Preparation and Mechanism of Flame-Retardant Cotton Fabric with Phosphoramidate Siloxane Polymer through Multistep Coating

To improve the water solubility of phosphoramidate siloxane and decrease the amount of flame-retardant additives used in the functional coating for cotton fabrics, a water-soluble phosphoramidate siloxane polymer (PDTSP) was synthesized by sol-gel technology and flame-retardant cotton fabrics were p...

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Published inPolymers Vol. 12; no. 7; p. 1538
Main Authors Xu, Denghui, Wang, Shijie, Wang, Yimin, Liu, Yun, Dong, Chaohong, Jiang, Zhiming, Zhu, Ping
Format Journal Article
LanguageEnglish
Published Basel MDPI AG 12.07.2020
MDPI
Subjects
Additives
Cellulose
Coating
Cotton
Cotton fabrics
Drinking water
Fabrics
flame retardancy
Flame retardants
Flammability
Fourier transforms
Heat measurement
Infrared analysis
Infrared reflection
Infrared spectroscopy
Investigations
multistep coating
Nitrogen
NMR
Nuclear magnetic resonance
Permeability
Phosphorus
Photoelectrons
Polymers
protective char
siloxane polymer
Siloxanes
Sol-gel processes
Solvents
Tensile strength
Textile composites
Textiles
Thermodynamic properties
Thermogravimetric analysis
X ray photoelectron spectroscopy
United States > US
China
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Abstract To improve the water solubility of phosphoramidate siloxane and decrease the amount of flame-retardant additives used in the functional coating for cotton fabrics, a water-soluble phosphoramidate siloxane polymer (PDTSP) was synthesized by sol-gel technology and flame-retardant cotton fabrics were prepared with a multistep coating process. A vertical flammability test, limited oxygen index (LOI), thermogravimetric analysis, and cone calorimetry were performed to investigate the thermal behavior and flame retardancy of PDTSP-coated fabrics. The coated cotton fabrics and their char residues after combustion were studied by attenuated total reflection infrared spectroscopy (FTIR-ATR), scanning electron microscopy (SEM), and X-ray photoelectron spectroscopy (XPS). All results presented that PDTSP-coated cotton fabrics had good flame retardancy and char-forming properties. PDTSP coating was demonstrated to posess gas-phase flame-retardant mechanism as well as a condensed phase flame-retardant mechanism, which can be confirmed by thermogravimetric analysis-Fourier transform infrared spectroscopy (TG-IR) and cone calorimetry test. Also, the preparation process had little effect on the tensile strength of cotton fabrics, although the air permeability and whiteness had a slight decrease. After different washing cycles, the coated samples still maintained good char-forming properties.
AbstractList To improve the water solubility of phosphoramidate siloxane and decrease the amount of flame-retardant additives used in the functional coating for cotton fabrics, a water-soluble phosphoramidate siloxane polymer (PDTSP) was synthesized by sol-gel technology and flame-retardant cotton fabrics were prepared with a multistep coating process. A vertical flammability test, limited oxygen index (LOI), thermogravimetric analysis, and cone calorimetry were performed to investigate the thermal behavior and flame retardancy of PDTSP-coated fabrics. The coated cotton fabrics and their char residues after combustion were studied by attenuated total reflection infrared spectroscopy (FTIR-ATR), scanning electron microscopy (SEM), and X-ray photoelectron spectroscopy (XPS). All results presented that PDTSP-coated cotton fabrics had good flame retardancy and char-forming properties. PDTSP coating was demonstrated to posess gas-phase flame-retardant mechanism as well as a condensed phase flame-retardant mechanism, which can be confirmed by thermogravimetric analysis-Fourier transform infrared spectroscopy (TG-IR) and cone calorimetry test. Also, the preparation process had little effect on the tensile strength of cotton fabrics, although the air permeability and whiteness had a slight decrease. After different washing cycles, the coated samples still maintained good char-forming properties.
Author Dong, Chaohong
Jiang, Zhiming
Xu, Denghui
Wang, Yimin
Liu, Yun
Zhu, Ping
Wang, Shijie
AuthorAffiliation Institute of Functional Textiles and Advanced Materials, College of Textile and Clothing, State Key Laboratory of Bio-Fibers and Eco-Textiles, Qingdao University, Qingdao 266071, China; 18561312665@163.com (D.X.); wsj960912@163.com (S.W.); 17863937942@163.com (Y.W.); liuyun0215@126.com (Y.L.); dongzhh11@163.com (C.D.)
AuthorAffiliation_xml – name: Institute of Functional Textiles and Advanced Materials, College of Textile and Clothing, State Key Laboratory of Bio-Fibers and Eco-Textiles, Qingdao University, Qingdao 266071, China; 18561312665@163.com (D.X.); wsj960912@163.com (S.W.); 17863937942@163.com (Y.W.); liuyun0215@126.com (Y.L.); dongzhh11@163.com (C.D.)
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Snippet To improve the water solubility of phosphoramidate siloxane and decrease the amount of flame-retardant additives used in the functional coating for cotton...
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StartPage 1538
SubjectTerms Additives
Cellulose
Coating
Cotton
Cotton fabrics
Drinking water
Fabrics
flame retardancy
Flame retardants
Flammability
Fourier transforms
Heat measurement
Infrared analysis
Infrared reflection
Infrared spectroscopy
Investigations
multistep coating
Nitrogen
NMR
Nuclear magnetic resonance
Permeability
Phosphorus
Photoelectrons
Polymers
protective char
siloxane polymer
Siloxanes
Sol-gel processes
Solvents
Tensile strength
Textile composites
Textiles
Thermodynamic properties
Thermogravimetric analysis
X ray photoelectron spectroscopy
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Title Preparation and Mechanism of Flame-Retardant Cotton Fabric with Phosphoramidate Siloxane Polymer through Multistep Coating
URI https://www.proquest.com/docview/2424280176
https://search.proquest.com/docview/2424096626
https://pubmed.ncbi.nlm.nih.gov/PMC7408352
https://doaj.org/article/0c18a4d6185f476797bc8f857536d7b1
Volume 12
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