Measurement of kinetics of Nb(C,N) precipitation using hot torsion testing

Hot torsion stress-relaxation tests can be used to detect P sub s values for austenite of niobium microalloyed steels. Measurement of P sub f times seem to be more difficult to obtain due to strain heterogeneity along the specimen radius inherent to the testing method. A PTT curve was obtained for a...

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Published inScripta metallurgica et materialia Vol. 29; no. 7; pp. 881 - 884
Main Authors Silveira e Silva, J.M, Barbosa, R
Format Journal Article
LanguageEnglish
Published Seoul Elsevier B.V 01.10.1993
Oxford Pergamon Press
New York, NY
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Abstract Hot torsion stress-relaxation tests can be used to detect P sub s values for austenite of niobium microalloyed steels. Measurement of P sub f times seem to be more difficult to obtain due to strain heterogeneity along the specimen radius inherent to the testing method. A PTT curve was obtained for a 0.026C--0.016Ti--0.11Nb--10 ppm N steel for a temperature range of 1023-1323K. Validation of the testing method was obtained by comparing the experimental data with a PTT curve predicted by Dutta and Sellars' model for strain induced precipitation.
AbstractList Precipitation of Nb(C,N) in austenite of microalloyed steels is a well studied subject. Strain induced precipitates play a critical part in retarding recrystallization of austenite in the finishing passes of hot rolling. Hence, knowledge of how precipitation takes place is of major industrial significance. Measurements of fraction precipitated as a function of time at constant temperature (PTT curves) have been obtained through several experimental methods. One of them uses the principle of stress relaxation in axial compression for measurements of kinetics of TiC precipitation in austenite of Ti microalloyed steels. However, the total true deformation that can be applied in compression is usually limited to about 0.8. On the other hand, deformation of austenite in industrial processes is executed in several passes under continuous cooling before precipitation takes place. Successive cycles of deformation followed by recrystallization leads to substantial grain refinement which in turn may effect the process of precipitation. Therefore, the capability of axial compression to reproduce a more realistic hot rolling scenario seems to be very limited as far as austenite conditioning is concerned. A viable alternative may be torsion testing. Hot torsion can be used, for instance, to apply several passes with strains, strain rates, delay times and temperatures similar to those found in an industrial process. It would be then desirable to combine the ability of torsion to simulate industrial schedules with the stress relaxation technique to obtain PTT curves. But before building up PTT curves from simulated as hot rolled' austenite, it is necessary to investigate if torsion experiments are able to detect precipitation. This paper describes an application of torsion testing and the stress relaxation techniques to measure kinetics of precipitation.
Hot torsion stress-relaxation tests can be used to detect P sub s values for austenite of niobium microalloyed steels. Measurement of P sub f times seem to be more difficult to obtain due to strain heterogeneity along the specimen radius inherent to the testing method. A PTT curve was obtained for a 0.026C--0.016Ti--0.11Nb--10 ppm N steel for a temperature range of 1023-1323K. Validation of the testing method was obtained by comparing the experimental data with a PTT curve predicted by Dutta and Sellars' model for strain induced precipitation.
Author Silveira e Silva, J.M
Barbosa, R
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Cites_doi 10.1007/BF02670165
10.1179/026708391790184564
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Issue 7
Keywords Precipitation
Microalloyed steel
Torsion test
Temperature effect
Stress relaxation test
Kinetics
High temperature
Experimental study
Niobium Carbides nitrides
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Snippet Hot torsion stress-relaxation tests can be used to detect P sub s values for austenite of niobium microalloyed steels. Measurement of P sub f times seem to be...
Precipitation of Nb(C,N) in austenite of microalloyed steels is a well studied subject. Strain induced precipitates play a critical part in retarding...
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SubjectTerms 360202 - Ceramics, Cermets, & Refractories- Structure & Phase Studies
ALLOYS
Applied sciences
AUSTENITIC STEELS
CARBIDES
CARBON COMPOUNDS
Condensed matter: structure, mechanical and thermal properties
DEFORMATION
Equations of state, phase equilibria, and phase transitions
Exact sciences and technology
IRON ALLOYS
IRON BASE ALLOYS
KINETICS
MATERIALS SCIENCE
Metals. Metallurgy
MICROSTRUCTURE
NIOBIUM CARBIDES
NIOBIUM COMPOUNDS
NIOBIUM NITRIDES
NITRIDES
NITROGEN COMPOUNDS
Physics
PNICTIDES
PRECIPITATION
REFRACTORY METAL COMPOUNDS
SEPARATION PROCESSES
Solubility, segregation, and mixing; phase separation
STEELS
TORSION
TRANSITION ELEMENT COMPOUNDS
Title Measurement of kinetics of Nb(C,N) precipitation using hot torsion testing
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