Measurement of kinetics of Nb(C,N) precipitation using hot torsion testing
Hot torsion stress-relaxation tests can be used to detect P sub s values for austenite of niobium microalloyed steels. Measurement of P sub f times seem to be more difficult to obtain due to strain heterogeneity along the specimen radius inherent to the testing method. A PTT curve was obtained for a...
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Published in | Scripta metallurgica et materialia Vol. 29; no. 7; pp. 881 - 884 |
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Main Authors | , |
Format | Journal Article |
Language | English |
Published |
Seoul
Elsevier B.V
01.10.1993
Oxford Pergamon Press New York, NY |
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Abstract | Hot torsion stress-relaxation tests can be used to detect P sub s values for austenite of niobium microalloyed steels. Measurement of P sub f times seem to be more difficult to obtain due to strain heterogeneity along the specimen radius inherent to the testing method. A PTT curve was obtained for a 0.026C--0.016Ti--0.11Nb--10 ppm N steel for a temperature range of 1023-1323K. Validation of the testing method was obtained by comparing the experimental data with a PTT curve predicted by Dutta and Sellars' model for strain induced precipitation. |
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AbstractList | Precipitation of Nb(C,N) in austenite of microalloyed steels is a well studied subject. Strain induced precipitates play a critical part in retarding recrystallization of austenite in the finishing passes of hot rolling. Hence, knowledge of how precipitation takes place is of major industrial significance. Measurements of fraction precipitated as a function of time at constant temperature (PTT curves) have been obtained through several experimental methods. One of them uses the principle of stress relaxation in axial compression for measurements of kinetics of TiC precipitation in austenite of Ti microalloyed steels. However, the total true deformation that can be applied in compression is usually limited to about 0.8. On the other hand, deformation of austenite in industrial processes is executed in several passes under continuous cooling before precipitation takes place. Successive cycles of deformation followed by recrystallization leads to substantial grain refinement which in turn may effect the process of precipitation. Therefore, the capability of axial compression to reproduce a more realistic hot rolling scenario seems to be very limited as far as austenite conditioning is concerned. A viable alternative may be torsion testing. Hot torsion can be used, for instance, to apply several passes with strains, strain rates, delay times and temperatures similar to those found in an industrial process. It would be then desirable to combine the ability of torsion to simulate industrial schedules with the stress relaxation technique to obtain PTT curves. But before building up PTT curves from simulated as hot rolled' austenite, it is necessary to investigate if torsion experiments are able to detect precipitation. This paper describes an application of torsion testing and the stress relaxation techniques to measure kinetics of precipitation. Hot torsion stress-relaxation tests can be used to detect P sub s values for austenite of niobium microalloyed steels. Measurement of P sub f times seem to be more difficult to obtain due to strain heterogeneity along the specimen radius inherent to the testing method. A PTT curve was obtained for a 0.026C--0.016Ti--0.11Nb--10 ppm N steel for a temperature range of 1023-1323K. Validation of the testing method was obtained by comparing the experimental data with a PTT curve predicted by Dutta and Sellars' model for strain induced precipitation. |
Author | Silveira e Silva, J.M Barbosa, R |
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Cites_doi | 10.1007/BF02670165 10.1179/026708391790184564 10.1007/BF02644407 10.1179/026708387790122846 10.1179/026708392790169821 10.1016/0036-9748(78)90304-6 10.1007/BF02658064 10.1007/BF02654563 10.1016/0956-7151(92)90006-Z 10.1007/BF02647491 10.1007/BF02674014 10.1007/BF02804360 10.2355/isijinternational.29.878 |
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Keywords | Precipitation Microalloyed steel Torsion test Temperature effect Stress relaxation test Kinetics High temperature Experimental study Niobium Carbides nitrides |
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Snippet | Hot torsion stress-relaxation tests can be used to detect P sub s values for austenite of niobium microalloyed steels. Measurement of P sub f times seem to be... Precipitation of Nb(C,N) in austenite of microalloyed steels is a well studied subject. Strain induced precipitates play a critical part in retarding... |
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SubjectTerms | 360202 - Ceramics, Cermets, & Refractories- Structure & Phase Studies ALLOYS Applied sciences AUSTENITIC STEELS CARBIDES CARBON COMPOUNDS Condensed matter: structure, mechanical and thermal properties DEFORMATION Equations of state, phase equilibria, and phase transitions Exact sciences and technology IRON ALLOYS IRON BASE ALLOYS KINETICS MATERIALS SCIENCE Metals. Metallurgy MICROSTRUCTURE NIOBIUM CARBIDES NIOBIUM COMPOUNDS NIOBIUM NITRIDES NITRIDES NITROGEN COMPOUNDS Physics PNICTIDES PRECIPITATION REFRACTORY METAL COMPOUNDS SEPARATION PROCESSES Solubility, segregation, and mixing; phase separation STEELS TORSION TRANSITION ELEMENT COMPOUNDS |
Title | Measurement of kinetics of Nb(C,N) precipitation using hot torsion testing |
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