Cellulose Nanocrystals Reinforced Zein/Catechin/β-Cyclodextrin Inclusion Complex Nanoparticles Nanocomposite Film for Active Food Packaging

In this study, following the green, environmentally friendly and sustainable development strategy, cellulose nanocrystals (CNCs) were prepared through a solvent-free esterification reaction between microcrystalline cellulose and maleic anhydride, combined with subsequent ultrasonic treatment, and ma...

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Published inPolymers Vol. 13; no. 16; p. 2759
Main Authors Jiang, Longwei, Han, Yanlong, Meng, Xiangyi, Xiao, Yawen, Zhang, Huajiang
Format Journal Article
LanguageEnglish
Published Basel MDPI AG 17.08.2021
MDPI
Subjects
antioxidant activity
Antioxidants
Aqueous solutions
biodegradable films
Biopolymers
Catechin
Cellulose
Cellulose esters
cellulose nanocrystals
Crystalline cellulose
Cyclodextrins
Elongation
Esterification
Ethanol
Food
food oxidation
Food packaging
Fourier transforms
Hydrogen bonds
Inclusion complexes
Infrared analysis
Maleic anhydride
Morphology
Nanocomposites
Nanocrystals
Nanoparticles
Oxidation
Permeability
Polymers
Scanning electron microscopy
Solvents
Soybeans
Sustainable development
Tensile strength
Ultrasonic processing
Water vapor
Zein
China
Japan
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Abstract In this study, following the green, environmentally friendly and sustainable development strategy, cellulose nanocrystals (CNCs) were prepared through a solvent-free esterification reaction between microcrystalline cellulose and maleic anhydride, combined with subsequent ultrasonic treatment, and maleic-anhydride-modified CNC-reinforced zein/catechin/β-cyclodextrin inclusion complex nanoparticles nanocomposite films were prepared by a facile solution casting. The amount of CNCs in the film matrix was 0–8 wt%, and their effect on structural, physicochemical and functional properties of the resulting films were investigated. SEM images showed that the addition of CNCs made the microstructure of the film more smooth and uniform. The intermolecular hydrogen bonds between CNCs and film matrix were supported by FT-IR. XRD analysis also confirmed the appearance of a crystalline peak due to the existence of CNCs inside the films. The incorporation of CNCs significantly reduced water vapor permeability, water solubility and the swelling degree of the nanocomposite film, and also significantly increased tensile strength and elongation at break from 12.66 to 37.82 MPa and 4.5% to 5.2% (p < 0.05). Moreover, nanocomposite film packaging with CNCs can effectively inhibit the oxidation of soybean oil.
AbstractList In this study, following the green, environmentally friendly and sustainable development strategy, cellulose nanocrystals (CNCs) were prepared through a solvent-free esterification reaction between microcrystalline cellulose and maleic anhydride, combined with subsequent ultrasonic treatment, and maleic-anhydride-modified CNC-reinforced zein/catechin/β-cyclodextrin inclusion complex nanoparticles nanocomposite films were prepared by a facile solution casting. The amount of CNCs in the film matrix was 0–8 wt%, and their effect on structural, physicochemical and functional properties of the resulting films were investigated. SEM images showed that the addition of CNCs made the microstructure of the film more smooth and uniform. The intermolecular hydrogen bonds between CNCs and film matrix were supported by FT-IR. XRD analysis also confirmed the appearance of a crystalline peak due to the existence of CNCs inside the films. The incorporation of CNCs significantly reduced water vapor permeability, water solubility and the swelling degree of the nanocomposite film, and also significantly increased tensile strength and elongation at break from 12.66 to 37.82 MPa and 4.5% to 5.2% ( p < 0.05). Moreover, nanocomposite film packaging with CNCs can effectively inhibit the oxidation of soybean oil.
In this study, following the green, environmentally friendly and sustainable development strategy, cellulose nanocrystals (CNCs) were prepared through a solvent-free esterification reaction between microcrystalline cellulose and maleic anhydride, combined with subsequent ultrasonic treatment, and maleic-anhydride-modified CNC-reinforced zein/catechin/β-cyclodextrin inclusion complex nanoparticles nanocomposite films were prepared by a facile solution casting. The amount of CNCs in the film matrix was 0–8 wt%, and their effect on structural, physicochemical and functional properties of the resulting films were investigated. SEM images showed that the addition of CNCs made the microstructure of the film more smooth and uniform. The intermolecular hydrogen bonds between CNCs and film matrix were supported by FT-IR. XRD analysis also confirmed the appearance of a crystalline peak due to the existence of CNCs inside the films. The incorporation of CNCs significantly reduced water vapor permeability, water solubility and the swelling degree of the nanocomposite film, and also significantly increased tensile strength and elongation at break from 12.66 to 37.82 MPa and 4.5% to 5.2% (p < 0.05). Moreover, nanocomposite film packaging with CNCs can effectively inhibit the oxidation of soybean oil.
Author Meng, Xiangyi
Xiao, Yawen
Zhang, Huajiang
Jiang, Longwei
Han, Yanlong
AuthorAffiliation 1 College of Engineering, Northeast Agricultural University, Harbin 150030, China; hanyl@neau.edu.cn (Y.H.); menxy97@126.com (X.M.); yawenxyw@163.com (Y.X.)
2 College of Food Science, Northeast Agricultural University, Harbin 150030, China
AuthorAffiliation_xml – name: 1 College of Engineering, Northeast Agricultural University, Harbin 150030, China; hanyl@neau.edu.cn (Y.H.); menxy97@126.com (X.M.); yawenxyw@163.com (Y.X.)
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Snippet In this study, following the green, environmentally friendly and sustainable development strategy, cellulose nanocrystals (CNCs) were prepared through a...
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SubjectTerms antioxidant activity
Antioxidants
Aqueous solutions
biodegradable films
Biopolymers
Catechin
Cellulose
Cellulose esters
cellulose nanocrystals
Crystalline cellulose
Cyclodextrins
Elongation
Esterification
Ethanol
Food
food oxidation
Food packaging
Fourier transforms
Hydrogen bonds
Inclusion complexes
Infrared analysis
Maleic anhydride
Morphology
Nanocomposites
Nanocrystals
Nanoparticles
Oxidation
Permeability
Polymers
Scanning electron microscopy
Solvents
Soybeans
Sustainable development
Tensile strength
Ultrasonic processing
Water vapor
Zein
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Title Cellulose Nanocrystals Reinforced Zein/Catechin/β-Cyclodextrin Inclusion Complex Nanoparticles Nanocomposite Film for Active Food Packaging
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https://search.proquest.com/docview/2566034127
https://pubmed.ncbi.nlm.nih.gov/PMC8400103
https://doaj.org/article/a94050c10185473ab306686ef03350f6
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