Single atom tungsten doped ultrathin α-Ni(OH)2 for enhanced electrocatalytic water oxidation

Electrocatalytic water oxidation is a rate-determining step in the water splitting reaction. Here, we report one single atom W 6+ doped Ni(OH) 2 nanosheet sample (w-Ni(OH) 2 ) with an outstanding oxygen evolution reaction (OER) performance that is, in a 1 M KOH medium, an overpotential of 237 mV is...

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Published in	Nature communications Vol. 10; no. 1; pp. 2149 - 10
Main Authors	Yan, Junqing, Kong, Lingqiao, Ji, Yujin, White, Jai, Li, Youyong, Zhang, Jing, An, Pengfei, Liu, Shengzhong, Lee, Shuit-Tong, Ma, Tianyi
Format	Journal Article
Language	English
Published	London Nature Publishing Group UK 14.05.2019 Nature Publishing Group Nature Portfolio
Subjects	147/135 147/137 147/28 639/638/675 639/638/77/886 639/638/77/887 Clean energy Current density Density functional theory Humanities and Social Sciences multidisciplinary Nanostructure Nickel compounds Oxidation Oxygen Oxygen evolution reactions Science Science (multidisciplinary) Tungsten Water splitting
Online Access	Get full text
ISSN	2041-1723 2041-1723
DOI	10.1038/s41467-019-09845-z

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Abstract	Electrocatalytic water oxidation is a rate-determining step in the water splitting reaction. Here, we report one single atom W 6+ doped Ni(OH) 2 nanosheet sample (w-Ni(OH) 2 ) with an outstanding oxygen evolution reaction (OER) performance that is, in a 1 M KOH medium, an overpotential of 237 mV is obtained reaching a current density of 10 mA/cm 2 . Moreover, at high current density of 80 mA/cm 2 , the overpotential value is 267 mV. The corresponding Tafel slope is measured to be 33 mV/dec. The d 0 W 6+ atom with a low spin-state has more outermost vacant orbitals, resulting in more water and OH − groups being adsorbed on the exposed W sites of the Ni(OH) 2 nanosheet. Density functional theory (DFT) calculations confirm that the O radical and O-O coupling are both generated at the same site of W 6+ . This work demonstrates that W 6+ doping can promote the electrocatalytic water oxidation activity of Ni(OH) 2 with the highest performance. Electrocatalytic water splitting for hydrogen and oxygen generation provides an attractive path to obtain clean energy, but the half reaction of oxygen evolution remains the bottleneck for the progress. Here, the authors show single atom tungsten doped ultrathin α-Ni(OH) 2 exhibits enhanced performance in electrocatalytic water oxidation.
AbstractList	Electrocatalytic water oxidation is a rate-determining step in the water splitting reaction. Here, we report one single atom W 6+ doped Ni(OH) 2 nanosheet sample (w-Ni(OH) 2 ) with an outstanding oxygen evolution reaction (OER) performance that is, in a 1 M KOH medium, an overpotential of 237 mV is obtained reaching a current density of 10 mA/cm 2 . Moreover, at high current density of 80 mA/cm 2 , the overpotential value is 267 mV. The corresponding Tafel slope is measured to be 33 mV/dec. The d 0 W 6+ atom with a low spin-state has more outermost vacant orbitals, resulting in more water and OH − groups being adsorbed on the exposed W sites of the Ni(OH) 2 nanosheet. Density functional theory (DFT) calculations confirm that the O radical and O-O coupling are both generated at the same site of W 6+ . This work demonstrates that W 6+ doping can promote the electrocatalytic water oxidation activity of Ni(OH) 2 with the highest performance. Electrocatalytic water splitting for hydrogen and oxygen generation provides an attractive path to obtain clean energy, but the half reaction of oxygen evolution remains the bottleneck for the progress. Here, the authors show single atom tungsten doped ultrathin α-Ni(OH) 2 exhibits enhanced performance in electrocatalytic water oxidation. Electrocatalytic water oxidation is a rate-determining step in the water splitting reaction. Here, we report one single atom W doped Ni(OH) nanosheet sample (w-Ni(OH) ) with an outstanding oxygen evolution reaction (OER) performance that is, in a 1 M KOH medium, an overpotential of 237 mV is obtained reaching a current density of 10 mA/cm . Moreover, at high current density of 80 mA/cm , the overpotential value is 267 mV. The corresponding Tafel slope is measured to be 33 mV/dec. The d W atom with a low spin-state has more outermost vacant orbitals, resulting in more water and OH groups being adsorbed on the exposed W sites of the Ni(OH) nanosheet. Density functional theory (DFT) calculations confirm that the O radical and O-O coupling are