A mechanochemically synthesized covalent organic framework as a proton-conducting solid electrolyte
Mechanochemistry has become an increasingly important synthetic tool for a waste-free environment. However, the poor quality of the so-derived materials in terms of their crystallinity and porosity has been their major drawback for any practical applications. In this report, we have for the first ti...
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| Published in | Journal of materials chemistry. A, Materials for energy and sustainability Vol. 4; no. 7; pp. 2682 - 269 |
|---|---|
| Main Authors | , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
01.01.2016
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| Subjects | |
| Online Access | Get full text |
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| Abstract | Mechanochemistry has become an increasingly important synthetic tool for a waste-free environment. However, the poor quality of the so-derived materials in terms of their crystallinity and porosity has been their major drawback for any practical applications. In this report, we have for the first time successfully leveraged such characteristics to show that the mechanochemically synthesized bipyridine based covalent organic framework (COF) outperforms its conventional solvothermal counterpart as an efficient solid-state electrolyte in PEM fuel cells. Marking the first such attempt in COFs, a Membrane Electrode Assembly (MEA) fabricated using the mechanochemically synthesized COF was observed to inhibit the fuel crossover and build up a stable Open Circuit Voltage (OCV = 0.93 V at 50 °C), thereby establishing itself as an effective solid electrolyte material (with a proton conductivity of 1.4 × 10
−2
S cm
−1
), while the solvothermally synthesized COF proved ineffective under similar conditions.
Mechanochemically synthesized bipyridine based covalent organic framework showing high proton conductivity of 0.014 S cm
−1
with improved performance over the solvothermal one giving a stable Open Circuit Voltage (0.93 V at 50 °C) on fabrication in PEM fuel cell. |
|---|---|
| AbstractList | Mechanochemistry has become an increasingly important synthetic tool for a waste-free environment. However, the poor quality of the so-derived materials in terms of their crystallinity and porosity has been their major drawback for any practical applications. In this report, we have for the first time successfully leveraged such characteristics to show that the mechanochemically synthesized bipyridine based covalent organic framework (COF) outperforms its conventional solvothermal counterpart as an efficient solid-state electrolyte in PEM fuel cells. Marking the first such attempt in COFs, a Membrane Electrode Assembly (MEA) fabricated using the mechanochemically synthesized COF was observed to inhibit the fuel crossover and build up a stable Open Circuit Voltage (OCV = 0.93 V at 50 °C), thereby establishing itself as an effective solid electrolyte material (with a proton conductivity of 1.4 × 10
−2
S cm
−1
), while the solvothermally synthesized COF proved ineffective under similar conditions.
Mechanochemically synthesized bipyridine based covalent organic framework showing high proton conductivity of 0.014 S cm
−1
with improved performance over the solvothermal one giving a stable Open Circuit Voltage (0.93 V at 50 °C) on fabrication in PEM fuel cell. Mechanochemistry has become an increasingly important synthetic tool for a waste-free environment. However, the poor quality of the so-derived materials in terms of their crystallinity and porosity has been their major drawback for any practical applications. In this report, we have for the first time successfully leveraged such characteristics to show that the mechanochemically synthesized bipyridine based covalent organic framework (COF) outperforms its conventional solvothermal counterpart as an efficient solid-state electrolyte in PEM fuel cells. Marking the first such attempt in COFs, a Membrane Electrode Assembly (MEA) fabricated using the mechanochemically synthesized COF was observed to inhibit the fuel crossover and build up a stable Open Circuit Voltage (OCV = 0.93 V at 50 degree C), thereby establishing itself as an effective solid electrolyte material (with a proton conductivity of 1.4 10 super(-2) S cm super(-1)), while the solvothermally synthesized COF proved ineffective under similar conditions. Mechanochemistry has become an increasingly important synthetic tool for a waste-free environment. However, the poor quality of the so-derived materials in terms of their crystallinity and porosity has been their major drawback for any practical applications. In this report, we have for the first time successfully leveraged such characteristics to show that the mechanochemically synthesized bipyridine based covalent organic framework (COF) outperforms its conventional solvothermal counterpart as an efficient solid-state electrolyte in PEM fuel cells. Marking the first such attempt in COFs, a Membrane Electrode Assembly (MEA) fabricated using the mechanochemically synthesized COF was observed to inhibit the fuel crossover and build up a stable Open Circuit Voltage (OCV = 0.93 V at 50 °C), thereby establishing itself as an effective solid electrolyte material (with a proton conductivity of 1.4 × 10⁻² S cm⁻¹), while the solvothermally synthesized COF proved ineffective under similar conditions. Mechanochemistry has become an increasingly important synthetic tool for a waste-free environment. However, the poor quality of the so-derived materials in terms of their crystallinity and porosity has been their major drawback for any practical applications. In this report, we have for the first time successfully leveraged such characteristics to show that the mechanochemically synthesized bipyridine based covalent organic framework (COF) outperforms its conventional solvothermal counterpart as an efficient solid-state electrolyte in PEM fuel cells. Marking the first such attempt in COFs, a Membrane Electrode Assembly (MEA) fabricated using the mechanochemically synthesized COF was observed to inhibit the fuel crossover and build up a stable Open Circuit Voltage (OCV = 0.93 V at 50 °C), thereby establishing itself as an effective solid electrolyte material (with a proton conductivity of 1.4 × 10 −2 S cm −1 ), while the solvothermally synthesized COF proved ineffective under similar conditions. |
| Author | Kurungot, Sreekumar Bhadra, Mohitosh Aiyappa, Harshitha Barike Shinde, Digambar Balaji Wadge, Pritish Banerjee, Rahul Garai, Bikash Biswal, Bishnu P Kandambeth, Sharath Kundu, Tanay |
| AuthorAffiliation | Academy of Scientific and Innovative Research (AcSIR) CSIR-National Chemical Laboratory Physical/Materials Chemistry Division |
| AuthorAffiliation_xml | – sequence: 0 name: CSIR-National Chemical Laboratory – sequence: 0 name: Academy of Scientific and Innovative Research (AcSIR) – sequence: 0 name: Physical/Materials Chemistry Division |
| Author_xml | – sequence: 1 givenname: Digambar Balaji surname: Shinde fullname: Shinde, Digambar Balaji – sequence: 2 givenname: Harshitha Barike surname: Aiyappa fullname: Aiyappa, Harshitha Barike – sequence: 3 givenname: Mohitosh surname: Bhadra fullname: Bhadra, Mohitosh – sequence: 4 givenname: Bishnu P surname: Biswal fullname: Biswal, Bishnu P – sequence: 5 givenname: Pritish surname: Wadge fullname: Wadge, Pritish – sequence: 6 givenname: Sharath surname: Kandambeth fullname: Kandambeth, Sharath – sequence: 7 givenname: Bikash surname: Garai fullname: Garai, Bikash – sequence: 8 givenname: Tanay surname: Kundu fullname: Kundu, Tanay – sequence: 9 givenname: Sreekumar surname: Kurungot fullname: Kurungot, Sreekumar – sequence: 10 givenname: Rahul surname: Banerjee fullname: Banerjee, Rahul |
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| Snippet | Mechanochemistry has become an increasingly important synthetic tool for a waste-free environment. However, the poor quality of the so-derived materials in... |
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| SubjectTerms | Assembly Covalence crystal structure Crystallinity electric potential difference Electrodes Electrolytes fuel cells fuels Mechanochemistry Open circuit voltage porosity Solid electrolytes |
| Title | A mechanochemically synthesized covalent organic framework as a proton-conducting solid electrolyte |
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