Stability of radical-functionalized gold surfaces by self-assembly and on-surface chemistry
We have investigated the radical functionalization of gold surfaces with a derivative of the perchlorotriphenylmethyl (PTM) radical using two methods: by chemisorption from the radical solution and by on-surface chemical derivation from a precursor. We have investigated the obtained self-assembled m...
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| Published in | Chemical science (Cambridge) Vol. 11; no. 34; pp. 9162 - 9172 |
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| Main Authors | , , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
England
Royal Society of Chemistry
13.08.2020
The Royal Society of Chemistry |
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| Abstract | We have investigated the radical functionalization of gold surfaces with a derivative of the perchlorotriphenylmethyl (PTM) radical using two methods: by chemisorption from the radical solution and by on-surface chemical derivation from a precursor. We have investigated the obtained self-assembled monolayers by photon-energy dependent X-ray photoelectron spectroscopy. Our results show that the molecules were successfully anchored on the surfaces. We have used a robust method that can be applied to a variety of materials to assess the stability of the functionalized interface. The monolayers are characterized by air and X-ray beam stability unprecedented for films of organic radicals. Over very long X-ray beam exposure we observed a dynamic nature of the radical-Au complex. The results clearly indicate that (mono)layers of PTM radical derivatives have the necessary stability to withstand device applications.
We have investigated the radical functionalization of gold with a derivative of the perchlorotriphenylmethyl radical using two methods: by chemisorption from the radical solution and by on surface chemical derivation from a precursor. |
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| AbstractList | We have investigated the radical functionalization of gold surfaces with a derivative of the perchlorotriphenylmethyl (PTM) radical using two methods: by chemisorption from the radical solution and by on-surface chemical derivation from a precursor. We have investigated the obtained self-assembled monolayers by photon-energy dependent X-ray photoelectron spectroscopy. Our results show that the molecules were successfully anchored on the surfaces. We have used a robust method that can be applied to a variety of materials to assess the stability of the functionalized interface. The monolayers are characterized by air and X-ray beam stability unprecedented for films of organic radicals. Over very long X-ray beam exposure we observed a dynamic nature of the radical-Au complex. The results clearly indicate that (mono)layers of PTM radical derivatives have the necessary stability to withstand device applications. We have investigated the radical functionalization of gold surfaces with a derivative of the perchlorotriphenylmethyl (PTM) radical using two methods: by chemisorption from the radical solution and by on-surface chemical derivation from a precursor. We have investigated the obtained self-assembled monolayers by photon-energy dependent X-ray photoelectron spectroscopy. Our results show that the molecules were successfully anchored on the surfaces. We have used a robust method that can be applied to a variety of materials to assess the stability of the functionalized interface. The monolayers are characterized by air and X-ray beam stability unprecedented for films of organic radicals. Over very long X-ray beam exposure we observed a dynamic nature of the radical–Au complex. The results clearly indicate that (mono)layers of PTM radical derivatives have the necessary stability to withstand device applications. We have investigated the radical functionalization of gold with a derivative of the perchlorotriphenylmethyl radical using two methods: by chemisorption from the radical solution and by on surface chemical derivation from a precursor. We have investigated the radical functionalization of gold surfaces with a derivative of the perchlorotriphenylmethyl (PTM) radical using two methods: by chemisorption from the radical solution and by on-surface chemical derivation from a precursor. We have investigated the obtained self-assembled monolayers by photon-energy dependent X-ray photoelectron spectroscopy. Our results show that the molecules were successfully anchored on the surfaces. We have used a robust method that can be applied to a variety of materials to assess the stability of the functionalized interface. The monolayers are characterized by air and X-ray beam stability unprecedented