both generated at the same site of W . This work demonstrates that W doping can promote the electrocatalytic water oxidation activity of Ni(OH) with the highest performance. Electrocatalytic water oxidation is a rate-determining step in the water splitting reaction. Here, we report one single atom W 6+ doped Ni(OH) 2 nanosheet sample (w-Ni(OH) 2 ) with an outstanding oxygen evolution reaction (OER) performance that is, in a 1 M KOH medium, an overpotential of 237 mV is obtained reaching a current density of 10 mA/cm 2 . Moreover, at high current density of 80 mA/cm 2 , the overpotential value is 267 mV. The corresponding Tafel slope is measured to be 33 mV/dec. The d 0 W 6+ atom with a low spin-state has more outermost vacant orbitals, resulting in more water and OH − groups being adsorbed on the exposed W sites of the Ni(OH) 2 nanosheet. Density functional theory (DFT) calculations confirm that the O radical and O-O coupling are both generated at the same site of W 6+ . This work demonstrates that W 6+ doping can promote the electrocatalytic water oxidation activity of Ni(OH) 2 with the highest performance. Electrocatalytic water oxidation is a rate-determining step in the water splitting reaction. Here, we report one single atom W6+ doped Ni(OH)2 nanosheet sample (w-Ni(OH)2) with an outstanding oxygen evolution reaction (OER) performance that is, in a 1 M KOH medium, an overpotential of 237 mV is obtained reaching a current density of 10 mA/cm2. Moreover, at high current density of 80 mA/cm2, the overpotential value is 267 mV. The corresponding Tafel slope is measured to be 33 mV/dec. The d0 W6+ atom with a low spin-state has more outermost vacant orbitals, resulting in more water and OH- groups being adsorbed on the exposed W sites of the Ni(OH)2 nanosheet. Density functional theory (DFT) calculations confirm that the O radical and O-O coupling are both generated at the same site of W6+. This work demonstrates that W6+ doping can promote the electrocatalytic water oxidation activity of Ni(OH)2 with the highest performance.Electrocatalytic water oxidation is a rate-determining step in the water splitting reaction. Here, we report one single atom W6+ doped Ni(OH)2 nanosheet sample (w-Ni(OH)2) with an outstanding oxygen evolution reaction (OER) performance that is, in a 1 M KOH medium, an overpotential of 237 mV is obtained reaching a current density of 10 mA/cm2. Moreover, at high current density of 80 mA/cm2, the overpotential value is 267 mV. The corresponding Tafel slope is measured to be 33 mV/dec. The d0 W6+ atom with a low spin-state has more outermost vacant orbitals, resulting in more water and OH- groups being adsorbed on the exposed W sites of the Ni(OH)2 nanosheet. Density functional theory (DFT) calculations confirm that the O radical and O-O coupling are both generated at the same site of W6+. This work demonstrates that W6+ doping can promote the electrocatalytic water oxidation activity of Ni(OH)2 with the highest performance. Electrocatalytic water oxidation is a rate-determining step in the water splitting reaction. Here, we report one single atom W6+ doped Ni(OH)2 nanosheet sample (w-Ni(OH)2) with an outstanding oxygen evolution reaction (OER) performance that is, in a 1 M KOH medium, an overpotential of 237 mV is obtained reaching a current density of 10 mA/cm2. Moreover, at high current density of 80 mA/cm2, the overpotential value is 267 mV. The corresponding Tafel slope is measured to be 33 mV/dec. The d0 W6+ atom with a low spin-state has more outermost vacant orbitals, resulting in more water and OH− groups being adsorbed on the exposed W sites of the Ni(OH)2 nanosheet. Density functional theory (DFT) calculations confirm that the O radical and O-O coupling are both generated at the same site of W6+. This work demonstrates that W6+ doping can promote the electrocatalytic water oxidation activity of Ni(OH)2 with the highest performance.Electrocatalytic water splitting for hydrogen and oxygen generation provides an attractive path to obtain clean energy, but the half reaction of oxygen evolution remains the bottleneck for the progress. Here, the authors show single atom tungsten doped ultrathin α-Ni(OH)2 exhibits enhanced performance in electrocatalytic water oxidation. Electrocatalytic water splitting for hydrogen and oxygen generation provides an attractive path to obtain clean energy, but the half reaction of oxygen evolution remains the bottleneck for the progress. Here, the authors show single atom tungsten doped ultrathin α-Ni(OH)2 exhibits enhanced performance in electrocatalytic water oxidation.
