Gas permeation parameters of mixed matrix membranes based on the polymer of intrinsic microporosity PIM-1 and the zeolitic imidazolate framework ZIF-8
Mixed matrix membranes (MMMs) based on the polymer of intrinsic microporosity PIM-1 and the zeolitic imidazolate framework ZIF-8 were prepared and their permeation and sorption properties investigated. Self-supported films with ZIF-8 contents up to 43vol% were studied using GC gas permeation apparat...
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| Published in | Journal of membrane science Vol. 427; no. 15; pp. 48 - 62 |
|---|---|
| Main Authors | , , , , , , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Amsterdam
Elsevier B.V
01.01.2013
Elsevier |
| Subjects | |
| Online Access | Get full text |
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| Abstract | Mixed matrix membranes (MMMs) based on the polymer of intrinsic microporosity PIM-1 and the zeolitic imidazolate framework ZIF-8 were prepared and their permeation and sorption properties investigated. Self-supported films with ZIF-8 contents up to 43vol% were studied using GC gas permeation apparatus and a McBain sorption microbalance. Permeability coefficients were determined for the following set of gases: He, H2, O2, N2, CO2, CH4. For “as-cast” films, an increase in ZIF-8 loading results in increases in the permeability and diffusion coefficients as well as in the separation factors α(H2/N2), α(H2/CH4), α(He/N2), α(O2/N2) and α(CO2/CH4). For all ZIF-8 contents studied, permeability is enhanced by treatment with ethanol. Data points on several Robeson diagrams are located above the 2008 upper bound. Free volume in MMMs containing ZIF-8 was studied using positron annihilation lifetime spectroscopy (PALS) and radio thermoluminescence (RTL) methods. It was shown that the introduction of ZIF-8 nanoparticles into the PIM-1 matrix results in an increase in free volume which may be assumed to arise from a combination of the contributions cavities and of more loosely packed polymer chains at the boundary between ZIF-8 particles and the PIM-1 matrix. The results obtained for the PIM-1/ZIF-8 MMMs are compared with literature data for other MMMs.
► Preparation of a new type of mixed matrix membranes (MMM) based on PIM-1 and ZIF-8. ► Increase in permeability and separation factors of MMM with increase in the content of ZIF-8. ► Sorption isotherms of CO2 in MMM with varying content of ZIF-8. ► Increase in free volume due to the introduction of ZIF-8 into PIM-1 matrix. ► Robeson diagrams: the data points of various PIM-1/ZIF-8 compositions are above the upper bounds for different gas pairs. |
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| AbstractList | Mixed matrix membranes (MMMs) based on the polymer of intrinsic microporosity PIM-1 and the zeolitic imidazolate framework ZIF-8 were prepared and their permeation and sorption properties investigated. Self-supported films with ZIF-8 contents up to 43vol% were studied using GC gas permeation apparatus and a McBain sorption microbalance. Permeability coefficients were determined for the following set of gases: He, H₂, O₂, N₂, CO₂, CH₄. For “as-cast” films, an increase in ZIF-8 loading results in increases in the permeability and diffusion coefficients as well as in the separation factors α(H₂/N₂), α(H₂/CH₄), α(He/N₂), α(O₂/N₂) and α(CO₂/CH₄). For all ZIF-8 contents studied, permeability is enhanced by treatment with ethanol. Data points on several Robeson diagrams are located above the 2008 upper bound. Free volume in MMMs containing ZIF-8 was studied using positron annihilation lifetime spectroscopy (PALS) and radio thermoluminescence (RTL) methods. It was shown that the introduction of ZIF-8 nanoparticles into the PIM-1 matrix results in an increase in free volume which may be assumed to arise from a combination of the contributions cavities and of more loosely packed polymer chains at the boundary between ZIF-8 particles and the PIM-1 matrix. The results obtained for the PIM-1/ZIF-8 MMMs are compared with literature data for other MMMs. Mixed matrix membranes (MMMs) based on the polymer of intrinsic microporosity PIM-1 and the zeolitic imidazolate framework ZIF-8 were prepared and their permeation and sorption properties investigated. Self-supported films with ZIF-8 contents up to 43vol% were studied using GC gas permeation apparatus and a McBain sorption microbalance. Permeability coefficients were determined for the following set of gases: He, H2, O2, N2, CO2, CH4. For “as-cast” films, an increase in ZIF-8 loading results in increases in the permeability and diffusion coefficients as well as in the separation factors α(H2/N2), α(H2/CH4), α(He/N2), α(O2/N2) and