A comparison of the environmental impact of pesticide multiresidues and their occurrence in river waters surveyed by liquid chromatography coupled in tandem with UV diode array detection and mass spectrometry
Twenty-two pesticides and metabolites selected on the basis of a regional priority list, were surveyed in surface river waters by high performance liquid chromatography coupled in tandem with UV diode array detection and mass spectrometry, after an off-line pre-concentration step. Pesticide concentr...
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| Published in | Chemosphere (Oxford) Vol. 55; no. 7; pp. 973 - 981 |
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| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
Oxford
Elsevier Ltd
01.05.2004
Elsevier |
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| Abstract | Twenty-two pesticides and metabolites selected on the basis of a regional priority list, were surveyed in surface river waters by high performance liquid chromatography coupled in tandem with UV diode array detection and mass spectrometry, after an off-line pre-concentration step. Pesticide concentrations ranged between 0.07 and 4.8 μg/l according to the compound and sampling period. Analytical results were linked to the environmental risk of pesticides, evaluated by their system investigation of risk by integration of score (SIRIS) rank. |
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| AbstractList | Twenty-two pesticides and metabolites selected on the basis of a regional priority list, were surveyed in surface river waters by high performance liquid chromatography coupled in tandem with UV diode array detection and mass spectrometry, after an off-line pre-concentration step. Pesticide concentrations ranged between 0.07 and 4.8 microg/l according to the compound and sampling period. Analytical results were linked to the environmental risk of pesticides, evaluated by their system investigation of risk by integration of score (SIRIS) rank. Twenty-two pesticides and metabolites selected on the basis of a regional priority list, were surveyed in surface river waters by high performance liquid chromatography coupled in tandem with UV diode array detection and mass spectrometry, after an off-line pre-concentration step. Pesticide concentrations ranged between 0.07 and 4.8 μg/l according to the compound and sampling period. Analytical results were linked to the environmental risk of pesticides, evaluated by their system investigation of risk by integration of score (SIRIS) rank. Water samples were collected from the Vannetin River at Epauche, France, and pesticide residues were measured using a multi-residue high-performance liquid chromatography method coupled with UV diode array detection and/or mass spectrometry. The Vannetin River is a tributary of the Marne River. The residues detected were compared with those expected from a regional priority list of pesticides based on their use and physicochemical properties. Atrazine, simazine, their metabolites, and metabenzthiazuon were found in all samples at concentrations ranging 0.2 4.8 mu g/l. The analytical methods performed well. Some differences were found between the pesticide occurrences and their regional priority list rankings, indicating the presence of possible flaws in the risk assessment and environmental impact of pesticides. |
| Author | Scribe, P Barcelo, D Irace-Guigand, S Aaron, J.J |
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| Keywords | Environmental analysis Local priority list Multiresidue analysis HPLC Pesticides Rank statistic Chemical analysis Metabolite HPLC chromatography Local priority list: Multiresidue analysis Ultraviolet detector Risk assessment Environment impact Surface water Diode array Stream Water pollution Sampling Degradation product Mass spectrometry Quantitative analysis |
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| Snippet | Twenty-two pesticides and metabolites selected on the basis of a regional priority list, were surveyed in surface river waters by high performance liquid... Water samples were collected from the Vannetin River at Epauche, France, and pesticide residues were measured using a multi-residue high-performance liquid... |
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| SubjectTerms | Applied sciences Chromatography, High Pressure Liquid Continental surface waters detectors Earth sciences Earth, ocean, space Engineering and environment geology. Geothermics Environmental analysis Exact sciences and technology France Hazardous Substances - analysis high performance liquid chromatography HPLC Local priority list Mass Spectrometry metabolites Multiresidue analysis Natural water pollution pesticide residues Pesticide Residues - analysis Pesticides Pollution Pollution, environment geology rivers Rivers - chemistry surface water ultraviolet radiation ultraviolet radiation diode array dectection Ultraviolet Rays water pollution Water treatment and pollution |
| Title | A comparison of the environmental impact of pesticide multiresidues and their occurrence in river waters surveyed by liquid chromatography coupled in tandem with UV diode array detection and mass spectrometry |
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