Hypervalent aryliodine compounds as precursors for radiofluorination

Over the last 2 decades or so, hypervalent iodine compounds, such as diaryliodonium salts and aryliodonium ylides, have emerged as useful precursors for labeling homoarenes and heteroarenes with no‐carrier‐added cyclotron‐produced [18F]fluoride ion (t1/2 = 109.8 min). They permit rapid and effective...

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Published inJournal of labelled compounds & radiopharmaceuticals Vol. 61; no. 3; pp. 196 - 227
Main Author Pike, Victor W.
Format Journal Article
LanguageEnglish
Published England Wiley Subscription Services, Inc 01.03.2018
Subjects
Aromatic compounds
aryliodonium ylide
Chemical synthesis
Cyclotrons
diaryliodonium salt
fluorine 18
Fluorine isotopes
Fluorine Radioisotopes - chemistry
Iodine compounds
Labeling
Medical imaging
PET
Positron emission
Positron emission tomography
Positron-Emission Tomography - methods
Precursors
radiofluorination
Radiopharmaceuticals - chemical synthesis
radiotracer
Salts
diaryliodonium salt
fluorine 18
aryliodonium ylide
radiofluorination
radiotracer
PET
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Abstract Over the last 2 decades or so, hypervalent iodine compounds, such as diaryliodonium salts and aryliodonium ylides, have emerged as useful precursors for labeling homoarenes and heteroarenes with no‐carrier‐added cyclotron‐produced [18F]fluoride ion (t1/2 = 109.8 min). They permit rapid and effective radiofluorination at electron‐rich as well as electron‐deficient aryl rings, and often with unrestricted choice of ring position. Consequently, hypervalent aryliodine compounds have found special utility as precursors to various small‐molecule 18F‐labeling synthons and to many radiotracers for biomedical imaging with positron emission tomography. This review summarizes this advance in radiofluorination chemistry, with emphasis on precursor synthesis, radiofluorination mechanism, method scope, and method application. Hypervalent iodine compounds, such as diaryliodonium salts and aryliodonium ylides, have emerged as useful precursors for labeling arenes, either as labeling synthons or as PET radiotracers, with no‐carrier‐added [18F]fluoride ion (t1/2 = 109.8 minutes). This review summarizes this advance in radiofluorination chemistry, with emphasis on precursor synthesis, radiofluorination mechanism, method scope, and method application.
AbstractList Over the last 2 decades or so, hypervalent iodine compounds, such as diaryliodonium salts and aryliodonium ylides, have emerged as useful precursors for labeling homoarenes and heteroarenes with no-carrier-added cyclotron-produced [ F]fluoride ion (t  = 109.8 min). They permit rapid and effective radiofluorination at electron-rich as well as electron-deficient aryl rings, and often with unrestricted choice of ring position. Consequently, hypervalent aryliodine compounds have found special utility as precursors to various small-molecule F-labeling synthons and to many radiotracers for biomedical imaging with positron emission tomography. This review summarizes this advance in radiofluorination chemistry, with emphasis on precursor synthesis, radiofluorination mechanism, method scope, and method application.
Over the last 2 decades or so, hypervalent iodine compounds, such as diaryliodonium salts and aryliodonium ylides, have emerged as useful precursors for labeling homoarenes and heteroarenes with no-carrier-added cyclotron-produced [18 F]fluoride ion (t1/2 = 109.8 min). They permit rapid and effective radiofluorination at electron-rich as well as electron-deficient aryl rings, and often with unrestricted choice of ring position. Consequently, hypervalent aryliodine compounds have found special utility as precursors to various small-molecule 18 F-labeling synthons and to many radiotracers for biomedical imaging with positron emission tomography. This review summarizes this advance in radiofluorination chemistry, with emphasis on precursor synthesis, radiofluorination mechanism, method scope, and method application.Over the last 2 decades or so, hypervalent iodine compounds, such as diaryliodonium salts and aryliodonium ylides, have emerged as useful precursors for labeling homoarenes and heteroarenes with no-carrier-added cyclotron-produced [18 F]fluoride ion (t1/2 = 109.8 min). They permit rapid and effective radiofluorination at electron-rich as well as electron-deficient aryl rings, and often with unrestricted choice of ring position. Consequently, hypervalent aryliodine compounds have found special utility as precursors to various small-molecule 18 F-labeling synthons and to many radiotracers for biomedical imaging with positron emission tomography. This review summarizes this advance in radiofluorination chemistry, with emphasis on precursor synthesis, radiofluorination mechanism, method scope, and method application.