ArticleNumber	2149
Author	Kong, Lingqiao White, Jai Zhang, Jing Yan, Junqing Liu, Shengzhong Li, Youyong Ma, Tianyi An, Pengfei Lee, Shuit-Tong Ji, Yujin
Author_xml	– sequence: 1 givenname: Junqing orcidid: 0000-0002-9966-6237 surname: Yan fullname: Yan, Junqing organization: Key Laboratory of Applied Surface and Colloid Chemistry, Ministry of Education; Shaanxi Engineering Lab for Advanced Energy Technology, School of Materials Science and Engineering, Shaanxi Normal University – sequence: 2 givenname: Lingqiao surname: Kong fullname: Kong, Lingqiao organization: Key Laboratory of Applied Surface and Colloid Chemistry, Ministry of Education; Shaanxi Engineering Lab for Advanced Energy Technology, School of Materials Science and Engineering, Shaanxi Normal University – sequence: 3 givenname: Yujin surname: Ji fullname: Ji, Yujin organization: Institute of Functional Nano & Soft Materials (FUNSOM), Jiangsu Key Laboratory for Carbon-Based Functional Materials & Devices, Soochow University – sequence: 4 givenname: Jai surname: White fullname: White, Jai organization: Discipline of Chemistry, School of Environmental and Life Sciences, University of Newcastle – sequence: 5 givenname: Youyong orcidid: 0000-0002-5248-2756 surname: Li fullname: Li, Youyong email: yyli@suda.edu.cn organization: Institute of Functional Nano & Soft Materials (FUNSOM), Jiangsu Key Laboratory for Carbon-Based Functional Materials & Devices, Soochow University – sequence: 6 givenname: Jing surname: Zhang fullname: Zhang, Jing organization: Beijing Synchrotron Radiation Facility, Institute of High Energy Physics, Chinese Academy of Sciences – sequence: 7 givenname: Pengfei surname: An fullname: An, Pengfei organization: Beijing Synchrotron Radiation Facility, Institute of High Energy Physics, Chinese Academy of Sciences – sequence: 8 givenname: Shengzhong surname: Liu fullname: Liu, Shengzhong email: liusz@snnu.edu.cn organization: Key Laboratory of Applied Surface and Colloid Chemistry, Ministry of Education; Shaanxi Engineering Lab for Advanced Energy Technology, School of Materials Science and Engineering, Shaanxi Normal University, iChEM, Dalian Institute of Chemical Physics, Dalian National Laboratory for Clean Energy, Chinese Academy of Sciences – sequence: 9 givenname: Shuit-Tong surname: Lee fullname: Lee, Shuit-Tong organization: Institute of Functional Nano & Soft Materials (FUNSOM), Jiangsu Key Laboratory for Carbon-Based Functional Materials & Devices, Soochow University – sequence: 10 givenname: Tianyi orcidid: 0000-0002-1042-8700 surname: Ma fullname: Ma, Tianyi email: tianyi.ma@newcastle.edu.au organization: Discipline of Chemistry, School of Environmental and Life Sciences, University of Newcastle
BackLink	https://www.ncbi.nlm.nih.gov/pubmed/31089139$$D View this record in MEDLINE/PubMed
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Snippet	Electrocatalytic water oxidation is a rate-determining step in the water splitting reaction. Here, we report one single atom W 6+ doped Ni(OH) 2 nanosheet... Electrocatalytic water oxidation is a rate-determining step in the water splitting reaction. Here, we report one single atom W doped Ni(OH) nanosheet sample... Electrocatalytic water oxidation is a rate-determining step in the water splitting reaction. Here, we report one single atom W6+ doped Ni(OH)2 nanosheet sample... Electrocatalytic water splitting for hydrogen and oxygen generation provides an attractive path to obtain clean energy, but the half reaction of oxygen...
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SubjectTerms	147/135 147/137 147/28 639/638/675 639/638/77/886 639/638/77/887 Clean energy Current density Density functional theory Humanities and Social Sciences multidisciplinary Nanostructure Nickel compounds Oxidation Oxygen Oxygen evolution reactions Science Science (multidisciplinary) Tungsten Water splitting
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Title	Single atom tungsten doped ultrathin α-Ni(OH)2 for enhanced electrocatalytic water oxidation
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