance of 321.95 F g
−1
at current density of 0.5 A g
−1
. In addition, the power and energy densities were obtained as 3588.3 W kg
−1
, and 44.7 W h kg
−1
, respectively. The stability of the prepared flexible electrode was tested in galvanostatic charge/discharge cycles, where the results showed the 96.3% retention even after 6000 cycles. These results exhibited that the proposed BN/GrP may be useful to prepare flexible energy-storage systems.
As-prepared BN/GrP free-standing flexible conductive paper showed high electrical conductivity of 5.36 × 10
4
S m
−1
with the sheet resistance of 8.87 Ω sq
−1
. Furthermore, BN/GrP showed excellent specific capacitance of 321.95 F g
−1
at current density of 0.5 A g
−1
. In addition, the power and energy densities were obtained as 3588.3 W kg
−1
, and 44.7 W h kg
−1
. |
|---|---|
| AbstractList | Flexible energy storage devices have received great interest due to the increasing demand for wearable and flexible electronic devices with high-power energy sources. Herein, a novel hybrid flexible hexagonal boron nitride integrated graphene paper (BN/GrP) is fabricated from 2D hexagonal boron nitride (h-BN) nanosheets integrated with graphene sheets dispersion via a simple vacuum filtration method. FE-SEM indicated that layered graphene nanosheets tightly confined with h-BN nanosheets. Further, the Raman spectroscopy confirmed successful integration of BN with graphene. As-prepared BN/GrP free-standing flexible conductive paper showed high electrical conductivity of 5.36 × 10⁴ S m⁻¹ with the sheet resistance of 8.87 Ω sq⁻¹. However, after 1000 continuous bending cycles, the BN/GrP sheet resistance increased just about 8.7% which indicated good flexibility of the paper. Furthermore, as-prepared BN/GrP showed excellent specific capacitance of 321.95 F g⁻¹ at current density of 0.5 A g⁻¹. In addition, the power and energy densities were obtained as 3588.3 W kg⁻¹, and 44.7 W h kg⁻¹, respectively. The stability of the prepared flexible electrode was tested in galvanostatic charge/discharge cycles, where the results showed the 96.3% retention even after 6000 cycles. These results exhibited that the proposed BN/GrP may be useful to prepare flexible energy-storage systems. Flexible energy storage devices have received great interest due to the increasing demand for wearable and flexible electronic devices with high-power energy sources. Herein, a novel hybrid flexible hexagonal boron nitride integrated graphene paper (BN/GrP) is fabricated from 2D hexagonal boron nitride (h-BN) nanosheets integrated with graphene sheets dispersion a simple vacuum filtration method. FE-SEM indicated that layered graphene nanosheets tightly confined with h-BN nanosheets. Further, the Raman spectroscopy confirmed successful integration of BN with graphene. As-prepared BN/GrP free-standing flexible conductive paper showed high electrical conductivity of 5.36 × 10 S m with the sheet resistance of 8.87 Ω sq . However, after 1000 continuous bending cycles, the BN/GrP sheet resistance increased just about 8.7% which indicated good flexibility of the paper. Furthermore, as-prepared BN/GrP showed excellent specific capacitance of 321.95 F g at current density of 0.5 A g . In addition, the power and energy densities were obtained as 3588.3 W kg , and 44.7 W h kg , respectively. The stability of the prepared flexible electrode was tested in galvanostatic charge/discharge cycles, where the results showed the 96.3% retention even after 6000 cycles. These results exhibited that the proposed BN/GrP may be useful to prepare flexible energy-storage systems. Flexible energy storage devices have received great interest due to the increasing demand for wearable and flexible electronic devices with high-power energy sources. Herein, a novel hybrid flexible hexagonal boron nitride integrated graphene paper (BN/GrP) is fabricated from 2D hexagonal boron nitride (h-BN) nanosheets integrated with graphene sheets dispersion via a simple vacuum filtration method. FE-SEM indicated that layered graphene nanosheets tightly confined with h-BN nanosheets. Further, the Raman spectroscopy confirmed successful integration of BN with graphene. As-prepared BN/GrP free-standing flexible conductive paper showed high electrical conductivity of 5.36 × 10 4 S m −1 with the sheet resistance of 8.87 Ω sq −1 . However, after 1000 continuous bending cycles, the BN/GrP sheet resistance increased just about 8.7% which indicated good flexibility of the paper. Furthermore, as-prepared BN/GrP showed excellent specific capacitance of 321.95 F g −1 at current density of 0.5 A g −1 . In addition, the power and energy densities were obtained as 3588.3 W kg −1 , and 44.7 W h kg −1 , respectively. The stability of the prepared flexible electrode was tested in galvanostatic