for films of organic radicals. Over very long X-ray beam exposure we observed a dynamic nature of the radical-Au complex. The results clearly indicate that (mono)layers of PTM radical derivatives have the necessary stability to withstand device applications.We have investigated the radical functionalization of gold surfaces with a derivative of the perchlorotriphenylmethyl (PTM) radical using two methods: by chemisorption from the radical solution and by on-surface chemical derivation from a precursor. We have investigated the obtained self-assembled monolayers by photon-energy dependent X-ray photoelectron spectroscopy. Our results show that the molecules were successfully anchored on the surfaces. We have used a robust method that can be applied to a variety of materials to assess the stability of the functionalized interface. The monolayers are characterized by air and X-ray beam stability unprecedented for films of organic radicals. Over very long X-ray beam exposure we observed a dynamic nature of the radical-Au complex. The results clearly indicate that (mono)layers of PTM radical derivatives have the necessary stability to withstand device applications. |
| Author | Junghoefer, Tobias Giangrisostomi, Erika Mas-Torrent, Marta Crivillers, Núria Rovira, Concepció Chassé, Thomas Veciana, Jaume Casu, Maria Benedetta Nowik-Boltyk, Ewa Malgorzata de Sousa, J. Alejandro Ovsyannikov, Ruslan |
| AuthorAffiliation | Institute of Physical and Theoretical Chemistry Facultad de Ciencias University of Tübingen Universidad de los Andes Helmholtz-Zentrum Berlin für Materialien und Energie (HZB) Networking Research Center on Bioengineering Biomaterials and Nanomedicine (CIBER-BBN) Laboratorio de Electroquímica Institut de Ciència de Materials de Barcelona (ICMAB-CSIC) Departamento de Química |
| AuthorAffiliation_xml | – name: University of Tübingen – name: Universidad de los Andes – name: Facultad de Ciencias – name: Laboratorio de Electroquímica – name: Institut de Ciència de Materials de Barcelona (ICMAB-CSIC) – name: Networking Research Center on Bioengineering Biomaterials and Nanomedicine (CIBER-BBN) – name: Departamento de Química – name: Helmholtz-Zentrum Berlin für Materialien und Energie (HZB) – name: Institute of Physical and Theoretical Chemistry |
| Author_xml | – sequence: 1 givenname: Tobias surname: Junghoefer fullname: Junghoefer, Tobias – sequence: 2 givenname: Ewa Malgorzata surname: Nowik-Boltyk fullname: Nowik-Boltyk, Ewa Malgorzata – sequence: 3 givenname: J. Alejandro surname: de Sousa fullname: de Sousa, J. Alejandro – sequence: 4 givenname: Erika surname: Giangrisostomi fullname: Giangrisostomi, Erika – sequence: 5 givenname: Ruslan surname: Ovsyannikov fullname: Ovsyannikov, Ruslan – sequence: 6 givenname: Thomas surname: Chassé fullname: Chassé, Thomas – sequence: 7 givenname: Jaume surname: Veciana fullname: Veciana, Jaume – sequence: 8 givenname: Marta surname: Mas-Torrent fullname: Mas-Torrent, Marta – sequence: 9 givenname: Concepció surname: Rovira fullname: Rovira, Concepció – sequence: 10 givenname: Núria surname: Crivillers fullname: Crivillers, Núria – sequence: 11 givenname: Maria Benedetta surname: Casu fullname: Casu, Maria Benedetta |
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| Notes | Electronic supplementary information (ESI) available: Survey spectra of SAM2A and fit results for the photoemission lines in the SAM2A C 1s spectra. SAM1 survey, stoichiometric analysis, and fit results for the photoemission lines in the SAM1 C 1s spectra. C 1s core level spectra at 460 and 640 eV. Fit results for SAM2 and SAM4 at 460 eV. Fit results for SAM2 and SAM4 at 640 eV. Electrochemical measurements, stability under air exposure, and stability under X-ray beam exposure. See DOI 10.1039/d0sc03399e ObjectType-Article-1 SourceType-Scholarly Journals-1 ObjectType-Feature-2 content type line 23 These authors contributed equally. |
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| Snippet | We have investigated the radical functionalization of gold surfaces with a derivative of the perchlorotriphenylmethyl (PTM) radical using two methods: by... |
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| SubjectTerms | Chemisorption Chemistry Exposure Gold Interface stability Monolayers Photoelectric emission Photoelectrons Self-assembled monolayers Self-assembly Spectra Stability analysis Surface stability |
| Title | Stability of radical-functionalized gold surfaces by self-assembly and on-surface chemistry |
| URI | https://www.ncbi.nlm.nih.gov/pubmed/34123165 https://www.proquest.com/docview/2439352302 https://www.proquest.com/docview/2540720567/abstract/ https://pubmed.ncbi.nlm.nih.gov/PMC8163401 |
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