Over the last 2 decades or so, hypervalent iodine compounds, such as diaryliodonium salts and aryliodonium ylides, have emerged as useful precursors for labeling homoarenes and heteroarenes with no‐carrier‐added cyclotron‐produced [ 18 F]fluoride ion ( t 1/2  = 109.8 min). They permit rapid and effective radiofluorination at electron‐rich as well as electron‐deficient aryl rings, and often with unrestricted choice of ring position. Consequently, hypervalent aryliodine compounds have found special utility as precursors to various small‐molecule 18 F‐labeling synthons and to many radiotracers for biomedical imaging with positron emission tomography. This review summarizes this advance in radiofluorination chemistry, with emphasis on precursor synthesis, radiofluorination mechanism, method scope, and method application.
Over the last 2 decades or so, hypervalent iodine compounds, such as diaryliodonium salts and aryliodonium ylides, have emerged as useful precursors for labeling homoarenes and heteroarenes with no‐carrier‐added cyclotron‐produced [18F]fluoride ion (t1/2 = 109.8 min). They permit rapid and effective radiofluorination at electron‐rich as well as electron‐deficient aryl rings, and often with unrestricted choice of ring position. Consequently, hypervalent aryliodine compounds have found special utility as precursors to various small‐molecule 18F‐labeling synthons and to many radiotracers for biomedical imaging with positron emission tomography. This review summarizes this advance in radiofluorination chemistry, with emphasis on precursor synthesis, radiofluorination mechanism, method scope, and method application.
Over the last 2 decades or so, hypervalent iodine compounds, such as diaryliodonium salts and aryliodonium ylides, have emerged as useful precursors for labeling homoarenes and heteroarenes with no‐carrier‐added cyclotron‐produced [18F]fluoride ion (t1/2 = 109.8 min). They permit rapid and effective radiofluorination at electron‐rich as well as electron‐deficient aryl rings, and often with unrestricted choice of ring position. Consequently, hypervalent aryliodine compounds have found special utility as precursors to various small‐molecule 18F‐labeling synthons and to many radiotracers for biomedical imaging with positron emission tomography. This review summarizes this advance in radiofluorination chemistry, with emphasis on precursor synthesis, radiofluorination mechanism, method scope, and method application. Hypervalent iodine compounds, such as diaryliodonium salts and aryliodonium ylides, have emerged as useful precursors for labeling arenes, either as labeling synthons or as PET radiotracers, with no‐carrier‐added [18F]fluoride ion (t1/2 = 109.8 minutes). This review summarizes this advance in radiofluorination chemistry, with emphasis on precursor synthesis, radiofluorination mechanism, method scope, and method application.
Author Pike, Victor W.
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  organization: National Institute of Mental Health, National Institutes of Health
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Issue 3
Keywords diaryliodonium salt
fluorine 18
aryliodonium ylide
radiofluorination
radiotracer
PET
Language English
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Snippet Over the last 2 decades or so, hypervalent iodine compounds, such as diaryliodonium salts and aryliodonium ylides, have emerged as useful precursors for...
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SubjectTerms Aromatic compounds
aryliodonium ylide
Chemical synthesis
Cyclotrons
diaryliodonium salt
fluorine 18
Fluorine isotopes
Fluorine Radioisotopes - chemistry
Iodine compounds
Labeling
Medical imaging
PET
Positron emission
Positron emission tomography
Positron-Emission Tomography - methods
Precursors
radiofluorination
Radiopharmaceuticals - chemical synthesis
radiotracer
Salts
Title Hypervalent aryliodine compounds as precursors for radiofluorination
URI https://onlinelibrary.wiley.com/doi/abs/10.1002%2Fjlcr.3570
https://www.ncbi.nlm.nih.gov/pubmed/28981159
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https://www.proquest.com/docview/1947617989
Volume 61
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