Investigation on cristobalite crystallization in silica-based ceramic cores for investment casting

In this work, cristobalite crystallization and its effects on mechanical and chemical behaviour of injection moulded silica-based ceramic cores were investigated. In order to simulate casting process condition, the sintered samples at 1220°C were also heated up to 1430°C. Flexural strength test was...

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Published inJournal of the European Ceramic Society Vol. 33; no. 15-16; pp. 3397 - 3402
Main Authors Kazemi, A., Faghihi-Sani, M.A., Alizadeh, H.R.
Format Journal Article
LanguageEnglish
Published Elsevier Ltd 01.12.2013
Subjects
Ceramic core
Ceramics
Cristobalite
Crystallization
Flexural strength
Fused silica
In situ cristobalite
Investment casting
Leachability
Modulus of rupture in bending
Simulation
Sintering
In situ cristobalite
Ceramic core
Leachability
Fused silica
Crystallization
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Abstract In this work, cristobalite crystallization and its effects on mechanical and chemical behaviour of injection moulded silica-based ceramic cores were investigated. In order to simulate casting process condition, the sintered samples at 1220°C were also heated up to 1430°C. Flexural strength test was carried out on both sintered and heat treated samples. Chemical resistance of the cores was evaluated by leaching the samples inside 43wt% KOH solution at its boiling point. Phase evolution and microstructure were investigated by thermal analyses (DTA and DSC), X-ray diffraction (XRD), scanning electron microscopy (SEM) and optical microscopy (OM). Results showed that cristobalite was crystallized on the surface of fused silica grains at about 1380°C. Flexural strength of the sintered cores was decreased after simulated casting heat treatment due to cristobalite phase transformation. The formed cristobalite on the surface of fused silica grains dramatically decreased the leachability of ceramic cores.
AbstractList The crystallisation of cristobalite and its effects on the mechanical and chemical behaviour of injection moulded silica-based ceramic cores were investigated. To simulate the casting process conditions, the samples sintered at 1220 C were also heated up to 1430 C. Flexural strength tests were carried out on both sintered and heat treated samples and the chemical resistance of the cores was evaluated by leaching the samples in 43 wt% KOH solution at its boiling point. Phase evolution and microstructure were investigated by DTA and DSC, XRD, SEM and optical microscopy. Results showed that cristobalite was crystallised on the surface of the fused silica grains at about 1380 C. The flexural strength of the sintered cores was reduced after casting heat treatment simulation due to cristobalite phase transformation. The cristobalite formed on the surface of the fused silica grains decreased the leachability of the ceramic cores.
In this work, cristobalite crystallization and its effects on mechanical and chemical behaviour of injection moulded silica-based ceramic cores were investigated. In order to simulate casting process condition, the sintered samples at 1220°C were also heated up to 1430°C. Flexural strength test was carried out on both sintered and heat treated samples. Chemical resistance of the cores was evaluated by leaching the samples inside 43wt% KOH solution at its boiling point. Phase evolution and microstructure were investigated by thermal analyses (DTA and DSC), X-ray diffraction (XRD), scanning electron microscopy (SEM) and optical microscopy (OM). Results showed that cristobalite was crystallized on the surface of fused silica grains at about 1380°C. Flexural strength of the sintered cores was decreased after simulated casting heat treatment due to cristobalite phase transformation. The formed cristobalite on the surface of fused silica grains dramatically decreased the leachability of ceramic cores.
Author Alizadeh, H.R.
Kazemi, A.
Faghihi-Sani, M.A.
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Ceramic core
Leachability
Fused silica
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Snippet In this work, cristobalite crystallization and its effects on mechanical and chemical behaviour of injection moulded silica-based ceramic cores were...
The crystallisation of cristobalite and its effects on the mechanical and chemical behaviour of injection moulded silica-based ceramic cores were investigated....
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elsevier
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StartPage 3397
SubjectTerms Ceramic core
Ceramics
Cristobalite
Crystallization
Flexural strength
Fused silica
In situ cristobalite
Investment casting
Leachability
Modulus of rupture in bending
Simulation
Sintering
Title Investigation on cristobalite crystallization in silica-based ceramic cores for investment casting
URI https://dx.doi.org/10.1016/j.jeurceramsoc.2013.06.025
https://search.proquest.com/docview/1494356427
https://search.proquest.com/docview/1692415727
Volume 33
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