charge/discharge cycles, where the results showed the 96.3% retention even after 6000 cycles. These results exhibited that the proposed BN/GrP may be useful to prepare flexible energy-storage systems. As-prepared BN/GrP free-standing flexible conductive paper showed high electrical conductivity of 5.36 × 10 4 S m −1 with the sheet resistance of 8.87 Ω sq −1 . Furthermore, BN/GrP showed excellent specific capacitance of 321.95 F g −1 at current density of 0.5 A g −1 . In addition, the power and energy densities were obtained as 3588.3 W kg −1 , and 44.7 W h kg −1 . Flexible energy storage devices have received great interest due to the increasing demand for wearable and flexible electronic devices with high-power energy sources. Herein, a novel hybrid flexible hexagonal boron nitride integrated graphene paper (BN/GrP) is fabricated from 2D hexagonal boron nitride (h-BN) nanosheets integrated with graphene sheets dispersion via a simple vacuum filtration method. FE-SEM indicated that layered graphene nanosheets tightly confined with h-BN nanosheets. Further, the Raman spectroscopy confirmed successful integration of BN with graphene. As-prepared BN/GrP free-standing flexible conductive paper showed high electrical conductivity of 5.36 × 104 S m-1 with the sheet resistance of 8.87 Ω sq-1. However, after 1000 continuous bending cycles, the BN/GrP sheet resistance increased just about 8.7% which indicated good flexibility of the paper. Furthermore, as-prepared BN/GrP showed excellent specific capacitance of 321.95 F g-1 at current density of 0.5 A g-1. In addition, the power and energy densities were obtained as 3588.3 W kg-1, and 44.7 W h kg-1, respectively. The stability of the prepared flexible electrode was tested in galvanostatic charge/discharge cycles, where the results showed the 96.3% retention even after 6000 cycles. These results exhibited that the proposed BN/GrP may be useful to prepare flexible energy-storage systems.Flexible energy storage devices have received great interest due to the increasing demand for wearable and flexible electronic devices with high-power energy sources. Herein, a novel hybrid flexible hexagonal boron nitride integrated graphene paper (BN/GrP) is fabricated from 2D hexagonal boron nitride (h-BN) nanosheets integrated with graphene sheets dispersion via a simple vacuum filtration method. FE-SEM indicated that layered graphene nanosheets tightly confined with h-BN nanosheets. Further, the Raman spectroscopy confirmed successful integration of BN with graphene. As-prepared BN/GrP free-standing flexible conductive paper showed high electrical conductivity of 5.36 × 104 S m-1 with the sheet resistance of 8.87 Ω sq-1. However, after 1000 continuous bending cycles, the BN/GrP sheet resistance increased just about 8.7% which indicated good flexibility of the paper. Furthermore, as-prepared BN/GrP showed excellent specific capacitance of 321.95 F g-1 at current density of 0.5 A g-1. In addition, the power and energy densities were obtained as 3588.3 W kg-1, and 44.7 W h kg-1, respectively. The stability of the prepared flexible electrode was tested in galvanostatic charge/discharge cycles, where the results showed the 96.3% retention even after 6000 cycles. These results exhibited that the proposed BN/GrP may be useful to prepare flexible energy-storage systems. Flexible energy storage devices have received great interest due to the increasing demand for wearable and flexible electronic devices with high-power energy sources. Herein, a novel hybrid flexible hexagonal boron nitride integrated graphene paper (BN/GrP) is fabricated from 2D hexagonal boron nitride (h-BN) nanosheets integrated with graphene sheets dispersion via a simple vacuum filtration method. FE-SEM indicated that layered graphene nanosheets tightly confined with h-BN nanosheets. Further, the Raman spectroscopy confirmed successful integration of BN with graphene. As-prepared BN/GrP free-standing flexible conductive paper showed high electrical conductivity of 5.36 × 10 4 S m −1 with the sheet resistance of 8.87 Ω sq −1 . However, after 1000 continuous bending cycles, the BN/GrP sheet resistance increased just about 8.7% which indicated good flexibility of the paper. Furthermore, as-prepared BN/GrP showed excellent specific capacitance of 321.95 F g −1 at current density of 0.5 A g −1 . In addition, the power and energy densities were obtained as 3588.3 W kg −1 , and 44.7 W h kg −1 , respectively. The stability of the prepared flexible electrode was tested in galvanostatic charge/discharge cycles, where the results showed the 96.3% retention even after 6000 cycles. These results exhibited that the proposed BN/GrP may be useful to prepare flexible energy-storage systems. Flexible energy storage devices have received great interest due to the