α(CO2/CH4). For all ZIF-8 contents studied, permeability is enhanced by treatment with ethanol. Data points on several Robeson diagrams are located above the 2008 upper bound. Free volume in MMMs containing ZIF-8 was studied using positron annihilation lifetime spectroscopy (PALS) and radio thermoluminescence (RTL) methods. It was shown that the introduction of ZIF-8 nanoparticles into the PIM-1 matrix results in an increase in free volume which may be assumed to arise from a combination of the contributions cavities and of more loosely packed polymer chains at the boundary between ZIF-8 particles and the PIM-1 matrix. The results obtained for the PIM-1/ZIF-8 MMMs are compared with literature data for other MMMs. ► Preparation of a new type of mixed matrix membranes (MMM) based on PIM-1 and ZIF-8. ► Increase in permeability and separation factors of MMM with increase in the content of ZIF-8. ► Sorption isotherms of CO2 in MMM with varying content of ZIF-8. ► Increase in free volume due to the introduction of ZIF-8 into PIM-1 matrix. ► Robeson diagrams: the data points of various PIM-1/ZIF-8 compositions are above the upper bounds for different gas pairs. |
| Author | Attfield, Martin P. Rebrov, Alexander Yampolskii, Yuri Shantarovich, Victor Lanč, Marek Gustov, Vadim Isaeva, Vera Starannikova, Ludmila Friess, Karel Mason, Christopher R. Bernardo, Paola Bushell, Alexandra F. Budd, Peter M. Bazzarelli, Fabio Carolus Jansen, Johannes |
| Author_xml | – sequence: 1 givenname: Alexandra F. surname: Bushell fullname: Bushell, Alexandra F. organization: School of Chemistry, University of Manchester, Manchester, M13 9PL, United Kingdom – sequence: 2 givenname: Martin P. surname: Attfield fullname: Attfield, Martin P. organization: School of Chemistry, University of Manchester, Manchester, M13 9PL, United Kingdom – sequence: 3 givenname: Christopher R. surname: Mason fullname: Mason, Christopher R. organization: School of Chemistry, University of Manchester, Manchester, M13 9PL, United Kingdom – sequence: 4 givenname: Peter M. surname: Budd fullname: Budd, Peter M. organization: School of Chemistry, University of Manchester, Manchester, M13 9PL, United Kingdom – sequence: 5 givenname: Yuri surname: Yampolskii fullname: Yampolskii, Yuri email: Yampol@ips.ac.ru organization: A. V. Topchiev Institute of Petrochemical Synthesis (TIPS), RAS, Russia – sequence: 6 givenname: Ludmila surname: Starannikova fullname: Starannikova, Ludmila organization: A. V. Topchiev Institute of Petrochemical Synthesis (TIPS), RAS, Russia – sequence: 7 givenname: Alexander surname: Rebrov fullname: Rebrov, Alexander organization: A. V. Topchiev Institute of Petrochemical Synthesis (TIPS), RAS, Russia – sequence: 8 givenname: Fabio surname: Bazzarelli fullname: Bazzarelli, Fabio organization: Institute on Membrane Technology, ITM-CNR, Rende, CS, Italy – sequence: 9 givenname: Paola surname: Bernardo fullname: Bernardo, Paola organization: Institute on Membrane Technology, ITM-CNR, Rende, CS, Italy – sequence: 10 givenname: Johannes surname: Carolus Jansen fullname: Carolus Jansen, Johannes organization: Institute on Membrane Technology, ITM-CNR, Rende, CS, Italy – sequence: 11 givenname: Marek surname: Lanč fullname: Lanč, Marek organization: Institute of Chemical Technology, Prague, Czech Republic – sequence: 12 givenname: Karel surname: Friess fullname: Friess, Karel organization: Institute of Chemical Technology, Prague, Czech Republic – sequence: 13 givenname: Victor surname: Shantarovich fullname: Shantarovich, Victor organization: N. N. Semenov Institute of Chemical Physics, RAS, Russia – sequence: 14 givenname: Vadim surname: Gustov fullname: Gustov, Vadim organization: N. N. Semenov Institute of Chemical Physics, RAS, Russia – sequence: 15 givenname: Vera surname: Isaeva fullname: Isaeva, Vera organization: N. D. Zelinsky Institute of Organic Chemistry, RAS, Russia |
| BackLink | http://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=26731342$$DView record in Pascal Francis |
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| CODEN | JMESDO |
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| SubjectTerms | artificial membranes carbon dioxide Diffusion coefficients diffusivity ethanol Free volume Gas permeability gases hydrogen methane Mixed matrix membranes nanoparticles nitrogen oxygen permeability Permeability–permselectivity diagrams polymers radio sorption Sorption isotherms spectroscopy thermoluminescence |
| Title | Gas permeation parameters of mixed matrix membranes based on the polymer of intrinsic microporosity PIM-1 and the zeolitic imidazolate framework ZIF-8 |
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