The stability of halloysite nanotubes in acidic and alkaline aqueous suspensions
The long term stability of natural halloysite nanotubes was studied at room temperature (22 ± 2 °C) in pure water, acidic and basic aqueous suspensions. The structural and morphological transformations of nanotubes were studied by TEM, SEM, nitrogen adsorption, XRD Raman and FTIR spectroscopy accomp...
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| Published in | Nanotechnology Vol. 23; no. 6; pp. 065705 - 1-10 |
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| Main Authors | , , |
| Format | Journal Article |
| Language | English |
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England
IOP Publishing
17.02.2012
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| Abstract | The long term stability of natural halloysite nanotubes was studied at room temperature (22 ± 2 °C) in pure water, acidic and basic aqueous suspensions. The structural and morphological transformations of nanotubes were studied by TEM, SEM, nitrogen adsorption, XRD Raman and FTIR spectroscopy accompanied by monitoring the concentration of dissolved Si(IV) and Al(III) in solution. It has been revealed that, in 1 mol dm−3 H2SO4 solution, the dissolution of halloysite is initiated on the inner surface of nanotubes, leading to the formation of amorphous spheroidal nanoparticles of SiO2 whereas, in 1 mol dm−3 NaOH solution, dissolution of the inner surface of nanotubes is accompanied by the formation of Al(OH)3 nanosheets. |
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| AbstractList | The long term stability of natural halloysite nanotubes was studied at room temperature (22 plus or minus 2 degree C) in pure water, acidic and basic aqueous suspensions. The structural and morphological transformations of nanotubes were studied by TEM, SEM, nitrogen adsorption, XRD Raman and FTIR spectroscopy accompanied by monitoring the concentration of dissolved Si(IV) and Al(III) in solution. It has been revealed that, in 1 mol dm super(-3) H sub(2)SO sub(4) solution, the dissolution of halloysite is initiated on the inner surface of nanotubes, leading to the formation of amorphous spheroidal nanoparticles of SiO sub(2) whereas, in 1 mol dm super(-3) NaOH solution, dissolution of the inner surface of nanotubes is accompanied by the formation of Al(OH) sub(3) nanosheets. The long term stability of natural halloysite nanotubes was studied at room temperature (22 ± 2 °C) in pure water, acidic and basic aqueous suspensions. The structural and morphological transformations of nanotubes were studied by TEM, SEM, nitrogen adsorption, XRD Raman and FTIR spectroscopy accompanied by monitoring the concentration of dissolved Si(IV) and Al(III) in solution. It has been revealed that, in 1 mol dm−3 H2SO4 solution, the dissolution of halloysite is initiated on the inner surface of nanotubes, leading to the formation of amorphous spheroidal nanoparticles of SiO2 whereas, in 1 mol dm−3 NaOH solution, dissolution of the inner surface of nanotubes is accompanied by the formation of Al(OH)3 nanosheets. The long term stability of natural halloysite nanotubes was studied at room temperature (22 ± 2 °C) in pure water, acidic and basic aqueous suspensions. The structural and morphological transformations of nanotubes were studied by TEM, SEM, nitrogen adsorption, XRD Raman and FTIR spectroscopy accompanied by monitoring the concentration of dissolved Si(IV) and Al(III) in solution. It has been revealed that, in 1 mol dm(-3) H(2)SO(4) solution, the dissolution of halloysite is initiated on the inner surface of nanotubes, leading to the formation of amorphous spheroidal nanoparticles of SiO(2) whereas, in 1 mol dm(-3) NaOH solution, dissolution of the inner surface of nanotubes is accompanied by the formation of Al(OH)(3) nanosheets. |
| Author | Bavykin, Dmitry V White, Rachel D Walsh, Frank C |
| Author_xml | – sequence: 1 givenname: Rachel D surname: White fullname: White, Rachel D organization: Engineering Sciences, University of Southampton Materials Engineering and Energy Technology Research Groups, Southampton SO17 1BJ, UK – sequence: 2 givenname: Dmitry V surname: Bavykin fullname: Bavykin, Dmitry V email: D.Bavykin@soton.ac.uk organization: Engineering Sciences, University of Southampton Materials Engineering and Energy Technology Research Groups, Southampton SO17 1BJ, UK – sequence: 3 givenname: Frank C surname: Walsh fullname: Walsh, Frank C organization: Engineering Sciences, University of Southampton Materials Engineering and Energy Technology Research Groups, Southampton SO17 1BJ, UK |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/22248689$$D View this record in MEDLINE/PubMed |
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| Snippet | The long term stability of natural halloysite nanotubes was studied at room temperature (22 ± 2 °C) in pure water, acidic and basic aqueous suspensions. The... The long term stability of natural halloysite nanotubes was studied at room temperature (22 ± 2 °C) in pure water, acidic and basic aqueous suspensions. The... The long term stability of natural halloysite nanotubes was studied at room temperature (22 plus or minus 2 degree C) in pure water, acidic and basic aqueous... |
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| SubjectTerms | Acids - chemistry Alkalies - chemistry Aluminum Silicates - chemistry Dissolution Monitoring Nanocomposites Nanomaterials Nanostructure Nanotubes Nanotubes - chemistry Nanotubes - ultrastructure Stability Surface chemistry Suspensions Water - chemistry |
| Title | The stability of halloysite nanotubes in acidic and alkaline aqueous suspensions |
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