increasing demand for wearable and flexible electronic devices with high-power energy sources. Herein, a novel hybrid flexible hexagonal boron nitride integrated graphene paper (BN/GrP) is fabricated from 2D hexagonal boron nitride (h-BN) nanosheets integrated with graphene sheets dispersion via a simple vacuum filtration method. FE-SEM indicated that layered graphene nanosheets tightly confined with h-BN nanosheets. Further, the Raman spectroscopy confirmed successful integration of BN with graphene. As-prepared BN/GrP free-standing flexible conductive paper showed high electrical conductivity of 5.36 × 104 S m−1 with the sheet resistance of 8.87 Ω sq−1. However, after 1000 continuous bending cycles, the BN/GrP sheet resistance increased just about 8.7% which indicated good flexibility of the paper. Furthermore, as-prepared BN/GrP showed excellent specific capacitance of 321.95 F g−1 at current density of 0.5 A g−1. In addition, the power and energy densities were obtained as 3588.3 W kg−1, and 44.7 W h kg−1, respectively. The stability of the prepared flexible electrode was tested in galvanostatic charge/discharge cycles, where the results showed the 96.3% retention even after 6000 cycles. These results exhibited that the proposed BN/GrP may be useful to prepare flexible energy-storage systems. |
| Author | Rajendran, Jerome Sundramoorthy, Ashok K Reshetilov, Anatoly N |
| AuthorAffiliation | Department of Chemistry SRM Institute of Science and Technology Subdivision of "Federal Research Center Pushchino Biological Research Center of the Russian Academy of Sciences" (FRC PBRC RAS) G.K. Skryabin Institute of Biochemistry and Physiology of Microorganisms of the Russian Academy of Sciences (IBPM RAS) |
| AuthorAffiliation_xml | – name: SRM Institute of Science and Technology – name: Department of Chemistry – name: Subdivision of "Federal Research Center Pushchino Biological Research Center of the Russian Academy of Sciences" (FRC PBRC RAS) – name: G.K. Skryabin Institute of Biochemistry and Physiology of Microorganisms of the Russian Academy of Sciences (IBPM RAS) |
| Author_xml | – sequence: 1 givenname: Jerome surname: Rajendran fullname: Rajendran, Jerome – sequence: 2 givenname: Anatoly N surname: Reshetilov fullname: Reshetilov, Anatoly N – sequence: 3 givenname: Ashok K surname: Sundramoorthy fullname: Sundramoorthy, Ashok K |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/35424276$$D View this record in MEDLINE/PubMed |
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| CitedBy_id | crossref_primary_10_1016_j_jhazmat_2022_129705 crossref_primary_10_3390_en15031162 crossref_primary_10_1007_s44174_024_00226_9 crossref_primary_10_1016_j_nanoen_2022_108060 crossref_primary_10_1039_D3RA06352F crossref_primary_10_1039_D3RA08208C crossref_primary_10_1016_j_chemosphere_2021_132106 crossref_primary_10_1039_D1RA03425A crossref_primary_10_1039_D3RA08312H crossref_primary_10_3390_cryst15010027 crossref_primary_10_1016_j_est_2024_114968 crossref_primary_10_1002_elan_202300093 crossref_primary_10_1021_acs_energyfuels_4c02987 crossref_primary_10_1039_D4RA00361F crossref_primary_10_3390_bios13090839 crossref_primary_10_1039_D3RA06904D crossref_primary_10_1039_D4RA05473C crossref_primary_10_1002_ece2_22 crossref_primary_10_1039_D0MA00974A crossref_primary_10_1016_j_molstruc_2025_141407 crossref_primary_10_1021_acsaelm_4c00709 |
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| Notes | 1 b value of the BN/GrP anodic curve; galvanostatic charge/discharge (GCD) curves for GrP and BN/GrP electrodes at a current density of 1 A g comparison of specific capacitances, retention and power density of the reported supercapacitors were provided. See DOI Electronic supplementary information (ESI) available: Schematic illustration for the preparation of freestanding BN/GrP flexible paper using BN/graphene dispersion, preparation of BN/GrP electrode for electrochemical measurements of supercapacitor; EDX mapping analysis of BN/GrP; the peak current was plotted against the scan rate to determine the 10.1039/d0ra10735b ObjectType-Article-1 SourceType-Scholarly Journals-1 ObjectType-Feature-2 content type line 14 content type line 23 |
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| SubjectTerms | Boron Boron nitride capacitance Chemistry Current density Discharge Dispersion electrical conductivity Electrical resistivity electrochemical capacitors Electrodes Electronic devices energy Energy storage filtration Graphene Nanocomposites nanosheets Nanostructure Raman spectroscopy Storage systems Supercapacitors Vacuum filtration |
| Title | Preparation of hybrid paper electrode based on hexagonal boron nitride integrated graphene nanocomposite for free-standing flexible supercapacitors |
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